• Title/Summary/Keyword: Porosities

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Effect of Porosity on the High-Cycle Fatigue Behavior of Al-Si-Mg Casting Alloy (Al-Si-Mg계 주조용 알루미늄 합금의 고주기 피로 거동에 미치는 기공의 영향)

  • Lee, Young-Jae;Kang, Won-Guk;Euh, Kwang-Jun;Cho, Kyu-Sang;Lee, Kee-Ahn
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.350-352
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    • 2009
  • The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore fur its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

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Recent Trends of Friction Stir Welding of Titanium (타이타늄 소재 마찰교반용접 기술 동향)

  • Chun, Chang-Keun;Kim, Sung-Wook;Kim, Heung-Joo;Chang, Woong-Seong;Noh, Joong-Suk
    • Journal of Welding and Joining
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    • v.31 no.2
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    • pp.16-20
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    • 2013
  • Titanium and its alloys have been widely using in the various field of industry application due to high corrosion resistant properties and mechanical properties. Titanium is highly reactive in the high temperature state and the formation of titanium oxide and porosities in the nuggets of fusion welding will results in the degradation of the mechanical properties. For this reason the studies of friction stir welding for titanium have been investigated recently. The FSW zones of titanium were classified by the weld nugget (WN), the linear transition boundary (TB) and the heat affected zone (HAZ). The WN along with titanium parent was characterized by the presence of twins and dislocations. The average grain size and hardness of WN has been changed according to heat input. The grain refinement resulted from the FSW increased the hardness in the stir zone. Sound dissimilar joints between SUS 304 and CP-Ti were achieved using an advancing speed of 50 mm/min and rotation speeds in the range of 700-1100 rpm. Aluminum 1060 and titanium alloy Ti-6Al-4V plates were lap joined by friction stir welding, hence the ultimate tensile shear strength of joint reached 100% of Al 1060. Mg alloy and Ti were successfully butt joined by inserting a probe into the Mg alloy plate with slightly offsetting. But Ti-Al intermetallic compound layers formed at the interface of these joints.

Microstructural and Wear Properties of WC-based and Cr3C2-based Cermet Coating Materials Manufactured with High Velocity Oxygen Fuel Process (고속 화염 용사 공정으로 제조된 WC계 및 Cr3C2계 Cermet 코팅 소재의 미세조직 및 마모 특성)

  • Kang, Yeon-Ji;Ham, Gi-Su;Kim, Hyung-Jun;Yoon, Sang-Hoon;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.25 no.5
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    • pp.408-414
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    • 2018
  • This study investigates the microstructure and wear properties of cermet (ceramic + metal) coating materials manufactured using high velocity oxygen fuel (HVOF) process. Three types of HVOF coating layers are formed by depositing WC-12Co, WC-20Cr-7Ni, and Cr3C2-20NiCr (wt.%) powders on S45C steel substrate. The porosities of the coating layers are $1{\pm}0.5%$ for all three specimens. Microstructural analysis confirms the formation of second carbide phases of $W_2C$, $Co_6W_6C$, and $Cr_7C_3$ owing to decarburizing of WC phases on WC-based coating layers. In the case of WC-12Co coating, which has a high ratio of $W_2C$ phase with high brittleness, the interface property between the carbide and the metal binder slightly decreases. In the $Cr_3C_2-20CrNi$ coating layer, decarburizing almost does not occur, but fine cavities exist between the splats. The wear loss occurs in the descending order of $Cr_3C_2-20NiCr$, WC-12Co, and WC-20Cr-7Ni, where WC-20Cr-7Ni achieves the highest wear resistance property. It can be inferred that the ratio of the carbide and the binding properties between carbide-binder and binder-binder in a cermet coating material manufactured with HVOF as the primary factors determine the wear properties of the cermet coating material.

THE EFFECT OF LASER IRRADIATION ON THE SURFACE CHARACTERISTICS OF TOOTH ENAMEL (레이저 처리가 치아 법랑질의 표면구조에 미치는 영향)

  • Lee, Ju-Hyun
    • Journal of the korean academy of Pediatric Dentistry
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    • v.33 no.2
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    • pp.201-206
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    • 2006
  • A recent laboratory study has demonstrated improved caries lesion resistance with enamel that was exposed to $CO_2$ laser irradiation for very short time period. When topical fluoride treatment was performed before or after laser irradiation, reductions in dental caries. The purpose of this scanning electron microscopic(SEM) study and atomic force microscope study was to characterize surface alterations in tooth enamel after in vitro laser irradiation alone and combined topical fluoride treatment either before or after laser irradiation. The treatment effects of laser irradiation led to the formation of an irregular, mild porosities and fine fissures, also created granular materials. But when laser irradiation was followed by APF, the enamel surface had homogenous architecture. The result led to the caries resistance effects by these granular structures have been considered to represent redeposited mineral phases due to the mobilization of calcium, phosphate, and fluoride from lased enamel.

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Analysis Technique for Chloride Penetration in High Performance Concrete Behavior Considering Time-Dependent Accelerated Chloride Diffusivity (촉진염화물 확산계수의 시간의존성을 고려한 고성능 콘크리트의 염화물 침투 해석기법)

  • Kwon, Seung-Jun;Park, Sun-Gyu
    • Journal of the Korea Concrete Institute
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    • v.25 no.2
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    • pp.145-153
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    • 2013
  • Recently, accelerated chloride diffusion coefficients are used for an evaluation of chloride behavior. Similar as apparent diffusion coefficients, accelerated diffusion coefficients decrease with time. In this study, decrease in diffusion coefficient with time is simulated with porosity. Utilizing DUCOM-program, porosities from 15 mix proportions are obtained and diffusion coefficients are modelled with regression analysis of porosity for 270 days. Considering non-linear binding capacity which means the relation between free and bound chloride ion, chloride behavior in high performance concrete is evaluated. Through utilizing the previous test results for concrete under chlorides for 180 days, the applicability of the proposed technique is verified. The proposed technique is evaluated to reasonably predict the chloride behavior in concrete with various w/c (water to cement) ratios and mineral admixtures (GGBFS and FA). It is also shown that decrease in chloride diffusion should be considered for chloride prediction in concrete with mineral admixture since it has very clear decrease in diffusivity with time.

RECONSTRUCTION OF ANTERIOR TEMPORAL DEPRESSION AFTER THE CORONAL APPROACH (Coronal approach 시행 후 발생한 측두부 함몰의 재건)

  • Kim, Il-Kyu;Ryu, Seong-Hyun;Kim, Jae-Woo;Kim, Dong-Soo;Choi, Jin-Ho
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.27 no.2
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    • pp.183-187
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    • 2005
  • The coronal approach has been used for over a century by neurosurgeons to access to the anterior cranium. Indications for the coronal approach expanded from use in the correction of congenital skeletal anomalies to applications in acute maxillofacial trauma and secondary deformity correction, oncologic surgery and reconstruction, and esthetic surgery. Complications were such as injury to frontal branch of the facial nerve, motor nerve paralysis, hematoma under flap, trismus, ptosis, epiphora, infection and anterior temporal depression. $Medpor^{(R)}$ is made up of dense polyethylene connected in porous structures. It is easily shapable without collapsing the pores due to it's hardness and tissue growth takes place at the porosities. Based on these advantages, $Medpor^{(R)}$ has been used in augmentation and restoration in craniofacial defect. A temporal depression after the coronal approach for treatment of Le Fort III fracture was successfully reconstruction with $Medpor^{(R)}$ and we report this case with review of literature.

Study on Optimal Welding Condition for Shipbuilding Steel Materials (조선강재의 최적 용접조건에 관한 연구)

  • Kim, Ok-Hwan
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.10 no.6
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    • pp.128-133
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    • 2011
  • In this study, the steel material for shipbuilding(LR-A class) was used, and FCAW was taken advantage of 3G attitude and they are welded by different welding ways. As a result of analyzing wave with welding monitoring system, the stable values are obtained which are the first floor(electronic current 164~182 A, voltage 24 V), the second floor(electronic current 174~190 A, voltage 22~25 V), the third floor(electronic current 158~188 A, voltage 22~25 V), and fourth floor(electronic current 172~184 A, voltage 22~25 V), at this time, the stable wave standard deviation and changing coefficient could be obtained. When the welding testing through nondestructive inspection was analyzed know defect of welding, there was no defect of welding in A, D, E, but some porosities in B, and slag conclusion near the surface in C, because the length of arc was not accurate, and the electronic current and voltage was not stable. After observing the change of heat affect zone through micro testing, each organization of floor formed as Grain Refinement, so welding part was fine, the distance of heat affect zone is getting wider up to change the values of the electronic current and voltage. As a result of degree of hardness testing, the hardness orders were the heat affect zone(HAZ), Welding Zone(WZ), and Base Metal(BM). When the distribution of degree of hardness is observed. B is the highest degree of hardness The reason why heat effect zone is higher than welding zone and base metal, welding zone is boiled over melting point($1539^{\circ}C$) and it starts to melt after the result of analysis through metal microscope, so we can know that delicate tissue is created at the welding zone. Therefore, in order to get the optimal conditions of the welding, the proper current of the welding and voltage is needed. Furthermore the precise work of welding is required.

Experiment of the Shelter Effect of Porous Wind Fences base on the Wind Tunnel Test (풍동실험을 이용한 다공성 방풍팬스의 방풍성능실험)

  • You, Jang-Youl;Jeon, Jong-Gil;Kim, Young-Moon
    • Proceeding of KASS Symposium
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    • 2006.05a
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    • pp.91-101
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    • 2006
  • We have conducted the study about the shelter effect against the wind by using the wind fence with various porosities and the measured distance from the wind fence, in three different types of it ; (Circle wind fence, Vertical wind fence, Horizontal wind fence) The shelter effect and turbulence characteristics of the selected wind barrier is throughly investigated by wind tunnel test. flow characteristics of velocities and turbulences behind wind fence were measured using hot-wire anemometer. we characterize the turbulence behind the wind fence by varying the porosity of 0 %, 20 %, 40%, and 60%, and the distances from the wind fence from 1 H to 9 H with maintaining the uniform flow velocity of 6 m/s. In addition, we investigated the overall characterization of the wind fence by measuring total of twenty eight points on the wind fence, which forms the lattice structure on it with seven points in lateral direction and four points in vertical direction. The results of analysis from the circle wind fence indicate that the degree of the turbulence is lowered and the velocity of the wind is decreased when the porosity of 40 % are used at the distance from 3 H to 9 H. On the other hand, the vertical, horizontal wind fence with the porosity of 20% is more advantageous at the distance of 2 H to 9 H. For the effectiveness of the wind fence depending on the position, the center part is the greatest and it decreases at the edges with 10 % to 30 % less than that of at the center.

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A STUDY ON THE BONDING BEHAVIOR OF PALLADIUM-BASED ALLOYS FOR CERAMO-MENTAL RESTORATION (도재 소부용 팔라디움계 합금의 도재 결합양상에 관한 연구)

  • Chang, Hoon;Lim, Ho-Nam;Choi, Boo-Byung
    • The Journal of Korean Academy of Prosthodontics
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    • v.27 no.1
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    • pp.143-179
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    • 1989
  • To observe the bonding behavior of palladium-based alloys to porcelain; 1. Pd-Co binary alloy with the higher cobalt content, 2. Pd-Co binary alloy with the lower cobalt content, 3. Pd-Ag-Sn ternary alloy, 4. Pd-Ag binary alloy, 5. Pd-Cu-Au ternary alloy and 6. Pd-Cu binary alloy were made as 6 groups of experimental alloys. Each group of alloy was divided into 4 sub-groups such as one sub-group that was not degassed and three sub-groups that degassed for 5 minutes, 10 minutes and 15 minutes. On each specimen, weight changes after degassing, morphological changes of oxide layer by changing the degassing time, compositional changes at metal-ceramic interface and bond strength of metal-ceramic measured with planar shear test were observed and compared. The results of the present study allow the following conclusions to be drawn: 1. The alloy showing the greatest bond strength was Pd-Cu alloy without gold and bond strength was decreased by alloying gold to them. 2. Although Pd-Co alloy showed the most prominent oxidation behavior, bond strength of them to porcelain was not greatly high by the formation of porosities at metal-ceramic interfaces. 3. Likewise tin, cobalt formed the peaks on line profiles at metal-ceramic interface, however copper did not exhibit such peaks on line profiles. 4. Mainly, oxide layer on Pd-Co alloy was composed with cobalt, and for Pd-Co alloy with higher cobalt content the rise of bond strength was not significant by increased degassing time. 5. On Pd-Ag alloy not containing tin, during degassing for 15 minutes silver content was increased at metal-ceramic interface. 6. As an oxidized element, tin formed the oxide layers that widen their area by increasing the degassing time, while cobalt and copper showed the morphological changes of particle or crystal on oxide layer.

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UV-INDUCED POLYMERIZATION OF SIZE-CONTROLLED PLATINUM/POLY[STYRENE-DIVINYLBENZENE-TRI(PROPYLENE GLYCOL) DIACRYLATE] HYDROPHOBIC CATALYST BEADS IN MICROFLUIDICS

  • WEI, JUN;LI, XIANG;SONG, TONG;SONG, ZI-FAN;CHANG, ZHEN-QI;MENG, DA-QIAO
    • Nuclear Engineering and Technology
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    • v.47 no.6
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    • pp.738-745
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    • 2015
  • The catalytic exchange of hydrogen isotopes between hydrogen and water has been known to be a very useful process for the separation of tritium from tritiated water. For the process, a highly active hydrophobic catalyst is needed. This study provides an effective fabrication method of size-controlled platinum/poly[styrene-divinylbenzene-tri(propylene glycol) diacrylate] [Pt/poly(SDB-TPGDA)] hydrophobic catalyst beads with a narrow size distribution. Platinum nanoparticles were prepared by ${\gamma}$-ray-induced reduction in the aqueous phase first, and then uniformly dispersed in SDB-TPGDA comonomer after the hydrophobization of platinum nanoparticles with alkylamine stabilizers. The porous Pt/poly(SDB-TPGDA) hydrophobic catalyst beads were synthesized by the UV-initiated polymerization of the mixture droplets prepared in a capillary-based microfluidic system. The size of as-prepared catalyst beads can be controlled in the range of $200-1,000{\mu}m$ by adjusting the flow rate of dispersed and continuous phases, as well as the viscosity of the continuous phase. Sorbitan monooleate and cyclohexanol were used as coporogens to control the porosities of the catalyst beads.