• Title/Summary/Keyword: Plastic viscosity

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Synthesis Conditions and Rheological Characteristics of Aluminum Phosphate (인산 알루미늄의 합성조건과 유동학적 특성)

  • 신화우;안세민;정동훈;강태욱;이광표
    • YAKHAK HOEJI
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    • v.35 no.4
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    • pp.319-325
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    • 1991
  • Aluminum phosphate gel was synthesized by reacting aluminum sulfate as a soluble aluminum salt to tribasic sodium phosphate in this study. The optimal synthesis conditions based on the yield of product were investigated by applying Box-Wilson experimental design. It was found that optimal synthesis conditions were as follows: Reaction temperature; $61~71^{\circ}C$, concentration of two reactants; 12.27~13.83%, concentration ratio of two reactants; [AI$_{2}$(SO$_{4}$)$_{3}$]/[Na$_{3}$PO$_{4}$]= 0.5, reaction time; 10.9~12.1 minutes, drying temperature of product; $60~72^{\circ}C$. Aluminum phosphate gel prepared by the optimal synthesis conditions was suspended with four types of natural and synthetic gums at the concentration of 0.375~1.5wv%. Their Theological properties of aluminum phosphate gels were examined with Haake-Rotovisco RV 20 rotational viscometer. It showed that the higher concentration of suspending agents and lower temperature, the higher viscosity. Aluminum phosphate gel suspended by pectin and agar showed plastic flow with rheopexy, and their gels suspended by sodium alginate and sod. CMC showed plastic flow with thixotropy.

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Measurement of Viscosity and Numerical Analysis of High Speed Injection Molding for Thin-Walled LGP (박형 도광판의 고속사출성형을 위한 수지 점도 측정 및 수치해석)

  • Jung, T.S.;Kim, J.S.;Ha, S.J.;Cho, M.W.
    • Transactions of Materials Processing
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    • v.23 no.1
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    • pp.41-48
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    • 2014
  • The light guide plate has become the major component for the backlight module in general information technology products (e.g. mobile phones, monitors, etc.). High speed injection molding has been adopted for thin walled LGP giving advantages such as weight, shape, size, and reduction in production costs. In the current study, the rheological characteristics of high liquidity plastic resin PC(HL8000) were measured using a capillary rheometer to improve the reliability of the numerical analysis for high speed injection molding. With the measured viscosity and PVT of PC(HL8000), numerical analysis of injection molding was conducted using the simulation software(Moldflow). Filling time and deflection were predicted and compared with those of traditional PC resins(H3000, H4000). The results show that PC(HL8000) has significantly different rheological characteristics during high speed injection molding. Hence proper properties of the resin should be used to improve the accuracy of numerical predictions.

An Experimental Study on Biaxial Tensile Characteristics of ETFE Film and Stress Relaxation of Tension Typed Membrane Structures (ETFE 필름의 2축 인장특성 및 텐션방식 막구조물의 응력완화 거동에 관한 실험적 연구)

  • Kim, Seung-Deog;Jeong, Eul-Seok;Kawabata, Masaya
    • Journal of Korean Association for Spatial Structures
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    • v.16 no.1
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    • pp.35-42
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    • 2016
  • Until recently, almost all ETFE film structures that have been erected is the cushion type because there are problems at lower allowable strength under elastic range and viscosity behaviour such as creep and relaxation of ETFE films under long-term stresses. But the number of tension type structures is currently increasing. This paper proposes the stretch fabrication of ETFE film to verify the applicability of ETFE films to tensile membrane structures. First of all, to investigate the possibility of application on tensile membrane structures, the stretch fabrication test is carried out, and it is verified that it is possible to increase the yield strength of the film membrane structures. After simulating the experiment also carries out an analytical investigation, and the effectiveness of the elasto-plastic analysis considering the viscous behavior of the film is investigated. Finally, post-aging tension measurement is conducted at the experimental facilities, and the viscosity behavior resulting from relaxation is investigated with respect to tensile membrane structures.

The Effect of Melamine Sulphonate High-Range Water Reducing Agent to the Fluidity of High-Flowability Paste (고유동페이스트의 유동특성에 미치는 멜라민계 고성능가수제의 영향)

  • Nam Ji-Hyun;Cho Eun-Young;Oh Sang-Gyun;Kim Jung-Kil
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2005.11a
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    • pp.71-74
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    • 2005
  • The viscosity of high-flowability paste is very high compared to normal concrete for the low water-binder ratio(W/B). Therefore, high-flowability concrete is positively necessary to high-range water reducing agent. High-Flowability paste can make much higher fluidity with no occurrence of segregation, by its higher viscosity and lower yield value than normal concrete. The flowability of high-flowability paste must be evaluated not only by convention consistency test such as slump test but also by the base of the rheological properties of the fresh concrete. The purpose of this study is to analyze the fluidity of high-flowability paste according to the addition ratio of the Melamine Sulphonate high-range water reducing agent.; high-flowability paste is considered as Bingham plastic fluid with the rheology parameters of the plaste viscosity and yield value.

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Rheological Property and Adjuvant Effect of l-Carrageenan (l-카라기난의 유동학적 성질과 어쥬번트 효과)

  • 김하형;김범수;이광재;이종혁;조두현;김윤중;정병욱
    • YAKHAK HOEJI
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    • v.46 no.1
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    • pp.6-10
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    • 2002
  • The present study investigated the rheological properties and adjuvant activity of IgG production of ι-Carrageenan prepared using two different methods . incubation at 37.4$^{\circ}C$ after either being heated or not being heated int 6$0^{\circ}C$ for 10 minutes. The carrageenan exhibited plastic flow with thixotropy in both cases, but the viscosity of the sample that had been heated was significantly higher. C57BL/6 mice were then immunized intraperitoneally with either of the carrageenans containing protein antigens. The maximum adjuvant effect was found when using the nonheated carrageenan, especially in term of IgG2a, IgG2b, and IgG3 production. In contrast, IgG1 antibody production was the same far both types of carrageenan. furthermore, when administered oral1y, neither type of carrageenan resulted in the production of any antibodies.

Three-Dimensional Finite Element Analysis for Compression Molding of Step-Type Random/Unidirectional Polymer Composite Laminates (단부형상을 갖는 무배향/일방향 복합적층판의 압축성형에 있어서 3차원 유한요소해석)

  • 송강석;채경철;김이곤
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 1999.11a
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    • pp.101-106
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    • 1999
  • Fiber reinforced plastic composites is widely used to make be lightening of aircraft and automotive owing to having high specific strength and specific modulus. And it is very important to know a charge shape in order to have good products in the compression molding. In particular, the product such as a bumper beam is composed of the random and unidirectional composite mats. Its deformation and charge shape are very different by stack type of random and unidirectional mats. In this paper, the characteristics of flow fronts such as a bulging phenomenon for step-type random/unidirectional composite mats and slip parameters are studied numerically. And the effects of viscosity ratio and stack type on the mold filling parameters are also discussed.

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Rheology Analysis of Cement Paste According to the Concentration of Borax Diluted Solution (붕사 희석액 농도에 따른 시멘트 페이스트의 레올로지적 분석)

  • Lee, Hyang-Sun;Lee, Yu-Jeong;Han, Dong-Yeop
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2019.05a
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    • pp.110-111
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    • 2019
  • Concrete with high thixotropy has a lower plastic viscosity when pour in, thus demonstrating fluidity, and After poured, the viscosity can be restored again to ensure stable progress without additional liquidity and material separation. Therefore, in this study, a basic study of thixotropy of concrete was proceeded through cross-linked bond of PVA and Borax. Therefore, it is judgment that the higher the concentration of boron solutions, the higher the strength of the interconnections between PVA and boron.

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Capillary Breakup of Viscoelastic Fluid and its Extensional Rheology (점탄성유체의 Capillary Breakup 가시화 및 신장유변물성 측정)

  • Jeon, Hyun Woo;Choi, Chan Hyuck;Kim, Byung Hoon;Park, Jinsoo
    • Journal of the Korean Society of Visualization
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    • v.19 no.1
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    • pp.81-87
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    • 2021
  • Extensional flow of viscoelastic fluids is widely utilized in various industrial processes such as electrospinning, 3D printing and plastic injection molding. Extensional rheological properties, such as apparent viscosity and relaxation time, play an important role in the design and evaluation of the viscoelastic fluid-involved processes. In this work, we propose a lab-built capillary breakup extensional rheometer (CaBER) based on flow image processing to investigate the capillary breakup of polyethylene oxide (PEO) solution and its extensional rheological properties. We found that the apparent extensional viscosity and extensional relaxation time of the PEO solution are independent of the strike time. The proposed CaBER is expected to be applied to characterization of the extensional rheological properties of viscoelastic fluids at low cost with high precision.

Experimental study on types of polycarboxylate superplasticizers and their on the rheological properties of the cement paste (폴리카본산계 고성능 감수제의 종류와 시멘트 페이스트의 레올로지 특성에 미치는 영향에 관한 실험적 연구)

  • Ko, Hye-Bin;Kong, Tae-Woong;Cho, In-Sung;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2020.11a
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    • pp.81-82
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    • 2020
  • Cement paste is the basic material constituting concrete and the most basic data of workability. This study quantitatively evaluated the measured data using a ring flow and a rotary viscometer to estimate the flow of cement paste, and also evaluated the flow and rheology over time. For this, the current work has studied admixtures that affect the fluidity of cement paste. As a result of the experiment, since fluidity and plastic viscosity are inversely proportional to each other, more experimental studies are needed to obtain high fluidity and high viscosity at the same time.

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Fabrication of Hot Embossing Plastic Stamps for Microstructures (마이크로 구조물 형성을 위한 핫 엠보싱용 플라스틱 스탬프 제작)

  • Cha Nam-Goo;Park Chang-Hwa;Lim Hyun-Woo;Park Jin-Goo;Jeong Jun-Ho;Lee Eung-Sug
    • Korean Journal of Materials Research
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    • v.15 no.9
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    • pp.589-593
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    • 2005
  • Nanoimprinting lithography (NIL) is known as a suitable technique for fabricating nano and micro structures of high definition. Hot embossing is one of NIL techniques and can imprint on thin films and bulk polymers. Key issues of hot embossing are time and expense needed to produce a stamp withstanding a high temperature and pressure. Fabrication of a metal stamp such as an electroplated nickel is cost intensive and time consuming. A ceramic stamp made by silicon is easy to break when the pressure is applied. In this paper, a plastic stamp using a high temperature epoxy was fabricated and tested. The plastic stamp was relatively inexpensive, rapid to produce and durable enough to withstanding multiple hot embossing cycles. The merits of low viscosity epoxy solutions were a fast degassing and a rapid filling the microstructures. The hot embossing process with plastic stamp was performed on PMMA substrates. The hot embossing was conducted at 12.6 bar, $120^{\circ}C$ and 10 minutes. An imprinted PMMA wafer was almost same value of the plastic stamp after 10 times embossing. Entire fabrication process from silicon master to plastic stamp was completed within 12 hours.