• Clean Technology
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• v.18 no.2
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• pp.155-161
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• 2012

The purpose of this study is to remove paraffin wax binder effectively from powder injection molded part using supercritical fluids in powder injection molding process. For a thin powder injection molded part about 1-2 mm thickness, paraffin wax binder can be removed rapidly without any defect by traditional supercritical extraction process which has fixed high temperature and pressure condition. But, for a thick powder injection molded part, there are limitations in removing paraffin wax binder by the fixed high process condition because crack occurs at the beginning step. Therefore, here we studied variable condition debinding process that starts with mild process condition at the beginning step and then increase the process conditions simultaneously at each step. To find out the initial process condition that has the highest extraction yield without any defect for each sample thickness, we investigated various supercritical debinding conditions using 1-4 mm thickness ceramic injection molded sample. By using the variable condition debinding process that starts with the initial process condition at the first step and then increasing process conditions simultaneously at each step (temperature from 333.15 to 343.15 K, pressure from 12 to 27 MPa, and $CO_2$ flow rate from 1.5 to 10 L/min), over 95% of paraffin wax binder was removed from the 4 mm thick (10 mm diameter) ceramic injection molded disk samples within 5 hours.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2012.05a
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• pp.523-524
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• 2012

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2012.05a
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• pp.99-100
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• 2012

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2013.05a
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• pp.1117-1118
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• 2013

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.964-965
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• 2006

The injection molded Fe sintered bodies were fabricated using two kinds of nano Fe powders, $Fe-5%vol.ZrO_2$ and $Fe-10vol.%ZrO_2$ powders. The relationship between microstructure and mechanical properties depending on the $ZrO_2$ contents and sintering temperature were characterized by SEM and TEM techniques. In the wear test, the $Fe-0vol%ZrO_2$ sintered bodies showed mainly adhesive wear, but in the Fe-5%vol. $ZrO_2$ and Fe-10vol. % $ZrO_2$ composites the main wear behavior showed abrasive wear mode.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.5
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• pp.2587-2593
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• 2014

Ceramic Injection Molding (CIM) is one of wide used processes in industry field and the applications are gradually being expanded to parts of medical and electric devices. In this study, the CIM process were analyzed with FEM and process parameters were studied and analyzed the effect on product quality. The shape of simple flat plate was compared to the shapes with the hole, with the round corner portion or with the side wall portion. If there are holes then the hole around the uneven density distribution and the defects such as weld lines could be occurred. The Large radius of the corners of the product give good formability and fluidity. Not only the shape parameters of product but also the process parameters during CIM are studied. The simulation results showed that the process parameters of temperature, initial fractions and velocity are important design parameters to improve the quality of products.

• Journal of Powder Materials
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• v.8 no.2
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• pp.91-97
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• 2001

The conventional debinding process in metal injection molding is very long time-consuming and unfriendly environmental method. Especially, in such a case of injection molded parts from hard and fine metal powder, such as WC-Co, an extremely long period of time is necessary in the conventional slow binder removal process. On the other hand, supercritical debinding is thought to be the effective method which is appropriate to eliminate the aforementioned inconvenience in the prior art. The supercritical fluid has high diffusivity and density, it can penetrate quickly into the inside of the green metal bodies, and extract the binder. In this paper, super-critical debinding is compared with wicking debinding process. Wax-based binder system is used in this study. The binder removal rate in supercritical $CO_2$ have been measured at $65^{\circ}C$, 75$^{\circ}C$ in the pressure range from 20 MPa to 28 MPa. Pores and cracks in silver bodies after sintering were observed using SEM When the super-critical $CO_2$ debinding was carried out at 75$^{\circ}C$, almost all the wax (about 70 wt% of binder) was removed in 2 hours under 28 MPa and 2.5 hours under 25 MPa.

• The Korean Journal of Rheology
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• v.11 no.1
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• pp.57-65
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• 1999

In order to measure yield stress of PIM feedstocks simply and effectively, a yield stress measuring technique was developed by a vane method. The vane method had an advantage that there was no wall-slip, while it had a drawback that it could not measure viscosity change at various shear rates. A Newtonian fluid was tested for the appropriateness of the measuring technique. The end effect of a vane was checked to produce an acceptable error. The torque peak has been considered to be developed at yielding of non-Newtonian fluids with yield stress. However, it was influenced very much by control system of the instrument so that the torque value at the stable region was taken to calculate yield stress. Torque at zero rotational speed was obtained by extrapolating the torque values at various speeds to remove the effect of the rotational drag. As general verification, yield stress of feedstocks made of Tungsten carbide powder with wax-based binder was measured at different temperatures and various powder concentrations.

• Journal of the Korean institute of surface engineering
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• v.51 no.2
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• pp.104-109
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• 2018

Fe-2 wt.%Ni alloys were fabricated by metal powder injection molding, and their oxidation behavior at $600-700^{\circ}C$ for 30 h in air was studied in order to find the effect of the small addition of Ni in the iron matrix on the high-temperature oxidation. Oxide scales that formed after oxidation consisted primarily of $Fe_2O_3$, where microscopic voids were scattered. Nickel was segregated initially at the scale/matrix interface, and later at the lower part of the $Fe_2O_3$ scale. At $600^{\circ}C$, Fe-2wt.%Ni alloys oxidized parabolically initially, and linearly after 15 h. At $650-700^{\circ}C$, they oxidized linearly from the initial period. Although Fe-2wt.%Ni alloys oxidized slower than pure iron, their oxidation rates were relatively fast.

• Design & Manufacturing
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• v.11 no.3
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• pp.29-34
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• 2017

Increased demand for parts with micro-pattern structure made of metals, ceramics, and composites in various fields such as medical ultrasonic sensors, CT collimators, and ultra-small actuator parts. Micro powder injection molding (PIM) is a technology for manufacturing micro size, high volume, complex, precision, net-shape components from either metal or ceramic powder. In the present study, a standard mold with a variable insert core capable of producing various micro patterns was investigated. An injection molding test was performed on a standard mold using a line type micro-pattern core having an aspect ratio of 2, a slenderness ratio of 70, a pattern size of $200{\mu}m$, and a pattern spacing of $150{\mu}m$. During the filling process, the deformation of the mold with large aspect ratio and slenderness ratio was analyzed by the experiment and the numerical simulation according to the position of the gate. We proposed a mold structure that minimizes mold deformation by gate modification and enables uniform pattern filling behavior.