• Bulletin of the Korean Chemical Society
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• v.27 no.4
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• pp.519-523
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• 2006

Poly(dimethyl siloxane) (PDMS) has been employed as a microchip material for DNA separation in microfluidic condition. Different sieving molecules such as cellulose derivatives having glucose building block (methyl cellulose (MC), hydroxyethyl cellulose (HEC), and hydroxypropyl methyl cellulose (HPMC)) and polyethylene oxide (PEO) having linear (ring-opened ethylene oxide) unit were used and their performance was compared in terms of separation efficiency and resolution. In general, PEO showed better separation performance than cellulose derivatives probably due to the nature of linear shape polymer conformation. It was possible to perform at least 15 consecutive running with 1.2% PEO at the electric field strength around 200 V/cm. Fast analysis of the standard $\Phi$X 174 RF DNA/Hae III (less than 130s) was obtained with the number of the theoretical plate around 250,000/m. Our PMDS microchip was applied to the measurement of CAG repeat number, which is related to male infertile disease.

• Bulletin of the Korean Chemical Society
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• v.24 no.9
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• pp.1333-1338
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• 2003

Hollow Fiber flow field-flow fractionation (HF-FlFFF) has been tested in polyacrylonitrile (PAN) membrane channel in order to compare it with polysulfone (PSf) membrane channel. It has been experimentally shown that the separation time of 0.05-0.304 ${mu}m$ polystyrene latex (PSL) standards in PAN membrane channel is shorter than that in PSf channel by approximately 65%. The optimized separation condition in PAN membrane is ${\dot V}_{out}/{\dot V}_{rad}=1.4/0.12\;mL/min$, which is equal to the condition in PSf membrane channel. In addition both the resolution ($R_s$) and plate height (H) in PAN membrane channel are better than that in PSf membrane channel. The membrane radius was obtained by back calculation with retention time. It shows that the PSf membrane is expanded by swelling and pressure, but the PAN membrane doesn't expand by swelling and pressure.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.11 no.5
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• pp.658-668
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• 1999

The objective of the present study is to investigate the effect of experimental parameters on the hydrodynamic characteristics in a horizontal tee-type evaporator using R-22. The experimental apparatus consisted of an unheated tee-type test section, a liquid-vapor separator, a preheated, mass flow meters, a plate heat exchanger, pump, and other measurement devices. The experimental parameters were mass flux(500 and 600kg/$m^2$s), inlet quality(0.1~0.3) and separation ratio(0.3~0.7). Absolute pressure at the inlet of the test section was 0.652 MPa. The branch-to-inlet inner diameter ratio was 0.61. Pressure gradient at the branch section was larger than that at the run section at the same separation ratio. Pressure drop per unit length increased at the run section and decreased at the branch section as the separation ratio increased. Pressure drop predicted by the separated flow model agreed with experimental data within -35 to +16%. Generally, predicted values showed similar trend with the data. Mass flow ratio of vapor refrigerant was affected by the inlet quality more than the mass flux.

• Clinics in Shoulder and Elbow
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• v.20 no.3
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• pp.153-161
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• 2017

Background: This study was conducted to compare the clinical and radiological outcomes of the locking hook plate fixation (HP) technique and the single tight rope (TR) technique applied for acute high-grade acromioclavicular (AC) joint separations. Methods: Between 2009 and 2014, 135 consecutive patients with acute AC joint separation Rockwood types III, IV, and V were subjected to surgical reconstruction. One hundred fourteen patients (84.4%) were available for retrospective evaluation. Of them, 62 and 52 were treated using the single TR group and clavicular HP group techniques, respectively. The visual analogue scale, Constant, American Shoulder and Elbow Surgeons (ASES), and Taft scores were used for clinical assessment. Postoperative shoulder range of motion was also assessed. An anteroposterior radiograph of the coracoclavicular distance (CCD) was obtained to evaluate the radiographic signs of recurrence. Results: The TR group patients had better Constant, ASES, and Taft scores than the HP group patients. The loss of reduction in terms of the CCD did not differ between groups. Subacromial osteolysis was observed in 34.6% of the cases in the HP group. However, there were no significant differences in the clinical outcomes between the patients with and without osteolysis in the HP group. Subcoracoid osteolysis, drill tunnel widening, and metal displacement were observed in 3.2%, 22.6%, and 4.8% of the cases in the TR group, respectively. Conclusions: The single TR technique was relatively more effective at treating acute high-grade AC joint injuries than the HP fixation technique (level of evidence: therapeutic; retrospective comparative study, Level III).

• Journal of the Korean Society of Safety
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• v.25 no.3
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• pp.71-77
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• 2010

This paper presents the results of a study on flexural capacity of large size RC slabs strengthened with carbon fiber reinforced polymer(CFRP) plates. A total of 5 specimens of 6.0m length were tested in four point bending after strengthening them with externally bonded CFRP plates. The CFRP plates were bonded without prestress and with two prestress levels, 0.4% and 0.6% of CFRP plate strain. Test variables included the type of strengthening, prestressing level, and the effects according to each test variables are analysed. The experimental results show that proposed methods can increase significantly the flexural capacity such as strength, stiffness of the beam and the increase ranged between 36.2% and 63.2% of the load-carrying capacity of the control beams. The non-prestressed specimen failed by separation of the plate from the beam due to premature debonding while most of the prestressed specimens failed by CFRP plate fracture. And the cracking loads and maximum loads were increased proportionally to the prestress level.

• Korean Journal of Air-Conditioning and Refrigeration Engineering
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• v.10 no.2
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• pp.193-201
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• 1998

A heat exchanging system employing the impinging air jet is still widely used In the various fields due to its inherent merits that include the easiness in engineering applications and the high heat and/or mass transfer characteristics. The purpose of this study is to investigate the enhancement of heat transfer and flow characteristics by placing a turbulence promoters in front of heat exchanging surface. In this study, a series of circular rods are placed at the upstream of a flat plate heat exchanger that is located at potential core region(H/W=2) of a two-dimensional impinging air jet. Heat transfer enhancement is achieved by inserting turbulence promoter that results in the flow acceleration and disturbance of boundary layer. The average Nusselt number of the flat plate with the turbulence promoters is found to be around 1.42 times higher than that of the flat plate without the turbulence promoters. Based on the results of flow visualization with a smoke wire, it is confirmed that the heat transfer enhancement is caused by the flow separation and disturbance of boundary layer by inserting the turbulence promoter.

• Proceedings of the KSME Conference
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• 2000.11b
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• pp.87-92
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• 2000

This study is to investigate the heat transfer characteristics the for a round turbulent jet impinging on the flat plate with and without rib. Liquid crystal/transient method was used to determine the Nusselt number distributions along the surface. The temperature on the surface was measured using liquid crystal and a digital color image processing system. The experiments were made fur the jet Reynolds number (Re) 23,000, the dimensionless nozzle-to-surface distance (L/d) from 2 to 10, and the rib type [height ($d_1$) 2mm, pitch (p) from 12 to 36mm]. It was found that for $L/d{\ge}6$ the average Nusselt numbers on the flat plate with rib type C ($p/d_1=16$) are higher than those without rib, mainly due to an increase in the turbulent intensity caused by flow separation, recirculation and reattachment on the wall surface.

• Proceedings of the KSME Conference
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• 2001.11b
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• pp.124-130
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• 2001

The heat transfer and flow measurements were made on a cylindrical pedestal mounted on a flat plate with a turbulent impinging air jet. The heat transfer coefficient distributions on the flat plate were measured using the shroud-transient technique and liquid crystal was used to measure the surface temperature. The jet Reynolds number (Re) is 23,000, the dimensionless nozzle-to-surface distance (L/d) from 2 to 10, the dimensionless pedestal diameter-to-height (H/D) from 0 to 1.5, the dimensionless 2nd pedestal diameter-to-height ($H/D_2$) from 0 to 0.4 and the distance from the stagnation point to 2nd pedestal (p/D). The results show that for H/D = 0.5 to 1.5, the Nusselt number distributions on the plate surface exhibit a maximum between $r/d\;{\cong}\;1.0$ and 1.5. The presence of the pedestal appears to cause the flow separation and reattachment on the plate surface, which results in the maximum heal transfer coefficient. Also, for p/D = 2.5 and $H/D_2$ = 0.3, the local Nusselt number in the region corresponding to $r/d\;{\cong}\;1.1$ was increased up to 50% compared to that for $H/D_2=0$.

• Proceedings of the KSME Conference
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• 2000.04b
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• pp.465-471
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• 2000

The flow characteristics around an elliptic cylinder with axis ratio of AR=2 located near a flat plate were investigated experimentally to study the interaction between the cylinder wake and the turbulent boundary layer. The pressure distributions on the cylinder surface and on the flat plate were measured with varying the angle of attack of the cylinder. In addition, the velocity profiles of wake behind the cylinder were measured using a hot-wire anemometry As the angle of attack increases, the location of peak pressure on the windward and leeward surfaces of the cylinder moves toward the rear and front of the cylinder, respectively. At positive angles of attack, the position of the minimum pressure on the flat plate surface is moved downstream, but it is moved upstream at negative angles of attack. With increasing the angle of attack, the vortex shedding frequency is gradually decreased and the critical angel of attack exists in terms of the gap ratio. By installing the elliptic cylinder at negative angle of attack, the turbulent boundary layer over the flat plate is disturbed more than that at positive incidence. This may be attributed to the shift of separation point on the lower surface of the cylinder according to the direction of the angle of attack.

• Bulletin of the Korean Chemical Society
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• v.32 no.3
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• pp.915-920
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• 2011

Four esters of succinic and maleic acid were synthesized, separated by thin-layer chromatography (TLC), and identified using matrix-assisted laser desorption/ionization-mass spectrometry (MALDI-MS). A comparison of matrix materials showed that 2,6-dihydroxybenzoic acid (2,6-DHB) yielded a greater ionization efficiency than 2,5-DHB prior to TLC separation. The location of each ester sample on the TLC plate was estimated by comparing the developed plate with a duplicate plate that had been visualized by immersion in a $KMnO_4$ solution. Generally, mass spectra obtained from the $KMnO_4$-visualized plate were relatively poor. Reproducible mass spectra with high peak abundance were difficult to obtain using the 2,6-DHB matrix from crude synthetic esters extracted from the TLC plates. Significant improvements in both reproducibility and sensitivity were realized by using pencil lead as the MALDI matrix. The current methodology will be beneficial to organic chemists since it can provide a guideline for simple and rapid characterization of small organic compounds.