• Title/Summary/Keyword: Phase and size control

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Study on Morphology Control of Polymeric Membrane with Clathrochelate Metal Complex (Clathrochelate계 금속 착물을 이용한 고분자 멤브레인 구조 제어)

  • Kim, Nowon;Jung, Boram
    • Membrane Journal
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    • v.24 no.6
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    • pp.472-483
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    • 2014
  • This study is preparation of microporous membranes by using macrocyclic metal ion complexes and extended cage complexes. It is a more favorable way to existing methods because polymer and metal ion-ligand complex system provides a fine control over the phase transition behavior. Chemical functionalization of the polar surface can be obtained. Metal-templated condensation of cyclohexanedione dioxime, hydroxyphenylboronic acid in the presence of metal salts proceeds cleanly in methanol to furnish the metal clathrochelate complexes. Organic/inorganic hybrid membranes were prepared with polyethersulfone (PES), polyvinylpyrrolidone (PVP), ethyleneglycol butyl ether (BE), metal clathrochelate s and DMF by using nonsolvent induced phase inversion method. The structure of membranes was characterized with scanning electron microscopy (SEM) and microflow permporometer. The addition of Fe(II) clathrochelate complex with p-hydroxyphenyl group leads to changes of membrane morphology such as narrow mean pore size distribution, increase of surface pore density and decrease of the largest pore size.

A Study on the Driving Circuit of Piezoelectric Ultrasonic Motor Using PLL Technique (PLL을 이용한 압전 초음파 모터의 구동회로에 관한 연구)

  • ;;Sergey Borodin
    • The Transactions of the Korean Institute of Electrical Engineers B
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    • v.52 no.1
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    • pp.33-38
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    • 2003
  • This paper describes control principles of the piezoelectric ultrasonic motor which is operated by the ultrasonic vibration generated by the piezoelectric element. The piezoelectric ultrasonic motor has excellent characteristics such as compact size, noiseless motion, low speed, high torque and controllability, and has been recently applied for the practical utilization in industrial, consumer, medical and automotive fields. In this paper, the design of two-phase push-pull inverter for driving the piezoelectric ultrasonic motor is described, and a new control method of automatic resonant frequency tracking using PLL(Phase-Locked Loop) technique is mainly presented. the experimental results by this inverter system for driving the piezoelectric ultrasonic motor are illustrated herein. The inverter system with PLL technique improved the speed stability of the piezoelectric ultrasonic motor.

A Study on Development of New 3-Phase Open-Phase Protector used in Distribution Panel (새로운 분전반용 3상 결상보호기 개발에 관한 연구)

  • Kwak, D.K.;Kim, J.H.;Park, Y.J.;Jung, D.Y.;Kim, D.K.;Kim, P.R.
    • Proceedings of the KIPE Conference
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    • 2012.07a
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    • pp.546-547
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    • 2012
  • In the three-phase power system using the three-phase load, when any one-phase is open-phase, the unbalanced current flows and the single-phase power supplied by power supply produces over-current. As a result, the enormous damage and electrical fire can be given to the power system. In order to improve these problems, this paper is proposed a new control circuit topology for open-phase protection using semiconductor devices. Therefore, the proposed open-phase protection device (OPPD) enhances the sensing speed and precision, and has the advantage of simple fitting in the three-phase distribution panel in the field, as it manufactures into small size and light weight. As a result, the proposed OPPD minimizes the electrical fire from open-phase, and contributes for the stable driving of the power system.

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Control of Grain Size on Friction Stir Welded AZ31 and AZ91 (AZ31과 AZ91의 마찰교반용접부 결정립 크기 제어)

  • Gwon, Gi-Su;Lee, Chang-U;Kim, Mok-Sun;Sato, Yutaka S.;Kim, Jeong-Han
    • Proceedings of the KWS Conference
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    • 2007.11a
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    • pp.328-331
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    • 2007
  • It was carried out to evaluate microstructure and mechanical properties of friction stir welded(FSW) on magnesium alloys. Two types magnesium alloy was used in this work, AZ31 wrought and AZ91 cast magnesium alloy. Microstructure near the weld zone showed general weld structures such as stir zone(SZ), thermo-mechanically affected zone(TMAZ) and heat affected zone(HAZ). In the AZ91 alloy, the SZ had a fine grain size and $\beta$ phase particles which were well distributed in matrix. It was characterized to redistribute by partial or full re-solution of the $\beta$ phase which is coarse in base metal during FSW processing. The hardness of the SZ slightly increase than the base metal in AZ31 Mg alloy.

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Numerical Analysis on the Collision Behaviors of in-flight Droplets During Gas Atomization (가스 분무 시 비행 액적의 충돌 현상에 관한 수치적 고찰)

  • Seok, Hyun Kwang
    • Korean Journal of Metals and Materials
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    • v.46 no.8
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    • pp.506-515
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    • 2008
  • Recently, it is exceedingly required to produce metal powders with tailored shape and phase altogether in order to fabricate high performance functional parts such as magnetic core or electro-magnetic noise suppressor for high frequency usage. Therefore, the collision phenomena of in-flight droplets against chamber wall or neighboring in-flight droplets each other is investigated by a computational method in order to get useful information about how to design the atomizing system and how to tailor process parameters not to make irregular-shaped powders during gas atomization process. As a results, smaller powders, lower melt temperature are known to be favorable for droplets not to collide against chamber wall. In additions, powders of narrower size distribution range, lower droplet generation rate, lower melt temperature, lower gas velocity are desirable to prevent droplet-collisions against neighboring in-flight droplets.

The Study on Improvement in Subcooling of TMA Clathrate for PCM in Ice Storage System (빙축열시스템 PCM용 TMA-포접화합물의 과냉도 개선에 대한 연구)

  • Kim, J.H.;Chung, N.K.;Kim, C.O.
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.1663-1666
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    • 2003
  • TMA clathrate that is used by PCM of ice storage system in this research creates hydrate crystallization at higher temperature than pure water, and application is expected as PCM because having comparative big dormant temperature without phase separation phenomenon. In case this research uses TMA clathrate by PCM, choose admixture by purpose to control or remove subcooling of TMA clathrate and evaluated experimentally. Subcooling is improved and can expect contraction of freezing machine running time and increase of coefficient of performance as that add admixture to TMA clathrate conclusively. Also, may supply thermal storage system that apply low temperature potential heat thermal storage material that subcooling is improved more extensively laying stress on medium size building and small size building, can expect allowance through localization of ice storage system.

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Preparation of Asymmetric Membranes by Addition of Nonsolvent (비용매 첨가제를 이용한 비대칭막의 제조)

  • Kim, Nowon
    • Membrane Journal
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    • v.25 no.1
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    • pp.32-41
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    • 2015
  • High performance polysulfone microfiltration membranes with a high were successfully prepared by vapor induced phase separation (VIPS) coupled with non-solvent induced phase separation (NIPS) process. Asymmetric Membranes were prepared with PSF/DMF/PVP/PEG/DMSO/water mixed solutions and water/IPA coagulant. PSF, DMF, PVP, PEG, DMSO, water was used as a membrane polymer, a solvent, a hydrophilic polymer additive, a polar protic liquid polymer, a polar aprotic nonsolvent, and a polar protic nonsolvent in the casting solution, respectively. The addition of polar aprotic nonsolvents, and polar protic nonsolvents is a convenient and effective method to control membrane structure. In order to control the morphology of polymeric membranes, the spontaneous emulsification induced by drawing water vapor into the exposed casting solution surface has been used. Control of the internal morphology of polymeric membranes by using mixed coagulation solution such as water and IPA is discussed in the present work. The pure water permeability, pore size distribution, surface hydrophilicity and membrane morphology were investigated. Due to the addition of DMSO to casting solution, the mean pore size increased almost $0.2{\mu}m$ and the water flux increased about 1000-1800 LMH.

Reduced Hybrid Ring Coupler Using Surface Micromachining Technology for 94-GHz MMIC Applications

  • Uhm, Won-Young;Beak, Tae-Jong;Ryu, Keun-Kwan;Kim, Sung-Chan
    • Journal of information and communication convergence engineering
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    • v.14 no.4
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    • pp.246-251
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    • 2016
  • In this study, we developed a reduced 94 GHz hybrid ring coupler on a GaAs substrate in order to demonstrate the possibility of the integration of various passive components and MMICs in the millimeter-wave range. To reduce the size of the hybrid ring coupler, we used multiple open stubs on the inside of the ring structure. The chip size of the reduced hybrid ring coupler with multiple open stubs was decreased by 62% compared with the area of the hybrid ring coupler without open stubs. Performance in terms of the loss, isolation, and phase difference characteristics exhibited no significant change after the use of the multiple open stubs on the inside of the ring structure. The reduced hybrid ring coupler showed excellent coupling loss of $3.87{\pm}0.33dB$ and transmission loss of $3.77{\pm}0.72dB$ in the measured frequency range of 90-100 GHz. The isolation and reflection were -48 dB and -32 dB at 94 GHz, respectively. The phase differences between two output ports were $180^{\circ}{\pm}1^{\circ}$ at 94 GHz.

The Grain Size Control of A356 Aluminum Alloy by Electromagnetic Stirring (수평식 전자교반을 이용한 A356 합금의 결정립 제어)

  • Ko J. H.;Seo P. K.;Choi W. S.;Kang C. G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.10a
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    • pp.111-114
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    • 2004
  • It is many devices to obtain the globular structure because the globularity of the structure is the key to the low apparent viscosity and also to good rheological properties. In this study, the morphology of the change of primary Al phase in A356 alloy by electro magnetic stirrer was investigated to obtain the globular structure. The parameters are the current, stirring time, pouring temperature individually. The greater current and longer stirring time was to get the finer the primary however in case of over the 80A of current and 60sec of stirring time, the primary Al was merged together and was increased. The effect of pouring temperature has an important effect on the size of primary phase. About the $675^{\circ}C$, the primary Al was very fined.

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The Effect of Rheology Flow with Grain Size Controlled Material on Solid Particles Behavior (결정립 제어 소재의 레오로지 유동이 고상입자의 거동에 미치는 영향)

  • Jung Y. S.;Seo P. K.;Kang C. G.
    • Transactions of Materials Processing
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    • v.14 no.4 s.76
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    • pp.351-359
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    • 2005
  • The semi-solid processing is now becoming of great interest for the production of various parts by pressure die casting. Also, the rheo-casting has been substituted for thixo-casting, because the rheo-casting can control the solid particles to globular and non-dendritic solid phase. In the rheo-casting process, the important thing is to control the solid particles behavior in semi-solid materials. So in this paper, to control solid particles behavior in semi-solid materials, we experimented about the die filling tests during the semi-solid die casting in 0.3, 0.4, 0.5 and 0, 6 solid fraction. The die filling in semi-solid die casting were simulated by MAGMA soft/thixo module. By the die filling tests and computer simulation, the effect of solid particles behavior in rheology flow had been investigated.