• Title/Summary/Keyword: Powder packing

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The Fabrication and Characteristics of Porous Alumina Ceramics by Pressureless Powder Packing Forming Method : I . Alumina (무가압분말충전성형법에 의한 다공성 세라믹스의 제조 및 특성 : I. 알루미나)

  • 박정현;황명익;김동희;최환욱;김용남
    • Journal of the Korean Ceramic Society
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    • v.36 no.6
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    • pp.662-670
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    • 1999
  • Porous alumina was fabricated from pressureless powder packing forming method using powders granulated by spray drying. It was investigated the pore size distribution of fabricated porous alumina. The results of microstructural observation showed that intraganular pore size and intragranular pore size. At 1700$^{\circ}C$ there were no intragranular pores but it showed homogeneous distribution of intergranular pore size. The bending strength and shrinkage increased as porosity decreased. In case of thermal shock resistance sudden decrease of bending strength to $\Delta$T was not shown because intergranular large pore prevented sudden crack propagation.

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The Fabrication and Characteristics of Porous Ceramics by Pressureless Powder Packing Forming Method ; II, Mullite & Cordierite (무가압분말 충전성형법에 의한 다공성 세라믹스의 제조 및 특성 : II. 뮬라이트 & 코디어라이트)

  • 박정현;황명익;김동희;최환욱;김용남
    • Journal of the Korean Ceramic Society
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    • v.36 no.6
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    • pp.671-678
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    • 1999
  • Porous ceramics were fabricated from pressureless powder packing forming method using mullite and cordierite powders granulate by spray drying. The bending strength and shrinkage of porous ceramics were increased and their porosity were decreased with increasing temperature. It showed homogeneous distribution of 2$\mu\textrm{m}$ intergranular pores of mullite at 1400$^{\circ}C$, 2.5$\mu\textrm{m}$ intergranular pores of cordierite at 1300$^{\circ}C$ respedtively. Above that temperature intragranular particles were sintered and sintering by intergranular necking was extremely proceeded. In the test of thermal shock resistance sudden decrease of bending strength to $\Delta$T was not shown because intergranular large pore prevented sudden crack propagation.

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Variation of Magnetic Properties of (Nd, Dy)-Fe-B Sintered Magnets with Compaction Conditions ((Nd, Dy)-Fe-B 소결자석의 성형조건에 따른 자기특성 변화)

  • NamKung, S.;Lee, M.W.;Han, S.J.;Jang, T.S.
    • Journal of Powder Materials
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    • v.19 no.1
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    • pp.1-5
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    • 2012
  • In order to improve the remanence of (Nd, Dy)-Fe-B sintered magnets, we investigated the influence of compaction conditions such as packing density, applied field and green density on the magnetic properties. While the remanence decreased with increasing the packing density and green density, it increased with the increase of the applied field. In addition, XRD analysis revealed that the remanence was enhanced as the degree of powder alignment was improved. The green density was more influential on the remanence than the packing density and applied field.

Characteristics of Bi(Pb)-Sr-Ca-Cu-O Superconductor Wire Fabricated using the Billet Insertion Method (Billet 장입 방식을 이용 제조한 Bi(Pb)-Sr-Ca-Cu-O 초전도 선재의 특성)

  • 장건익;유재근;홍계원
    • Journal of the Korean Ceramic Society
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    • v.33 no.4
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    • pp.471-477
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    • 1996
  • During Bi(Pb)-Sr-Ca-Cu-O superconductor wire fabrication the effect of the initial packing density on the final characteristics of superconductor wire was systematically studied. To increase the powder packing density with uniform distribution of superconducting core a billet insertion method processed by CIP was applied instead of the commonly used vibration and ramming method of powder insertion into silver sheath. Compared with the vibration and ramming method the billent insertion technique processed by CIP cause the 30% incre-specimen with 130${\mu}{\textrm}{m}$(core thickness : 45 ${\mu}{\textrm}{m}$)and 5.24 mm width processed at 84$0^{\circ}C$for 200hrs. shows specimen with 130${\mu}{\textrm}{m}$ (core thickness ; 45${\mu}{\textrm}{m}$)and 5.24 mm width processed at 84$0^{\circ}C$ for 200 hrs. shows maximum 34A for Ic and 16, 700 A/cm2 for Ic measured at 77K and 0T. Also the sample rolled 3 times shows maximum 7, 2A for Ic and 11, 000 A/cm2 for 77K and 0T. Based on X-ray experimental results the formation of Bi-2223 and texture were significantly well developed at the interface between the superconducting core and silver sheath as compared with those of the interior area of superconducting core.

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Powder Packing Behavior and Constrained Sintering in Powder Processing of Solid Oxide Fuel Cells (SOFCs)

  • Lee, Hae-Weon;Ji, Ho-Il;Lee, Jong-Ho;Kim, Byung-Kook;Yoon, Kyung Joong;Son, Ji-Won
    • Journal of the Korean Ceramic Society
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    • v.56 no.2
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    • pp.130-145
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    • 2019
  • Widespread commercialization of solid oxide fuel cells (SOFCs) is expected to be realized in various application fields with the advent of cost-effective fabrication of cells and stacks in high volumes. Cost-reduction efforts have focused on production yield, power density, operation temperature, and continuous manufacturing. In this article, we examine several issues associated with processing for SOFCs from the standpoint of the bimodal packing model, considering the external constraints imposed by rigid substrates. Optimum compositions of composite cathode materials with high volume fractions of the second phase (particles dispersed in matrix) have been analyzed using the bimodal packing model. Constrained sintering of thin electrolyte layers is also discussed in terms of bimodal packing, with emphasis on the clustering of dispersed particles during anisotropic shrinkage. Finally, the structural transition of dispersed particle clusters during constrained sintering has been correlated with the structural stability of thin-film electrolyte layers deposited on porous solid substrates.

The Variation of Packing Density According to Powder Size Distribution and Epoxy Resin in Soft Magnetic Composite (연자성 복합체에서 파우더 크기 분포와 Epoxy Resin에 따른 Packing Density 변화)

  • Lee, Chang Hyun;Oh, Sea Moon;Shin, Hyo Soon;Yeo, Dong Hun;Kim, Jin Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.30 no.12
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    • pp.782-787
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    • 2017
  • There is growing interest in power inductors in which metal soft magnetic powder and epoxy resin are combined. In this field, the process technology for increasing the packing density of magnetic particles in an injection molding process is very important. However, little research has been reported in this regard. In order to improve the packing density, we investigated and compared the sedimentation heights of pastes for three types of soft magnetic alloy powders as a function of the mixing ratios and the type of resin used. Experimental results showed that the packing density was the highest (71.74%) when the mixing ratio was 80 : 16 : 4 (Sendust : Fe-S : CIP) according to the particle size using an SE-4125 resin. In addition, the packing density was found to be inversely related to the layer separation distance. As a result, it was confirmed that the dispersion of solid particles in the paste was important for curing; however, the duration of the curing process can greatly affect the packing density of the final composite.

Preparation of SiC-Al alloy Composite by Pressureless Powder Packing Forming Method (분말 충전 성형법을 이용한 SiC-Al Alloy 복합체의 제조)

  • 박정현;송준광;백승수;염강섭;강민수
    • Journal of the Korean Ceramic Society
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    • v.34 no.4
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    • pp.343-350
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    • 1997
  • To fabricate the ceramic/metal(SiC/ Al alloy) composite, SiC preform was prepared by Pressureless Powder Packing Forming Method and 6061 Al alloy was infiltrated into the preform. Uniform compact having an average pore size of 10 ${\mu}{\textrm}{m}$ and narrow pore size distribution was prepared. Phenolic resin solution(40 wt%) was penetrated into the SiC compact, and then the compact was preheated at the temperature of 120$0^{\circ}C$. The pore size distribution and the microstructure of the preform were not changed by preheating. An uniform microstructure without any crack in the preform was obtained in SiC-Al alloy composite. The infiltration of 6061. Al alloy into the preform began at the temperature of 130$0^{\circ}C$ and the amount of infiltration increased in proportion to the infiltration temperature and the soaking time. The increasement rate of the infiltration amount decreased after 3 h. As a result of the infiltration at 140$0^{\circ}C$ for 4 h, Al alloy was well distributed in the interparticle channels and the relative density of the composite was above 98%. The strength and the fracture toughness of the composite were 303 MPa and 21.65 MPam1/2, respectively.

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Effect of Powder Size on the Rheological Characteristics of Sm-Co Type Compound for Powder Injection Molding (사출성형용 컴파운드의 유연학적 특성에 미치는 SH-CO 계 분말의 입도 영향)

  • 정우상;김윤배;정원용
    • Journal of the Korean Magnetics Society
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    • v.11 no.4
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    • pp.157-162
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    • 2001
  • Rheological characteristics of Sm-Co type plastic magnet compound for powder injection molding process were investigated with the variation of the magnetic powder size, their relative contents and volume fraction using the mixture of fine and coarse powder. Shear viscosity of Sm-Co type compound was decreased with increasing the size of coarse powder due to the increase of powder packing density. However, the smaller the average size of fine powder resulted in the higher viscosity of compound due to the increase of agglomeration force. In case of mechanically milled Sm-Co type powder, the viscosity of compound with the mixture of coarse powder of 125∼75 ㎛ and fine powder of average size of 4.9 ㎛ greatly depends on their relative contents and shows a minimum value at the 60 % coarse powder fraction. This means that the compound shows a maximum packing density at the 60% coarse powder fraction. Compound viscosities satisfied well the rheological model with the volume fraction of magnetic powder, and maximum volume fraction of magnetic powder in Sm-Co type compound for powder injection molding was about 66%.

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Numerical Simulation of Cold Compaction of 3D Granular Packings

  • Chen, Yuan;Imbault, Didier;Doremus, Pierre
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.189-190
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    • 2006
  • During cold compaction processes loose powder is pressed under tooling action in order to produce complex shaped engineering components. Here, the analysis of the plastic deformation of granular packings is of fundamental importance to the development of computer simulation models. Powders can be idealized by packing discrete particles, where each particle is a sphere meshed with finite elements. The pressing of a body centered cubic packing was compared with numerical prediction and experimental data. The global response was expressed in force-displacement curve, and the accuracy of the numerical models analyzed for high relative densities up to 0.95.

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