• Title/Summary/Keyword: Polarization measurement

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Electrochemical Characteristics under Cavitation-Erosion Environment of STS 304 and Hot-Dip Aluminized STS 304 in Sea Water Solution (천연해수 용액에서 STS 304와 용융 알루미늄 도금된 STS 304의 캐비테이션-침식 환경 하에서의 전기화학적 특성)

  • Chong, Sang-Ok;Kim, Seong-Jong
    • Journal of the Korean institute of surface engineering
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    • v.49 no.1
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    • pp.26-31
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    • 2016
  • In this paper, the characteristics of a cavitation-erosion damage behavior on the STS 304 and hot-dip aluminized STS 304 under cavitation environment in sea water solution was investigated. The electrochemical experiments were carried out by potential measurement, anodic/cathodic polarization test, Tafel analysis, and also galvanostatic experiment in current density variables for the samples. The apparatus of cavitation-electrochemical experiment was manufactured in compliance with modified ASTM G-32 standard, with the conditions of sea water temperature of $25^{\circ}C$ and the measurement, amplitude of $30{\mu}m$. The damage behavior was analyzed by an observation of surface mophologies and a measurement of damage depth by a scanning electron microscope(SEM) and a 3D microscope, respectively, after electrochemical test. After polarization experiment under cavitation environment, much higher damage depths for the hot-dip aluminized STS 304 were observed comparing to the untreated STS 304. In addition, higher corrosion current density in hot-dip aluminized STS 304 presented than that of untreated STS 304 as a result of Tafel analysis.

Measurement of the Indoor Wireless Environment at 2.45 GHz (2.45 GHz 대역 실내 무선 환경 측정)

  • Hwang Jae-Ho
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2006.05a
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    • pp.1005-1008
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    • 2006
  • In this paper, we provide data of wireless environment in indoor for Bluetooth and wireless LAN systems. To accurately measure transmission characteristic for influence of the indoor wall, we used radiation measurement system with antennas. And various structure and material of the indoor wall are measured. Results of the measurement show that the attenuation of power is about $1\sim3dB$ for cement wall(25cm). In the case of cement wall with steel frame, the attenuation of power was increased using horizontal polarization but was not affect using vertical polarization.

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The dependence of the electric field effect of diffraction efficiency using polarization beam on calcogenide thin films (칼코게나이드 박막에서 편광 빔 회절 효율의 전계 효과 의존성)

  • Jang, Sun-Joo;Yeo, Cheol-Ho;Park, Jeong-Il;Lee, Hyun-Yong;Chung, Hong-Bay
    • Proceedings of the KIEE Conference
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    • 1999.07d
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    • pp.1861-1863
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    • 1999
  • The polarization gratings were fabricated in chalcogenide $As_{40}Ge_{10}Se_{15}S_{35}$ thin film applicable to a medium of the polarization holography and their diffraction efficiencies$(\eta)$ were monitored by real-time measurement. The polarization gratings prepared consisted of the multi-layer thin film system. As a method to improve the $\eta$, we have investigated its change for the field effect. As the results, the value of $\eta$ strongly depended on the voltage applied to the film and the maximum value, $\eta_{max}$ was enhanced to be about 4 times in comparison with that of not biased sample. In addition, an increase in the $\eta$ can be estimated to be due to additional creation of new defects caused by the electric field across the film.

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A new, hybrid, heterodyne, fiber-optic electric field sensor scheme and its applications (I/Q 변조 풀이 방식의 헤테로다인 간섭계를 이용한 미소 전기장 및 복굴절 측정)

  • 윤신영;조규만;이용산
    • Korean Journal of Optics and Photonics
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    • v.8 no.2
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    • pp.161-164
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    • 1997
  • A new hybrid, heterodyne, fiber-optic electric field sensor scheme is presented. In this scheme, a dual polarization, dual frequency, stabilized He-Ne laser is used for the light source of the interferometer, Probe beam is delivered to the sensor head using polarization maintaining fiber. In the sensor head, $LiTaO_3$ electro-optic crystal is used for sensing element. Phase retardation is induced on the dual frquency, dual polarization probe beam due to applied electric field across the crystal. Induced phase retardation is demodulated by in-phase and quadrature demodulation technique. In this way, we can obtain optimum sensitivity for electric field measurement regardless a quasi-static phase difference between two polarization components.

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Real Time Measurement of Protease Activity of Live Uronema marinum (Ciliata: Scuticociliatida) by Fluorescence Polarization Assay

  • Lee Eun Hye;Kwon Se Ryun;Kim Chun Soo;Chung Joon Ki;Lee Hyung Ho;Kim Ki Hong
    • Fisheries and Aquatic Sciences
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    • v.5 no.4
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    • pp.311-313
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    • 2002
  • Proteolytic activity of live Uronema manum was analyzed by fluorescence polarization (FP) technique. Protease activity was measured by a decrease in FP value using fluorescein isothiocynate (FITC)-casein as a protein substrate. The results demonstrated an inverse linear relationship between fluorescence polarization (FP) values and live ciliate concentration over the range $1\times10^4\;to\;2\times10^5$ cells/well. However, the FP values of $10-10^3$ live parasites were not different significantly from that of control. Time-dependent decrease in FP value was shown in the wells containing live U. marinum. In the present study, FP assay had the benefit to provide measurements of substrate hydrolysis by live parasites in real-time, and did not require separations, precipitations, or transfers of reaction mixture.

Improvement of Chemical Mechanical Polishing (CMP) Performance of Nickel by Additions of Abrasive and Various Oxidizers (산화제 및 연마제 첨가를 통한 Nickel CMP 특성 개선 연구)

  • Choi, Gwon-Woo;Kim, Nam-Hoon;Seo, Yong-Jin;Lee, Woo-Sun
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.7
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    • pp.605-609
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    • 2005
  • Chemical mechanical polishing (CMP) of Ni was performed by the various ratios of four kinds of oxidizers and an addition of alumina powders as an abrasive in each slurry with the different oxidizers. Moreover, the interaction between the Ni and the each oxidizer was discussed by potentiodynamic polarization measurement, in order to compare the effects of Ni-CMP and electrochemical characteristics on the Ni with the different oxidizers. As an experimental result, the removal rate of Ni reached a maximum at 1 $vol\%$ of $H_2O_2$. Also the removal rates of Ni increased with the audition of alumina abrasives in each slurry. The potentiodynamic polarization of Ni under dynamic condition showed a significant difference in electrochemical behavior by addition of $H_2O_2$ in solutions. Ni showed the perfect passivation behavior in solution without $H_2O_2$ under potentiodynamic polarization condition, while active dissolution dominates in solution with the addition of $H_2O_2$. The results indicate that the surface chemistry and electrochemical characteristics of Ni play an important role in controlling the polishing behavior of Ni.

Measurements of optical wavelength using an optical fiber retarder (광섬유 위상지연기를 이용한 광파장 측정)

  • 이현우;김용평
    • Korean Journal of Optics and Photonics
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    • v.12 no.1
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    • pp.5-9
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    • 2001
  • A wavemeter was realized using the phenomena that the phase lag between principal polarization states in an optical retarder is a function of wavelength. The change in the polarization state of the optical beam as it passes through the optical retarder is dependent on wavelength. The wavelength of the optical beam is determined by comparing the power difference between principal polarization states. A prototype wavemeter was successfully implemented using a polarization maintaining fiber with birefringence $3\times10^{-4}$ and length 100 mm as the optical retarder. The measurement resolution was 0.08 nm over a wavelength region of 1554.38 nm-1557.l9 nm, which agreed well with theoretically calculated results. In addition, the dependence of operating characteristics on temperature was analyzed theoretically and experimentally.mentally.

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A Study on the Post-Weld Heat Treatment Effect Affecting Corrosion Behavior and Mechanical Property of Welding Part of RE36 Steel for Marine Structure (해양구조물용 RE36강 용접부의 부식거동 및 기계적 특성에 미치는 용접후 열처리 효과에 관한 연구)

  • 김성종;문경만
    • Journal of Welding and Joining
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    • v.19 no.1
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    • pp.65-74
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    • 2001
  • A study on the corrosion behavior in case of As-welded and PWHT temperature 55$0^{\circ}C$ of welding part of RE36 steel for marine structure was investigated with parameters such as micro-Vickers hardness, corrosion potential measurement of weld metal(WM), base metal(BM) and heat affected zone(HAZ), both Al anode generating current and Al anode weight loss quantity under sacrificial anode cathodic protection conditions. And also we carried out slow strain rate test(SSRT) in order to research both limiting cathodic polarization potential for hydrogen embrittlement and optimum cathodic protection potential as well as mechanical properties by post-weld heat treatment(PWHT) effect. Hardness of HAZ was the highest among three parts(WM, BM and HAZ) and the highest galvanic corrosion susceptibility was HAZ. And the optimum cathodic polarization potential showing the best mechanical properties by SSRT method was from -770mV to -875mV(SCE). In analysis of SEM fractography, applied cathodic potential from -770mV to -875mV(SCE) it appeared dimple pattern with ductile fracture while it showed transgranular pattern (Q. C : quasicleavage) under -900mV(SCE). However it is suggested that limiting cathodic polarization potential indicating hydrogen embrittlement was under -900mV(SCE).

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Effect of Delayed Oxygen Evolution in Anodic Polarization on the Passive Film Characteristic and Localized Corrosion Resistance of Titanium Alloys (타이타늄 합금에서 산소발생전위 지연이 부동태 피막 특성과 국부부식 저항성에 미치는 영향)

  • Oh, Yu Soo;Seo, Dong-Il;Lee, Jae-Bong
    • Corrosion Science and Technology
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    • v.19 no.3
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    • pp.156-162
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    • 2020
  • The objective of this study was to investigate delayed oxygen evolution and localized corrosion resistance of titanium alloys by performing potentiodynamic polarization, potentiostatic polarization, and Mott-Schottky measurements. Delayed oxygen evolution was compared among titanium alloys, 316 stainless steel, and platinum. Difference in delayed oxygen evolution between titanium alloys and other metals was attributed to specific surface characteristic of each metal. Delayed oxygen evolution of titanium alloys resulted from the predominant process of ionic conduction over electronic conduction. The effect of oxygen evolution on localized corrosion of titanium alloys was investigated using electrochemical critical localized corrosion temperature (E-CLCT) technique. Mott-Schottky measurement was performed to clarify the difference in film properties between titanium alloys and stainless steels. Titanium alloys were found to have much lower donor density than stainless steels by 1/28. These results indicate that delayed oxygen evolution has little influence on the concreteness of passive film and the resistance to localized corrosion of titanium alloys.

Electroplating on the Lead Frames Fabricated from Domestic Copper Plate (국산동판을 사용한 리드프레임 도금기술에 관한 연구)

  • Jang, Hyeon-Gu;Lee, Dae-Seung
    • Journal of the Korean institute of surface engineering
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    • v.19 no.3
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    • pp.92-108
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    • 1986
  • An electroplating on the lead frame fabricated from domestic copper plate was studied experimentally. In this study, nickel was plated on the thin copper lead frame and silver layer was coated on the nickel film in the cyanide electrolyte. The effect of process variables such as current density, plating time, coating thickness and flow rate of electrolytic solution on the properties of coating was investigated. Some samples on each step were fabricated during electroplating. The results obtained from polarization measurement, observation of SEM photograph, adhesion test of coating and microhardness test are as follows. On silver plating, polarization resistance of potentiostatic cathodic polarization curve is reduced as the flow rate of Ag electrolytic solution increases. And above resistance is also reduced when the minor chemicals of sodium cyanide and sodium carbonate are added in potassium silver cyanide bath. The reduced polarization resistance makes silver deposition on the cathode easy. An increase in the current density and the coating thickness causes the particle size of deposit to coarsen, and consequently the Knoop microhardness of the coating decreases. On selective plating an increase in the flow rate of plating solution lead to do high speed plating with high current density. In this case, the surface morphology of deposit is of fine microstructure with high Knoop hardness. An increasing trend of the adhesion of coating was shown with increasing the current density and flow rate of electrolytic solution.

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