• Title/Summary/Keyword: Phase diagram

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Studies in Iron Manufacture Technology through Analysis of Iron Artifact in Han River Basin during the Proto-Three Kingdoms

  • Kim, Soo-Ki
    • Conservation and Restoration of Cultural Heritage
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    • v.1 no.1
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    • pp.9-22
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    • 2012
  • The most widely excavated iron artifacts used as weapons or farm tools from central southern regions of Korea were subjects of non-metallic inclusion analysis through metallographic examination, microhardness measurement, and scanning electron microscopy with energy dispersive X-ray spectroscopy. Through metallographic interpretation and study of the analyzed results, the steel manufacturing and iron smelting using heat processing in the iron artifacts excavated from the central southern region of the ancient Korean peninsula was studied, and the analysis of the non-metallic inclusions mixed within the metallic structures was interpreted as the ternary phase diagram of the oxide to infer the type of iron ores for the iron products and the temperature of the furnace used to smelt them. Most of the ancient forged iron artifacts showed $Al_2O_3/SiO_2$ with high $SiO_2$ contents and relatively low $Al_2O_3$ contents for iron ore, indicating t hat for $Al_2O_3$ below 5%, it is presumed that magnetic iron ores were reduced to bloom iron (sponge iron) with direct-reduction process for production. The temperature for extraction of wustite for $Al_2O_3$ below 1% was found to be $1,020{\sim}1,050^{\circ}C$. Considering the oxide ternary constitutional diagram of glassy inclusions, the steel-manufacturing temperature was presumed to have been near $1,150{\sim}1,280^{\circ}C$ in most cases, and minimum melting temperature of casting iron part excavated in Daeseong-ri. Gyeonggi was near $1,400^{\circ}C$, and it is thought that hypoeutectic cast iron of about 2.3% carbon was casted and fragility of cast iron was improved by decarburizing in solid state.

Recovery of Li from the Lithium Containing Waste Solution by D2EHPA (리튬함유 폐액으로부터 D2EHPA에 의한 리튬의 회수)

  • Ahn, Hyo-Jin;Ahn, Jae-Woo;Lee, Ki-Woong;Son, Hyun-Tae
    • Resources Recycling
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    • v.23 no.5
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    • pp.21-27
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    • 2014
  • A study on the solvent extraction for the recovery of Li from lithium-containing waste solution was investigated using $D_2EHPA$ as an extractant. The experimental parameters, such as the pH of the aqueous solution, concentration of extractant and phase ratio were observed. Experimental results showed that the extraction percentage of Li was increased with increasing the equilibrium pH. More than 50% of Li was extracted in eq. pH 6.0 by 20% $D_2EHPA$. From the analysis of McCabe-Thiele diagram, 95% of Li was extracted by four extraction stage at phase ratio(O/A) of 3.0. Stripping of Li from the loaded organic phases can be accomplished by sulfuric acid as a stripping reagent and 90 ~ 120 g/L of $H_2SO_4$ was effective for the stripping of Li. Finially, Li was concentrated about 11.85 g/L by continuous stripping process, and then lithium carbonate was prepared by precipitation method.

The Stipulation of Unity Painting Color Concept to Chinese Traditional Yin Yang and Five Elements Color

  • Wei, Na
    • International Journal of Advanced Culture Technology
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    • v.10 no.3
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    • pp.184-191
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    • 2022
  • Unity Painting is a concept that the researcher put forward to locate his own creative style in his creation. Unity Painting, with a clue of reflecting the characteristics of contemporary oriental visual culture, combines the contemporary painting features of a variety of western painting languages. It aims to link the painting system formed in the context of oriental culture with the world's contemporary art and try to present a new contemporary painting with oriental genes. According to the Chinese literature, the researcher sorted out the five main colors (五正色), ten colors for Heavenly Stems (十天干色彩), five intermediate colors (五间色), and five colors as the expression of the Chi of Thriving and Fading and the Chi of Birth and Death, and deduced the summary and stipulation of the color of yin-yang and five elements under the concept of Unity Painting. Based on this, the researcher drew the color-phase and its variation stipulation diagram of ten colors for Heavenly Stems, the orientation of Heavenly Stems (天干方位), color-phase variation diagram (色相变化图), as well as the stipulation system diagram of the five elements (五行), Heavenly Stems and Earthly Branches (干支), energy, time and colors. Through the research and collation of the literature, the researcher took the stipulated five elements color (五行色彩) as the basis of the color concept of creation to complete the work. This paper discusses how to find the starting point of contemporary art creation in the context of traditional oriental culture, sorts out the practical creation logic, and provides ideas for subsequent researchers, with a view to better establishing the identity of the creator and providing research significance and value in the context of the study of oriental art.

A Study Of The Current-Diagram Method For Calculating Induction Motor Characteristics With Adjustable Frequency (가변주파수에 있어서 유도전동기특성의 도시산정법에 관한 연구)

  • Min Ho Park
    • 전기의세계
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    • v.18 no.4
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    • pp.22-30
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    • 1969
  • The development of the frequency convertors using semiconductors devices makes it possible to control the speed of A.C. motors easily. It is now economically feasible to provide them with power at adjustble frequency using silicon-controlled rectifier (or thyristor) inverters. In such a case, in order to operate an induction motor efficiently over a wide speed range, it must be supplied from a variable frecuency source of which frequency is adjustable over the speep range of the motor. It is desired to observe the changes in characteristics as primary current, torque-speed of induction moter etc. at any optional frequncy. Although the charactheristies can be obtained by means of the conventional methods they require very complicated precedures of calcuations. The Current Diagram Method in this paper suggests a new approach to simpler calcuations of the characteristics, using the motor constants at reference frequency. The conclusions of this study are summarized as follows: (1) The equations of stator current at adjusted frequency were derived to construct graphical chart and the current circle required for the Current Diagrm Method. (2) The radius, center of the current circle and the vector locus, the basis for calculating the characteristics, at any desired frequency could be easily determined with the aid of both the derived graphical chart and current circle at reference frequency. (3) The method was shown to be applicable to the various types of 3-phase induction motors and also dealt with its application to the split-phase, condenser motors.

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Preparation of Regenerated Cellulose Fiber via Carbonation. I. Carbonation and Dissolution in an Aqueous NaOH Solution

  • Oh, Sang Youn;Yoo, Dong Il;Shin, Younsook;Lee, Wha Seop;Jo, Seong Mu
    • Fibers and Polymers
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    • v.3 no.1
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    • pp.1-7
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    • 2002
  • Cellulose carbonate was prepared by the reaction of cellulose pulp and $CO_2$ with treatment reagents, such as aqueous $Zncl_2$ (20-40 wt%) solution, acetone or ethyl acetate, at -5-$0^{\circ}C$ and 30-40 bar ($CO_2$) for 2 hr. Among the treatment reagents, ethyl acetate was the most effective. Cellulose carbonate was dissolved in 10% sodium hydroxide solution containing zinc oxide up to 3 wt% at -5-$0^{\circ}C$. Intrinsic viscosities of raw cellulose and cellulose carbonate were measured with an Ubbelohde viscometer using 0.5 M cupriethylenediamine hydroxide (cuen) as a solvent at $20^{\circ}C$ according to ASTM D1795 method. The molecular weight of cellulose was rarely changed by carbonation. Solubility of cellulose carbonate was tested by optical microscopic observation, UV absorbance and viscosity measurement. Phase diagram of cellulose carbonate was obtained by combining the results of solubility evaluation. Maximum concentration of cellulose carbonate for soluble zone was increased with increasing zinc oxide content. Cellulose carbonate solution in good soluble zone was transparent and showed the lowest absorbance and the highest viscosity. The cellulose carbonate and its solution were stable in refrigerator (-$5^{\circ}C$ and atmospheric pressure).

Improvement plan for Function Definition using CAFAT in the Construction VE (건설 VE에서 CAFAT을 이용한 기능정의 개선방안)

  • Choi, Chang-Hoon;Kim, Soo-Yong
    • Korean Journal of Construction Engineering and Management
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    • v.7 no.3 s.31
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    • pp.102-111
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    • 2006
  • In the analysis of function, which is the core and early phase among the procedure of construction VE Job Plan, the accuracy of function definition directly connects to VE result. However, the method of defining function, which is currently used is not accurate and comprehended or is difficult to utilize it systematically. Also, there is not a clear definition about the function for selecting VE so that many difficulties occur in the organic connection between each of functions in the summarization of function after defining function. Therefore, this study cleared the definition of function and made up any counter measured problem occurred in FAST Diagram later on and suggested CAFAT(Combined Antithetic Function Analysis Technique) in order to induce better phase in functional analysis.