• Title/Summary/Keyword: Powder characteristic

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Utilizability of Waste Concrete Powder as a Material for Soil Pavement (흙도로포장용 재료로서 폐콘크리트 미분말의 활용성 연구)

  • Kim, Yong-Jic;Choi, Yun-Wang;Kim, Young-Jin
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.3 no.3
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    • pp.277-282
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    • 2015
  • This study is conducted to utilize waste concrete powder (WCP) made as a by-product manufacturing high quality recycled aggregate. The blaine fineness of the used waste concrete powder was $928cm^2/g$. As the main characteristic of waste concrete powder, it showed an angular type similar to cement, but hydrated products were attached on the surface of particles. In addition, the size of the particles of waste concrete powder was larger than OPC and in terms of chemical components it had higher $SiO_2$ contents. For using WCP in soil cement-based pavement, the qualities, physical and chemical properties, of WCP should be researched. In the first step, the specified compressive strength of mortar for two types of clay sand soil and clay soil respectively was experimented to be 15 MPa and then optimum mixing ratio of chemical solidification agent were decided in the range of 1.5 - 3.0% in the replacement with cement weight content. In the second step, based on the prior experimental results, recycling possibility of WCP in soil cement-based pavement was studied. In the result of experiment the mixing ratio of WCP were 5, 10, 15 and 20% in the replacement with soil weight and the compressive strength of mortar was somewhat decreased according to the increase of the mixing ratio of WCP.

The Variation Rate of Shear Modulus for Anisotropic Magneto-rheological Elastomer due to Volume Fraction of CIP (CIP 부피비에 따른 이방성 MRE의 전단계수 변화율)

  • Jeong, Un-Chang;Yoon, Ji-Hyun;Yang, In-Hyung;Lee, You-Yub;Oh, Jae-Eung
    • Transactions of the Korean Society for Noise and Vibration Engineering
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    • v.21 no.12
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    • pp.1132-1137
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    • 2011
  • MRE(magneto-rheological elastomers) is a material which shows reversible and various modulus in magnetic field. Comparing to conventional rubber vibration isolator, MREs are able to absorb vibration of broader frequency range. These characteristic phenomena result from the orientation of magnetic particles named carbonyl iron powder(CIP) in rubber matrix. In this paper, simulation on variation rate of shear modulus for anisotropic MRE due to volume fraction of CIP and an effective permeability model was applied to predict the field-induced shear modulus of MREs. Also, the variation rate of shear modulus for anisotropic MRE was derived using magneto-mechanical theory. Based on Maxwell-Garnett mixing rule, the increment of shear modulus was calculated to evaluate the shear modulus of MREs with column structure of CIP due to induced current. The simulation results on variation rate of shear modulus can be applied to the variable mechanical system of MRE such as tunable vibration absorber, stiffness variable bush and mount.

A Study on the Effects of Contaminant Types on the Wear Degradation Characteristics in Internal Gear Pumps (불순물 입자의 유형에 따른 내접기어 펌프에서의 마모열화 특성 연구)

  • Shin, Jung-Hun;Ji, Kyung-Ryeol;Kim, Hyoung-Eui
    • Tribology and Lubricants
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    • v.27 no.3
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    • pp.134-139
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    • 2011
  • The mechanical equipments which are exposed to impure environment undergo significant reductions in their own lifetimes. Several environmental test procedures have been developed to analyze these phenomena. Moreover in the industry to require shorter development duration, accelerated life testers artificially add test containments into machines. In this research JIS Z 8901 test powder was added into internal gear pumps which are used as oil pumps in vehicles and thus the effects of the addition on the degradation of the pumps were examined. Three kinds of contaminants were selected. Two of the contaminants are identical in particle size but different in the composition of the ingredients. The other pair have identical ingredients and composition but different particle size. The quantity of contaminants was also an interesting factor in this study. The results show that each JIS contaminant caused notable degradation in the discharge flow characteristic of pumps while friction torque degradation did not have any tendency. Finally leakage rates were deduced and equivalent wear volume ratios were calculated.

Photoluminescence Property of Lu2Si2O7:Ce3+ Powder for Scintillator

  • Kim, Kyung-Nam;Cao, Guozhong
    • Korean Journal of Materials Research
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    • v.26 no.4
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    • pp.212-215
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    • 2016
  • In this paper, cerium doped lutetium pyrosilicate (LPS) powders with cerium content (0.05 and 0.07 mol%) were prepared by sol-gel process. The formation of lutetium pyrosilicate (LPS) phase was confirmed by XRD analysis for the powders heated at $1,200^{\circ}C$; in these powders, a single phase of $Lu_2Si_2O_7$ (LPS) was observed. Cerium doped lutetium pyrosilicate (LPS) powder was agglomerated and constituted of small spherical particles with diameters of about 300 nm. The photoluminescence spectra of the $Lu_2Si_2O_7:Ce^{3+}$ powders showed the characteristic of excitation and there was an emission spectrum for $Ce^{3+}$ in the host of $Lu_2Si_2O_7$. The emission spectrum shows a broad band in the range of 350-525 nm; the broad wavelength on the right side of the spectra should be ascribed to the same 5d-4f transitions of $Ce^{3+}$, as in the case of cerium doped $Lu_2Si_2O_7$ single crystals.

Sputtering Deposition of $CuInSe_{2}$ and $CuInZnSe_{2}$ Thin Films using Mixture Binary Chalcogenide Powders

  • Wibowo, Rachmat Adhi;Guk, Jun-Pyo;Kim, Gyu-Ho
    • 한국신재생에너지학회:학술대회논문집
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    • 2007.06a
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    • pp.257-260
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    • 2007
  • In this study, $CuInSe_{2}$ (CISe) and $CuInZnSe_{2}$ (CIZSe) thin films were prepared on Corning 1737 glass by radio frequency (RF) magnetron sputtering from binary chalcogenide mixed powder targets. The targets were initially prepared by mixing appropriate weights of CuSe, InSe powder and various ZnSe contents. From the film bulk analysis result, it is observed that Zn concentration in the films increases proportionally with the addition of ZnSe in the sputtering targets. Under optimized conditions, CISe and CIZSe thin films grow as a chalcopyrite structure with strong (112), (220/204) and (312/116) reflections. Films are found to exhibit a high absorption coefficient of $10^{4}$ $cm^{-1}$. An increasing of optical band gap from 1.0 eV (CISe) to 1.25 eV (CIZSe) is found to be proportional with an increasing of Zn concentration as expected. All films have a p-type semiconductor characteristic with a carrier concentration in the order of 1014 $cm^{-3}$, a mobility about $10^{1}$ $cm^{2{\cdot}-1}{\cdot}s^{-1}$ and a resistivity at the range of $10^{2}-10^{6}$ W${\cdot}$m.

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Thermal Characteristic Simulation and Property Evaluation of High Melting Point Materials by Pulsed Current Activated Sintering Process (PCAS공정에 의한 고융점 소결체 열전달 해석 및 특성분석)

  • Nam, Hyo-Eun;Jang, Jun-Ho;Park, Hyun-Kuk;Oh, Ik-Hyun
    • Journal of Sensor Science and Technology
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    • v.26 no.3
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    • pp.214-222
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    • 2017
  • In this study, the effects of internal heat treatment associated sintering temperatures were simulated by the Finite Element Method (FEM). The sintering mechanism of pulsed current activated sintering process (PCAS) is still unclear because of some unexplainable heat transfer phenomena in coupled multi-physical fields, as well as the difficulty in measuring the interior temperatures of metal powder. We have carried out simulation study to find out thermal distributions between graphite mold and Ruthenium powder prior to PCAS process. For PCAS process, heating rate was maintained at $100^{\circ}C/min$ the simulation indicates that the sintering temperature range was between $1000^{\circ}C$ to $1300^{\circ}C$ under 60 MPa. The heat transfer inside the Ruthenium sintered-body sample was modelled through the whole process in order to predict the minimum interior temperature. Thermal simulation shows that the interior temperature gradient decreased by graphite punch length and calculation results well agreed with the PCAS field test results.

Shape Control of Platinum Nanoparticles Using a Metal Salt (금속 염을 이용한 백금 나노입자의 형상제어)

  • Kwak, Seoung Yeul;Lee, Jin Ho;Kim, Jin Woo;Jung, Taek Kyun;Kim, Young Do
    • Journal of Powder Materials
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    • v.19 no.6
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    • pp.393-397
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    • 2012
  • $AgNO_3$ has the characteristic is controlling the inhibition or promotion of particle growth by adsorbing onto specific facets of platinum nanoparticles. Therefore, in this study, $AgNO_3$ was added to control the shape of platinum nanoparticles during the liquid phase reduction process. Consequently, platinum cubes were synthesized when $AgNO_3$ of 1.1 mol% (with respect to the Pt concentration) was added into the solution. Platinum octahedrons were synthesized when 32 mol% (with respect to the Pt concentration) was added into the solution. These results demonstrate that the metal salt $AgNO_3$, effectively controlled the relative growth rates of each facet of Pt nano particles.

Fabrication and Characteristic Evaluation of Hybrid Carbon Nanotubes Reinforced SKD11 Cold Work Tool Steel (탄소나노튜브 강화 SKD11 냉간금형용 하이브리드 탄소나노소결체 제조 및 특성 평가)

  • Jung, Sung-Sil;Moon, Je-Se;Lee, Dae-Yeol;Youn, Kuk-Tae;Park, Chun-Dal;Song, Jae-Sun
    • Journal of Powder Materials
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    • v.20 no.4
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    • pp.291-296
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    • 2013
  • SKD11 (ASTM D2) tool steel is a versatile high-carbon, high-chromium, air-hardening tool steel that is characterized by a relatively high attainable hardness and numerous, large, chromium rich alloy carbide in the microstructure. SKD11 tool steel provides an effective combination of wear resistance and toughness, tool performance, price, and a wide variety of product forms. The CNTs was good additives to improve the mechanical properties of metal. In this study, 1, 3 vol% CNTs was dispersed in SKD11 matrix by mechanical alloying. The SKD11+ CNT hybrid nanocomposites were investigated by FE-SEM, particle size distribution, hardness and wear resistance. The CNT was well dispersed in the SKD11 matrix and the mechanical properties of the composite were improved by CNTs addition. It shows good feasibility as cold work die tool.

Effects of Excess PbO and Ball-Milling on the Microstructure, Sintering Behavior and Mechanical Properties of PZT Ceramics (과잉 PbO 첨가 및 미분쇄에 의한 PZT 압전세라믹스의 미세구조제어와 소결특성 및 기계적 성질)

  • 전봉관;남효덕;김상태
    • Journal of the Korean Ceramic Society
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    • v.32 no.6
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    • pp.726-734
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    • 1995
  • Pb(Zr0.53Ti0.47)O3 (PZT) ceramics having different microstructures were fabricated at low temperatures using calcined PZT powders with addition of excess PbO powder and/or ball milling. The effects of excess PbO and ball milling time on the microstructure, the sintering characteristic, and the mechanical properties of these ceramics were studied. Fine powders with average particle size of 0.38㎛ could be obtained by ball milling with 2.5 mm Ф zirconia balls for 120 hours. By the addition of 2mol% of excess PbO to these powders, it was possible to obtain well-densitified PZT ceramics at low sintering temperature of 980℃. Densification behavior of PZT was affected by the addition of excess PbO powder, while, grain growth was hardly affected by PbO addition. It was observed that Vicker's hardness decreased and fracture toughness increased with the increasing amount of PbO. At 1mol% excess PbO, it was shown that the minimum values of hardness and maximum fracture toughness were achieved. In addition, with increasing sintering time, the fracture toughness decreased and the hardness increased.

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Charge-discharge Characteristic of the Mg-Ni Hydrogen Storage Alloy System (MgNi계 수소흡장합금의 충방전특성)

  • Oh, Myung-Hark;Chung, Won-Sub;Kim, In-Gon
    • Transactions of the Korean hydrogen and new energy society
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    • v.10 no.3
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    • pp.177-184
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    • 1999
  • The charge-discharge characteristics of the $Mg_2Ni-x$ wt.%Nd (x = 0~3) electrodes were investigated. The electrodes were prepared by the mechanical grinding of the induction-melted $Mg_2Ni$ alloy powders with Ni and/or Nd using planetary ball mill apparatus. The discharge capacity of the $Mg_2Ni$ alloy increased with the increase in the nickel content. The electrode possessing 100 wt.% nickel powder showed the initial capacity of 760 mAh/g and the capacity decay with the cycle number was less than that of the 55 wt.% nickel powder. The Nd was added to this composition. It was found that the $Mg_2Ni-100$ wt.%Ni -0.2 wt.%Nd alloy showed an excellent charge-discharge cycle characteristics compared with the other reported Mg-Ni alloy system. The discharge capacity was 400 mAh/g after 70 cycles. Such an improved cycle life seems to be attributed to the improvement in the corrosion characteristics of the alloy. The anodic polarization curve of the $Mg_2Ni-100$ wt.%Ni-0.2 wt.%Nd alloy exhibited better passivating behavior than that of the $Mg_2Ni-100$ wt.%Ni.

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