• Title/Summary/Keyword: Pore Morphology

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Effect of the Mold Temperatures on the Microstructure and Mechanical Properties of Low Pressure Die-Cast Product (저압주조품의 미세조직과 기계적성질에 미치는 금형온도의 영향)

  • Lee, Jeong-Keun;Park, Chong-Sung;Kim, Myung-Ho
    • Journal of Korea Foundry Society
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    • v.18 no.3
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    • pp.254-261
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    • 1998
  • Microstructure and mechanical properties of the low pressure die-cast Al wheels were investigated by microscope, image analyzer, NDT (non-destructive test), and tensile test. The variation of SDAS (secondary dendrite arm spacing), porosity per unit area, quality grade, and tensile properties with the mold temperatures were examined. SDAS was gradually decreased with a decrease in temperature. However, the lowest value of porosity per unit area was observed at the mold temperature of $405^{\circ}C$ and the optimum mold temperature was found to be $405^{\circ}C$. Besides, from the observation of pore morphology, it was also found that the pore formation was mainly caused by shrinkage during solidification. The tensile strength, elongation, and impact toughness were markedly decreased, however the yield strength was nearly constant. The decrease of mechanical properties is attributed to the increase of porosity.

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Bio-degradable 3D-scaffold fabrication using rapid-prototyping system (쾌속조형시스템을 이용한 생체 조직 재생용 지지체 제작과 특성분석)

  • Kim, Ji-Woong;Park, Ko-Eun;Lee, Jun-Hee;Park, Su-A;Kim, Wan-Doo
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.1697-1699
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    • 2008
  • The purpose of tissue engineering is to repair or replace damaged tissues or organs by a combination of cells, scaffold, suitable biochemical and physio-chemical factors. Among the three components, the biodegradable scaffold plays an important role in cell attachment and migration. In this study, we designed 3D porous scaffold by Rapid Prototyping (RP) system and fabricated layer-by-layer 3D structure using Polycarprolactone (PCL) - one of the most flexible biodegradable polymer. Furthermore, the physical and mechanical properties of the scaffolds were evaluated by changing the pore size and the strand diameter of the scaffold. We changed nozzle diameter (strand diameter) and strand to strand distance (pore size) to find the effect on the mechanical property of the scaffold. And the surface morphology, inner structure and storage modulus of PCL scaffold were analyzed with SEM, Micro-CT and DMA.

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Assesment of Human Skin Surface and Measurement of Temperature upon Applying Pump Type Cosmetics (펌프 타입 화장품 도포에 따른 피부 표면 평가와 온도 측정)

  • Cho, Wan-Goo;Park, Jee-Eun
    • Journal of the Korean Applied Science and Technology
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    • v.27 no.2
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    • pp.144-151
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    • 2010
  • Over the years, scientists have developed many test methods to evaluate the efficacy of skin care products. The needs for objective assessment have stimulated to develop instruments that are capable of reliably monitoring some parameters in evaluating skin conditions. The beauty is evaluated as a measure of smoothness of skin surface. Quantitative size measurements of skin pores is also important concept to evaluate the their conditions. The purpose of this paper is to measure the temperature change of skin and the size of pores in the skin. The pore sizes were changed by its varying skin temperature. They were decreased by applying a essence which is contained with propellant and contents.

Hydrophobic Membrans of Tetrafluoroethylene and 2,2,4, Trifluoro 5 Trifluorometoxy 1,3 Dioxole

  • Gordano, A.;Clarizia, G.;Tocci, E.;Drioli, E.
    • Korean Membrane Journal
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    • v.1 no.1
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    • pp.50-58
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    • 1999
  • Symmetric asymmetric and composite perfluoropolymer membranes made with HYFLON AD have been prepared and evaluated. Porous and non porous symmetric membranes have been prepared by solvent evaporation with various processing conditions. Non-contact atomic force microscopy (AFM) was used to investigate the membrane morphology in air. Analysis of the images gave quantitative imformation on the surface pore strcture in particular on the pore size distributin. Possible useful uses of porous membranes are envisaged in the field of gas-liquid separations such as membrane contactors (MSc) Molecular Dynamics(MD) simulations structure of HYFLON AD 60X copolymer supporting these results are also reported. Amorphous perfluoropolymer membranes appears to be ideal other than in MCs when separation processes have to be performed in hostile environments i.e. high temperatures and aggressive non-aqueous media such as chemicals and solvents. In these cases HYFLON AD mem-branes can exploit the outstanding resistance of perfluoropolymers.

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Coarsening Effects on the Formation of Microporous Membranes

  • Song, Seung-Won
    • Proceedings of the Membrane Society of Korea Conference
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    • 1995.04a
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    • pp.1-4
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    • 1995
  • The microstructure of polymer membranes produced via thermally induced phase separation (TIPS) of polymer solutions is a strong function of both the early-stage (by spinodal decomposition or nucleation & growth) and the late-stage phase separation (referred to in general as coarsening). In the case of early stage effects, the membrane morphology resulting from a nucleation & growth mechanism is either a poorly interconnecsed, stringy, beady structure which is mechanically fragile or a well interconnected structure with highly nonuniform pore sizes. In contrast, spinodal decomposition results in a well interconnected, mechanically strong membrane with highly uniform pore sizes. Here I describe recent quantitative studies of the coarsening effects on the microstructure of membranes produced via TIPS process. The dependence of microstructure on coarsening time, quench depth, solution viscosity, and polymer molecular weight was investigated in order to distinguish among three possible coarsening mechanisms, Ostwald ripening, coalescence, and hydrodynamic flow, which may be responsible for structural evolution after the early-stage phase Separation (spinodal decomposition or nucleation & growth).

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Porous Materials Based on Nickel and Aluminum

  • Dubinina, L.V.;Lopatin, V.U.;Narva, V.K.;Shugaev, V.A.;Vin, Tein
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.614-615
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    • 2006
  • Investigation of influence the morphology of initial powder particles, application pore-formers for sintering of nickel powders and application of flux for sintering of aluminum was made. Using different methods was prepared material with size of porous in wide range size of pores ($1-500{\mu}m$). Using the flux for gravity sintering of aluminum in air atmosphere was manufactured porous material with porosity about 45%..

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Corrosion resistance performance of arc thermal sprayed Al and Al/epoxy dual metal polymeric coating in 3.5 wt.% NaCl-contaminated concrete pore solution (3.5 wt.% NaCl로 오염된 콘크리트 기공 용액에서 아크 용사 Al 및 Al/에폭시 이중 금속 고분자 코팅의 내식성 성능)

  • Singh, Jitendra Kumar;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.11a
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    • pp.119-120
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    • 2023
  • Corrosion of the steel rebar in coastal environment caused huge economical loss of the globe. Therefore, coating on the steel rebar being used to mitigate the corrosion. In the present study, we have applied epoxy coating on arc thermal sprayed Al coating (a dual metal/polymeric coating) vis-à-vis compared with as coated one (Al coating). The corrosion studies were performed in simulated concrete pore solution with 3.5 wt. % NaCl solution. The morphology of the dual epoxy/Al coating is smooth while Al coating shows rankle and defects. Due to defects, Al coating is susceptible to corrosion while dual epoxy/Al coating has performed excellent compared to as coated one at extended period of immersion.

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Morphology and distribution of some marine diatoms, Family Rhizosoleniaceae, in Korean coastal waters: a genus Rhizosolenia 1

  • Yun, Suk-Min;Lee, Jin-Hwan
    • ALGAE
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    • v.25 no.4
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    • pp.173-182
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    • 2010
  • Four Rhizosolenia species of marine diatom were appeared at 30 sites in Korean coastal waters from September 2008 to February 2010. The cell shape, diameter, length of pervalvar axis, external process, segment and areolation characters of the species were examined. All four species were cylindrically shaped, but the external processes differed. Segment striations were regularly straight, and velum showed hexagonal, circular pore and narrow slit. Rhizosolenia formosa and R. hyalina were only occurred in September 2008 from the Yellow Sea, R. bergonii was appeared throughout the year from Korea Strait and Yangyang coasts, and R. setigera was abundantly showed in all seasons from all site. R. formosa is a newly recorded species in Korean coastal waters.

Effects of carbonization temperature on pore development in polyacrylonitrile-based activated carbon nanofibers

  • Lee, Hye-Min;An, Kay-Hyeok;Kim, Byung-Joo
    • Carbon letters
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    • v.15 no.2
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    • pp.146-150
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    • 2014
  • In this work, activated carbon nanofiber (ACNF) electrodes with high double-layer capacitance and good rate capability were prepared from polyacrylonitrile nanofibers by optimizing the carbonization temperature prior to $H_2O$ activation. The morphology of the ACNFs was observed by scanning electron microscopy. The elemental composition was determined by analysis of X-ray photoelectron spectroscopy. $N_2$-adsorption-isotherm characteristics at 77 K were confirmed by Brunauer-Emmett-Teller and Dubinin-Radushkevich equations. ACNFs processed at different carbonization temperatures were applied as electrodes for electrical double-layer capacitors. The experimental results showed that the surface morphology of the CNFs was not significantly changed after the carbonization process, although their diameters gradually decreased with increasing carbonization temperature. It was found that the carbon content in the CNFs could easily be tailored by controlling the carbonization temperature. The specific capacitance of the prepared ACNFs was enhanced by increasing the carbonization temperature.

Effect of High-Temperature Spinning and PVP Additive on the Properties of PVDF Hollow Fiber Membranes for Microfiltration

  • Cha, Bong-Jun;Yang, Jung-Mok
    • Macromolecular Research
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    • v.14 no.6
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    • pp.596-602
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    • 2006
  • The effect of high-temperature spinning and poly(vinyl pyrrolidone) (PVP) additive on poly(vinylidene fluoride) (PVDF) hollow fiber membranes was investigated using differential scanning calorimetry, X-ray diffraction measurement, and scanning electron microscopy, together with the corresponding microfiltration performances such as water flux, rejection rate, and elongational strength. Using high-temperature spinning, porous hollow fiber membranes with particulate morphology were prepared through PVDF crystallization. The particulate structure of the membranes was further modified by the addition of miscible PVP with PVDF. Due to these effects, the rejection rate and strength of the fibers were increased at the expense of reduced water flux and mean pore size, which indicates that high-temperature spinning and PVP addition are vary effective to control the morphology of PVDF hollow fiber membranes for microfiltration.