• Title/Summary/Keyword: Pole-figure

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Texture and surface analysis of NiO prepared on biaxially textured Ni substrates by MOCVD method (2축 정렬된 Ni 선재 위에 MOCVD법에 의한 NiO의 조직 및 표면 분석)

  • 선종원;김형섭;지봉기;박해웅;홍계원;박순동;정충환;전병혁;김찬중
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2002.02a
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    • pp.119-122
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    • 2002
  • The NiO buffer layers for YBCO coated conductor were prepared on textured Ni substrates by MOCVD method and the degree of texturizing and the surface roughness were analyzed X-ray pole figure and AFM and SEM. Processing variables were oxygen partial pressure and substrate temperature. (200) textured NiO layer was formed at 450~$470^{\circ}C$ and oxygen partial pressure of 1.67 Torr. Out-of-plane($\omega$-scan) and in-plane($\Phi$-scan) texture were $10.34^{\circ}$ and $10.00^{\circ}$ respectively. The surface roughness estimated by atomic force microscopy was in the range of 3.1~4.6 nm.

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Effect of Prefiring Time on Epitaxy and crystallinity of Pb(Zr, Ti)O$_3$ Thin Films in Low Temperature Pyrolysis (저온도포열분해에 의해 제조된 Pb(Zr, Ti)O$_3$ 박막의 에피탁시와 결정화도에 미치는 전열처리 시간의 영향)

  • 황규석;이형민;김병훈
    • Journal of the Korean Ceramic Society
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    • v.35 no.9
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    • pp.969-973
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    • 1998
  • Pb(Zr, Ti)O3 (PZT) (Zr:Ti= 52: 48) thin films were prepared on MgO(100) substrates by dipping-py-rolysis process using metal naphthenates as starting materials. Thin films were fabricated by spin coating technique and the precursor films were prefired at 20$0^{\circ}C$ in air for 0.5, 1, 2, 3, and 24 h followed by final heat treatment at 75$0^{\circ}C$ for 30min. Film prefired for 24 h lost orientational properties and pole figure analysis showed the lost of the epitaxial relationship between the films and substrate while highly a/c-axis oriented thin films were obtained for the samples prefired for 1, 2, and 3h.

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Simplified 3D Finite Element Analysis of Linear Inductor Motor for Integrated Magnetic Suspension/Propulsion Applications (자기부상 및 추진 일체형 리니어 인덕터 모터의 간이형 3차원 유한요소해석)

  • Jeong, Sang-Sub;Jang, Seok-Myeong
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.49 no.6
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    • pp.371-379
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    • 2000
  • The 4-pole linear homopolar synchronous motor (LHSM), so called linear inductor motor, is composed of the figure-of-eight shaped 3-phase armature windings, DC field windings, and the segmented secondary with the transverse bar track. To reduce the calculation time, the simplified 3D finite element model with equivalent reluctance and/or permanent magnet is presented. To obtain a clear understanding, propriety and usefulness of the developed model, we compare with the results of simplified 3D FEA, general 3D FEA and test. Consequently, the results of simplified and 3D FEM analysis are nearly identical, but much larger than that of static test at d-axis armature excitation. Therefore the improved FEA model, such as full model with half slot, is needed for the precise analysis.

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Synthesis of fiber-textured diamond films by MWPECVD (마이크로파 플라즈마 CVD법에 의한 섬유집합조직 다이아몬드막의 합성)

  • 박재철;김병상
    • Electrical & Electronic Materials
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    • v.9 no.5
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    • pp.470-475
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    • 1996
  • Fiber-textured diamond films have been deposited on scratched silicon(100) substrate by micro wave .plasma enhanced chemical vapor deposition at the condition of micro wave power : 950 W, pressure : 60 torr, H$_{2}$ gas flow rate : 50 sccm, CH$_{4}$ gas flow rate : 1.5 sccm, substrate temperature : about 900.deg. C and deposition time : 20 hours. The films were characterized by mean of scanning electron microscopy, Raman spectroscopy and X-ray analysis.

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A study of texture through the depth of superconductor core (BSCCO 선재에서 초전도심의 깊이에 따른 집합조직 연구)

  • 지봉기;임준형;이동욱;장석헌;주진호;나완수
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 2001.02a
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    • pp.6-8
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    • 2001
  • We evaluated the degree of texture through depth of the superconductor core of Bi-Sr-Ca-Cu-O(BSCCO) superconductor tape. The degree of texture was characterized by pole figure analysis, indicating that the degree of texture varied significantly with depth of the superconductor core. It was observed that the degree of texture was higher near the interface than inside the superconducting core. Based on the result of degree of texture, the region near the interface is thought to carry significant current compared to that inside the core.

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Epitaxial Growth of Pb(Zr, Ti)$O_3$Thin Films on $LaAlO_3$ Substrates by Dipping-Pyrolysis Process

  • Hwang, Kyu-Seog;Kim, Byung-Hoon
    • The Korean Journal of Ceramics
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    • v.3 no.4
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    • pp.253-256
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    • 1997
  • Epitaxially grown Pb(Zr, Ti)O$_3$thin films were prepared on LaAlO$_3$substrates by the dipping pyrolysis process using metal naphthenates as starting materials Homogeneous Pb-Zr-Ti solutions with toluene were spin-coated onto the substrates and pyrolyzed at 50$0^{\circ}C$ Highly oriented Pb(Zr, Ti)O$_3$films confirmed by X-ray diffraction $\theta$-2$\theta$ scans were obtained by heat-treated at 75$0^{\circ}C$ in air The X-ray pole-figure analysis and reciprocal-space mapping of the resulting 0.6$\mu\textrm{m}$ films showed that the thin films comprising the c-axis oriented tetragonal phase have an epitaxial relationship with the LaAlO$_3$substrates.

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Texture in hot-pressed silicon carbide (고온가압소결한 탄화규소의 집합조직)

  • 김영욱;김원중
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.5 no.4
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    • pp.343-350
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    • 1995
  • A Abstract Systematic studies of the effects of crystalline forms of starting powders and p processing variables on the texture of hot - pressed silicon carbide are described. The results I indicate that hot - pressing of $\beta$ - SiC can produce strong textures and composite type duplex microstructure due to the ${\beta} {\rightarrow} {\alpha}$ phase transformation of SiC. The texture variations d during post - annealing have been observed. In the case of using a - SiC as starting pow¬d ders, the degree of preferred orientation by hot - pressing is relatively weak.

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Deposition of NiO on hi-axially textured Ni substrates fort YBCO coated conductor by a MOCVD method (양축정렬된 textured Ni 기판위에 MOCVD법을 이용한 YBCO coated conductor 완충층용 NiO 증착)

  • 선종원;김형섭;박순동;정충환;전병혁;김잔중
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.531-534
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    • 2002
  • NiO buffer layers for YBCO coated conductors were deposited on hi-axially textured Ni substrates by MOCVD(metal organic chemical vapor deposition) method, using single solution source. To establish the processing condition, oxygen partial pressure and deposition temperature were changed. The surface orientation and degree of texture were estimated by X-ray diffraction, X-ray pole figure and atomic force microscopy. The FWHMs of in-plane and out-of-plane of the NiO films were about 10$^{\circ}$. The surface roughness was a function of deposition temperature. The AFM surface roughness of NiO films is in the range of 3∼10 nm, when NiO films was grown at 450∼530$^{\circ}C$.

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Texture development in cold-roiled and heat-treated Ni tapes (냉간가공과 열처리한 Ni 테이프에서의 집합조직 발달)

  • 이동욱;지봉기;임준형;주진호;정충환;박순동;전병혁;홍계원;김찬중
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.07a
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    • pp.535-538
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    • 2002
  • Cube-textured Ni substrates for YBCO coated conductors were fabricated by cold-rolling and annealing of Ni powder compacts. To establish the optimum sintering temperature, tensile test was performed for the Ni rod sintered at various temperatures. The Ni rods prepared at above 100$0^{\circ}C$ showed good mechanical properties due to the complete densification of the Ni rods. The Ni rods were rolled to final thickness of 100 ${\mu}{\textrm}{m}$ and then annealed at 100$0^{\circ}C$ for various annealing time for texture development. The texture analysis made by 2 $\theta$ scan and pole-figure showed that the cube texture was developed in a short time of a few munitues. The FWHM of in-plane and out of plane texture of the prepared Ni tapes was 8-10$^{\circ}$. The AEM surface roughness of the Ni tapes was as smooth as 3 nm.

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