• Title/Summary/Keyword: Post curing

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Effects of Post Cure Conditions on Thermal Characteristics of A1$_2$O$_3$ Filled Epoxy Resin Composite System (A1$_2$O$_3$ 충전된 에폭시 수지 복합재료계의 후기 경화조건에 따른 열적특성)

  • Cho, Young-Shin;Shim, Mi-Ja;Kim, Sang-Wook
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.227-230
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    • 1998
  • The effects of post curing conditions on thermal properties of alumina filled epoxy resin system DGEBA/MDA/SN were investigated. As the post curing time increased at 15$0^{\circ}C$, the glass transition temperature increased from 121 to 124, slightly. As the heating rate increased, high thermal decomposing temperature (T$_{d}$) and most decomposing temperature (T$_{p}$) increased. For the case of post-cured system at 15$0^{\circ}C$ for 4 days showed lower values than virgin system. At the post curing condition the system must have been thermally degraded.ded.

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Correlation between UV-dose and Shrinkage amounts of Post-curing Process for Precise Fabrication of Dental Model using DLP 3D Printer (DLP 공정을 이용한 정밀 치아모델 제작에서 UV 조사량과 후경화 수축률의 상관관계 분석)

  • Shin, Dong-Hun;Park, Young-Min;Park, Sang-Hu
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.17 no.2
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    • pp.47-53
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    • 2018
  • Nowadays, additive manufacturing (AM) technology is a promising process to fabricate complex shaped devices applied in medical and dental services. Among the AM processes, a DLP (digital light processing) type 3D printing process has some advantages, such as high precision, relatively low cost, etc. In this work, we propose a simple method to fabricate precise dental models using a DLP 3D printer. After 3D printing, a part is commonly post-cured using secondary UV-curing equipment for complete polymerization. However, some shrinkage occurs during the post-curing process, so we adaptively control the UV-exposure time on each layer for over- or under-curing to change the local shape-size of a part in the DLP process. From the results, the shrinkage amounts in the post-curing process vary due to the UV-dose in 3D printing. We believe that the proposed method can be utilized to fabricate dental models precisely, even with a change of the 3D CAD model.

Influence of tooth position within the field of view on the intensity of cone-beam computed tomographic imaging artifacts when assessing teeth restored with various intracanal materials

  • de Oliveira Pinto, Martina Gerlane;Melo, Saulo Leonardo Sousa;Cavalcanti, Yuri Wanderley;de Lima, Elisa Diniz;Bento, Patricia Meira;de Melo, Daniela Pita
    • Imaging Science in Dentistry
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    • v.50 no.2
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    • pp.141-151
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    • 2020
  • Purpose: This study aimed to quantify the influence of tooth position within the field-of-view (FOV) on cone-beam computed tomography (CBCT) imaging artifacts' intensity when assessing teeth restored with various intracanal materials. Materials and Methods: Seventy single-rooted teeth were divided into 7 groups (10 teeth per group): NiCr post (NC), AgPd post (AP), metal core fiberglass post (MCFG), fiberglass post (FG), anatomical fiberglass post (AFG), fiberglass post cemented with core build-up cement (FGCo), and anatomical fiberglass post cemented with core build-up cement (AFGCo). All posts were cemented using a regular dual-curing resin cement (Allcem), except FGCo and AFGCo which were cemented with a core build-up dual-curing resin cement (AllcemCore). Each tooth was scanned on a CS9000 in 5 positions within the FOV: a central position, anterior horizontal peripheral, peripheral superior, peripheral inferior, and posterior horizontal peripheral position. Hyperdense, hypodense, remaining teeth areas and ROI areas were quantitatively analyzed using ImageJ software. Results: Posterior horizontal peripheral position increased the intensity of artifacts on FGCo and AFGCo post groups (P<0.05), and specifically the hypodense artifact intensity on FG and AFG post groups (P<0.05). NC and AP groups presented greater intensity of artifacts than any other post groups(P<0.05). Conclusion: Artifact intensity increases in the presence of high atomic number materials and when the object is not centered within the FOV. The impact of positioning within the FOV on artifact was greater for fiberglass posts cemented with core build-up dual-curing cement than for metal posts and fiberglass posts cemented with regular dual-curing cement.

The Study of Curing Day Reduction by Step Curing of HTPB/AP Propellant (HTPB/AP계열의 고체 추진제의 Step 경화 방법을 통한 경화일(기간) 단축)

  • Kim, Kahee;Park, Jung-Ho;Choi, Sunghan
    • Journal of the Korean Society of Propulsion Engineers
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    • v.24 no.6
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    • pp.101-107
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    • 2020
  • In this paper, step-curing, which includes the change of curing temperature on the curing process, was applied to reduce curing day of HTPB/AP based propellant. This study targets the improvement of productivity of HTPB/AP based solid rocket motor. Comparison of mechanical properties of propellant resulted in the change of normal curing condition (60℃, 5 days) to step-curing condition (60℃, 1 day / 65℃, 3 days). Post-cure test was conducted to determine the impact on the shelf life of the solid rocket motor. The aging characteristics of propellants were analyzed by measuring mechanical properties and thermal expansion factor. To step-cured propellant, accelerated aging test was performed for 12 weeks, followed by tensile test. Sm(bar) and Em(%) were higher than 8 bar and 40% each, showing excellent mechanical properties.

Effects of Post-curing on Thermal Stability of Epoxy-sioxane IPN Structure (Epoxy-siloxane IPN의 열적 안정성에 미치는 후기경화의 영향)

  • Cho, Young-Shin;Shim, Mi-Ja;Kim, Sang-Wook
    • Proceedings of the KIEE Conference
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    • 1999.11d
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    • pp.944-946
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    • 1999
  • The thermal stability of the post cured epoxy-polysiloxane IPN structure was observed by using DSC and TGA. As the post curing time increased the glass transition temperature increased and the secondary exothermic peak disappeared. The thermally decomposing activation energy calculated by using Kissinger expression was 225.6 kJ/mol. The thermal stability of the grafted IPN of epoxy and silicon compound depends on the composing ratio and post curing conditions of time and temperature.

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Effects of Curing Agent Content and Post-curing Conditions on Dielectric Deterioration Characteristics of DGEBA/MDA/SN System (경화제 함량과 후기경화조건에 따른 DGEBA/MDA/SN계의 절연열화 특성)

  • 조영신;박수길;임기조;심미자;김상욱
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1997.11a
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    • pp.313-316
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    • 1997
  • The effects of aromatic curing agent of MDA contents and post curing conditions on dielectric deterioration characteristics of DGEBA/MDA/SN system were investigated. The dielectric properties were measured by using needle-plane electrode geometry under the commercial AC high electric field application. As the curing agent content increased, the dielectric breakdown strength increased and then decreased slightly. All the trees initiated from the tip of needle electrode and the shape of the tree in this system was a dendrite type.

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CURING REACTION OF THE LIGHT CURED FLOWABLE COMPOSITE RESINS THROUGH THE ENDODONTIC TRANSLUCENT FIBER POST (투명 fiber 포스트를 통한 광중합형 접착레진의 중합 반응)

  • Ahn Seok;Park Sang-Won;Yang Hong-So;Vang Mong-Sook;Park Ha-Ok
    • The Journal of Korean Academy of Prosthodontics
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    • v.44 no.1
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    • pp.1-9
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    • 2006
  • Purpose: The purpose of this study was to evaluate the efficacy and substitute possibility of a newly developed flowable composite resins as a luting cement for translucent fiber post. Material & Method: Two kinds of 12 mm translucent fiber Post (D.T. Light-Post (Bisco, USA) and FRC Postec (Ivoclar vivadent, Liechtenstein) was inserted into the teflon mold (7 mm diameter, 9 mm long) and Filtek-Flow (3M ESPE. USA), a light activated flowable composite resin, was polymerized for 60 seconds through the post. Also, the post was cut from the tip to 9 mm, 6 mm, 3 mm, and Filtek-Flow was light cured according to each length. For comparison, 60 seconds light-cured and 24 hours self-cured two dual cured resin cement (Duo-cement (Bisco, USA) and 2 Panavia-F (Kuraray, Japan)) samples were prepared as control group. Also cavities (1 mm in width, 1 mm in depth and 12 mm in length) were prepared using acrylic plate and aluminum bar, and flowable composite resin was flied and light cured by the diffused light from the fiber post's side wall. The degree of polymerization was measured according to the distance from curing light using Vickers' hardness test. Result: Within the limitation of this study, the following conclusions were drawn: 1. Vickers' hardness of light cured dual cured resin cement and flowable composite resin decreased from Panavia-F, Filtek-Flow and Duo-cement accordingly (p<0.05). In the dual curing resin cement, light curing performed group showed higher surface hardness value than self cured only group (p<0.05). 2. Surface hardness ratio (light cured through fiber post /directly light cured) of D.T. Light-Post using Filtek-Flow showed about 70% in the 6 mm deep and about 50% in the 12 mm deep FRC Postec showed only 40% of surface hardness ratio. 3. Surface hardness ratio by diffused light from the post's side wall showed about 50% at 6 mm and 9 mm deep, and about 40% at 12 mm deep in D.T. Light-Post. However, FRC Postec showed about 40% at 6 mm deep, and almost no polymerization in 9 mm and 12 mm deep.

A Study on the Effect of Accelerated Curing on 28-Days Compressive Strength of Concrete (촉진양생이 콘크리트의 28일 압축강도에 미치는 영향에 관한 연구)

  • 최세규;유승룡;김생빈
    • Magazine of the Korea Concrete Institute
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    • v.8 no.4
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    • pp.141-148
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    • 1996
  • The pulished works on Accelerated Curing Effect were generally performed around from 1960 to 1970th century for 18 to 24 hours - total curing periods. It is not possible to define the effect of temperature rise because those results were obtaine mainly by using the manually operated steam-curing tank. Thus, it may not be available to apply those data immediately on the domestic PC wall production line. The testing specimens were made from the standard mix proportion according to those of domestic PC factories to establish a basic data for the Accelerated Curing Effect. The experimental tests were conducted according to the conditions of each sub-curing periods. By comparing the results of compression tests on de-molded and 28-day water-curing specimens, we find that the most effective curing condition to obtain more than the required design strength after 28 day of water curing may be as follows: the presteaming period does not affect seriously and less than$30^{circ}C/hr$- the rate of temperature rise andless than $82^{circ}C$ - maximum temperature are necessary. It seems that post-curing procedure is very important factor to increase the effect of accelerated curing.

Evaluation of Material Properties of Fire-damaged Concrete Under Post-fire Curing Regimes Using Impact Resonance Vibration Method (충격 공진 기법을 이용한 화재 손상 콘크리트의 재양생 조건별 재료물성 평가)

  • Park, Sun-Jong;Yim, Hong Jae
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.5
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    • pp.42-48
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    • 2017
  • When concrete structures expose to fire, the structures were damaged accompanied with degradation of material properties of concrete. In order to determine the reuse of fire-damaged concrete structures, it is needed a careful determination considering conditions of fire damage, such as exposure temperature and exposure time, and also potential to restore fire damage. This study investigates on the evaluation of residual material properties of fire-damaged concrete under different post-fire curing regimes. An experimental study was performed on concrete samples to measure the dynamic elastic modulus by the impact resonance vibration method. Upon the experimental results, the evidence of restoration of material properties was confirmed on specific post-fire curing regimes, higher humidity conditions. Additionally, a correlation analysis was performed on the dynamic elastic modulus with the tensile strength for identifying the effects of post-fire curing regimes on both material properties of fire-damaged concrete.

A Study on the effect of Accelerated Curing on Hydration and Compressive Strength of Concrete (촉진양생이 콘크리트의 수화 및 압축강도에 미치는 영향에 관한 연구)

  • 김생빈;유승룡;김동신;최세규
    • Proceedings of the Korea Concrete Institute Conference
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    • 1996.04a
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    • pp.107-111
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    • 1996
  • The testing specimens were made from the standard mix proportion according to those of domestic PC factories to establish a basic data for the Accelerated Curing Effect. The experimental tests were conducted according to the conditions of each sub-curing periods. By comparing the results of compression tests on de-molded and 28-day water-curing specimens, we find that the most effective curing condition to obtain more than the required design strength after 28 days of water curing may be as follwings; the presteaming period does not affect seriously and less than $30^{\circ}C$/hr-the rate of temperature rise and less than $82^{\circ}C$ - maximum temperature are necessary. It seems that post-curing procedure is very important factor to increase the effect of accelerated curing.

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