• The Transactions of The Korean Institute of Electrical Engineers
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• v.57 no.9
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• pp.1572-1578
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• 2008

The effect of the organoclay_10A nanoparticles on the DSC and Structural and Dielectrics Properties(1Hz-1MHz) for epoxy/Organoclay_10A Nanocomposites has been studied. Dielectric properties of epoxy-Organoclay nanocomposites were investigated at 1, 3, 5, 7, 9 filler concentration by weight. Epoxy nanocomposites samples were prepared with good dispersion of layered silicate using power ultrasonic method in the particles. As structural analysis, the interlayer spacing have decreased with filled nanoparticles contents increase using power ultrasonic dispersion. The maximum increase interlayered spacing was observed to decease for above 5wt% clay loading. The other hand, as decrease with concentration filler of the layered silicate were increased dispersion degree of nanoparticles in the matrix. The interesting dielectric properties for epoxy based nanocomposites systems are attributed to the large volume fraction of interfacesin the bulk of the material and the ensuring interactions between the charged nanoparticle surface and the epoxy chains.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2008.11a
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• pp.287-288
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• 2008

에폭시-층상실리케이트 나노콤포지트의 균질분산과 층상실리케이트내로 침투되는 박리정도를 향상시키기 위해 친환경적 분산기법인 물리적방법으로 Homogenizer와 Power Ultrasonic를 적용한 기법을 실시하였다. Homogenizer의 최적속도를 얻기 위해 분산시킨 나노콤포지트의 박리정도, 유리천이온도를 구할 수 있었고, Homogenizer와 Ultrasonic을 동시에 적용하여 최적시간을 구하기 위해 적용된 나노콤포지트를 절연파괴 강도의 Weibull Plots을 통하여 판단할 수 있는 좋은 결과를 얻을 수 있었다.

• Journal of Power System Engineering
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• v.17 no.6
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• pp.142-148
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• 2013

High-power ultrasonic promotes a chemical reaction by its own energy, thus it has been used for sonochemistry applications. For example, it has been mostly used for mixing, reaction catalyst, dispersion and disintegration. High-power ultrasonic transducer is made with structure based on a Bolt-clamped Langevin type Transducer (BLT), But it has difficulty in the development because degradation of piezoelectric ceramic by the heat generation of BLT. In this study, for a development of the transducer of 25 kHz and 1000 W used in sonochemistry and industrial cleaning, BLT with a hole in its center and tubular type waveguide of the transducer were designed based on finite element method (FEM). The transducer was fabricated based on the design parameter, and the impedance characteristics are measured experimentally and compared with the numerical results.

• Korea-Australia Rheology Journal
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• v.13 no.2
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• pp.61-65
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• 2001

Thermoplastic nanocomposites based on the copolymers of polypropylene (PP)-polystyrene (PS) and organically modified montmorillonite (org-MMT) were produced by using power ultrasonic wave in an intensive mixer. Owing to the unique action of the ultrasonic wave, free radicals of styrene monomers and macroradicals of PP were generated, by which copolymers of PP and PS were formed. Another important aspect of using ultrasonic wave during the mixing process was to enhance nano-scale dispersion of org-MMT by destructing the agglomerates of org-MMT in the polymer matrix. Optimum conditions for the in-situ copolymerization and melt intercalation were studied with various concentrations of styrene monomer, sonication time and different kinds of clay. It was found that a novel attempt carried out in this study yielded further improvement in the mechanical performance of the nanocomposites compared to those produced by the conventional melt mixing process.

• Journal of Power System Engineering
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• v.12 no.1
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• pp.58-65
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• 2008

A method to test thin-walled tubes by guided ultrasonic wave is reported. The principle is that applicate two types of axially symmetric ultrasonic tube modes and "longitudinal" modes with particle displacement, which is coupled in axial and radial directions for transverse failures and torsional modes, oscillating in the circumferential direction only, for longitudinal failures. Both types of modes propagate along the tube in the axial direction. Therefore, a pulse-echo technique is possible. The pulses are excited and received at one end of the tube without contact electro-dynamic transducers. As soon as the tubes is put into a transducer coil at one end, the test of the whole tube can be accomplished in a few milliseconds. It is not necessary to rotate and transport the tubes during the test.

• Journal of the Korean Society for Nondestructive Testing
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• v.24 no.4
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• pp.331-340
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• 2004

Deployment of an advanced on-line monitoring of the component integrity offers a prospect of improved performance, enhanced safety, and reduced overall cost for nuclear power plants. Ultrasonic guided waves have been known as one of the promising techniques that could be utilized for on-line monitoring. The present work is aimed at developing a new method for on-line monitoring of the pipes during the operation period of nuclear power plants. For this purpose, the steam generator (S/G) tube was selected as an object of tile experiment. Dispersion corves and the incident angles corresponding to the specific modes were calculated for the S/G tube. The modes of guided waves were identified by the time-frequency diagrams obtained by the short time Fourier transform. It was experimentally confirmed that there was no mode conversion when the ultrasonic guided waves passed over the curved region of the S/G tube. An optimum mode of guided wave for the S/G tube was suggested and verified by the experiment.

• Korean Journal of Materials Research
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• v.20 no.8
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• pp.439-443
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• 2010

Nano sized SiC particles (270 nm) are easily agglomerated in nickel sulfamate electrolytic bath during a composite electrodeposition process. The agglomeration of nano particles in composite coatings can significantly reduce the mechanical properties of the composite coatings. In this study, Ni-SiC nano composite coatings were fabricated using a conventional electrodeposition process with the aid of ultrasound. Nano particles were found to be distributed homogeneously with reduced agglomeration in the ultrasonicated samples. Substantial improvements in mechanical properties were observed in the composite coatings prepared in presence of ultrasound over those without ultrasound. Ni-SiC composite coatings were prepared with variable ultrasonic frequencies ranging from 24 kHz to 78 kHz and ultrasonic powers up to 300 watts. The ultrasonic frequency of 38 kHz with ultrasonic power of 200 watt was revealed to be the best ultrasonic conditions for homogeneous dispersion of nano SiC particles with improved mechanical properties in the composite coatings. The microstructures, phase compositions, and mechanical properties of the composite coatings were observed and evaluated using SEM, XRD, Vickers microhardness, and wear test. The Vickers microhardness of composite coatings under ultrasonic condition was significantly improved as compared to the coatings without ultrasound. The friction coefficient of the composite coating prepared with an ultrasonic condition was also smaller than the pure nickel coatings. A synergistic combination of superior wear resistance and improved microhardness was found in the Ni-SiC composite coatings prepared with ultrasonic conditions.

• Journal of the Korean Society for Nondestructive Testing
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• v.24 no.2
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• pp.142-150
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• 2004

A preliminary study of the behavior of ultrasonic guided wave mode in a pipe using a comb transducer for maintenance inspection of power plant facilities has been verified experimentally. The mode identification has been carried out in a pipe using the time-frequency analysis methods such as the wavelet transform(WT) and the short time Fourier transform (STFT), compared with theoretically calculated group velocity dispersion curves for longitudinal and flexural modes. The results are in good agreement with analytical predictions and show the effectiveness of using the time-frequency analysis method to identify the individual modes. It was found out that the longitudinal mode(0,1) is less affected by mode conversion compared with the other modes. Therefore, L(0,1) is selected as an optimal mode for the evaluation of the surface defect in a pipe.

• The Journal of the Acoustical Society of Korea
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• v.40 no.5
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• pp.408-416
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• 2021

In the ultrasonic dispersion, in order to avoid direct contact of the radiation surface of ultrasonic transducers with a liquid sample, the liquid sample is separated by a glass container and it receives ultrasonic energy through an acoustic medium. The transmission efficiency of the ultrasonic energy in the multi-layered ultrasonic system is an important factor. In this study, we suggested a method that can improve the ultrasonic energy transfer efficiency by using a propylene glycol solution as a liquid matching layer in the multi-layered acoustic system. In this method, a propylene glycol solution was filled between the Langevin-type ultrasonic transducer and the luminol solution and the sonoluminescence phenomena in the luminol solution, which is caused by nonlinear effect of high power ultrasound radiated from the transducer, was examined by using a Photo Multiplier Tube (PMT). The transmission efficiency depending on the concentration of propylene glycol solution was observed, and we can see that as the concentration of the propylene glycol solution increased, the matching effect increased while the acoustic attenuation increased. It was confirmed that there is an optimal concentration compromised these two conflicting conditions, and the optimum concentration of the propylene glycol solution was determined experimentally.

• Polymer(Korea)
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• v.38 no.3
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• pp.378-385
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• 2014

Multiwall carbon nanotubes (MWCNTs) were modified with a water soluble polymer, poly(vinyl alcohol), PVA, using a simple ultrasonic wave in water. Under the irradiation of ultrasound, PVA chains were severed as macroradicals and instantly grafted onto the surface of MWCNTs due to the radical scavenging effect of MWCNTs. To control the grafting PVA onto MWCNTs, the ultrasonication power and irradiation time were changed from 300 to 500 W and from 10 to 50 min, respectively. The grafted PVA onto MWCNTs was confirmed by FTIR, TGA, SEM, and TEM. Dispersion stability of the modified MWCNTs was monitored by Turbiscan. The amount of grafted PVA on MWCNTs increased with the increase in the sonication power and irradiation time. The grafted PVA on MWCNTs induced the improved dispersion stability of the modified MWCNTs in water. These findings exhibit that ultrasound can be readily used for the grafting polymer chains on MWCNTs.