• Title/Summary/Keyword: Phase and size control

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Effect of sintering programs and surface treatments on monolithic zirconia

  • Seren Nur Dokuzlu ;Meryem Gulce Subasi
    • The Journal of Advanced Prosthodontics
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    • v.16 no.1
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    • pp.25-37
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    • 2024
  • PURPOSE. To investigate the effect of sintering programs and surface treatments on surface properties, phase transformation and flexural strength of monolithic zirconia. MATERIALS AND METHODS. Zirconia specimens were sintered using three distinct sintering programs [classic (C), speed (S), and superspeed (SS)] (n = 56, each). One sample from each group underwent scanning electron microscopy (SEM) and grain size analysis following sintering. Remaining samples were divided into five subgroups (n = 11) based on the surface treatments: control (CL), polish (P), glaze (G), grind + polish (GP), and grind + glaze (GG). One sample from each subgroup underwent SEM analysis. Remaining samples were thermally aged. Monoclinic phase volume, surface roughness, and three-point flexural strength were measured. Monoclinic phase volume and surface roughness were analyzed by Kruskal-Wallis and Dunn tests. Flexural strength was analyzed by two-way ANOVA and Weibull analysis. The relationships among the groups were analyzed using Spearman's correlation analysis. RESULTS. Sintering program, surface treatment, and sintering × surface treatment (P ≤ .010) affected the monoclinic phase volume, whereas the type of surface treatment and sintering × surface treatment affected the surface roughness (P < .001). Type of sintering program or surface treatment did not affect the flexural strength. Weibull analysis revealed no significant differences between the m and σo values. Monoclinic phase volume was positively correlated with surface roughness in the SGG and SSP groups. CONCLUSION. After sintering monolithic zirconia in each of the three sintering programs, each of the surface treatments can be used. However, for surface quality and aging resistance, G or GG can be recommended as a surface finishing method.

Low-cost Single-Phase Half-bridge Active Power Filter with One Current Sensor (단일 전류센서를 갖는 저가의 단상 반브릿지 능동전력필터)

  • 김희중;한병문;박용식
    • The Transactions of the Korean Institute of Power Electronics
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    • v.4 no.4
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    • pp.342-348
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    • 1999
  • This paper describes a low-cost single-phase active power filter, which consists of a half-bridge P\A미1 inverter with a s simple control circuit. In order to verify the performance of proposed active power filter, many computer simulations w with EMTP codes and experimental works with a hardware prototype were done. Both results confirm that the p proposed active power filter shows excellent performance to eliminate the harmonics generated in the single-phase non l linear‘ load. The active power filter has advantage of low implementation cost and compact size. using a half-bridge i inverter and a simple control circuit with only one current sensor. So. it can be fabricated as a plug-in type.

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EFFECTS OF HEAT TREATMENTS ON MICROSTRUCTURES AND MECHANICAL PROPERTIES OF DUAL PHASE ODS STEELS FOR HIGH TEMPERATURE STRENGTH

  • Noh, Sanghoon;Choi, Byoung-Kwon;Han, Chang-Hee;Kang, Suk Hoon;Jang, Jinsung;Jeong, Yong-Hwan;Kim, Tae Kyu
    • Nuclear Engineering and Technology
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    • v.45 no.6
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    • pp.821-826
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    • 2013
  • In the present study, the effects of various heat treatments on the microstructure and mechanical properties of dual phase ODS steels were investigated to enhance the high strength at elevated temperature. Dual phase ODS steels have been designed by the control of ferrite and austenite formers, i.e., Cr, W and Ni, C in Fe-based alloys. The ODS steels were fabricated by mechanical alloying and a hot isostatic pressing process. Heat treatments, including hot rolling-tempering and normalizing-tempering with air- and furnace-cooling, were carefully carried out. It was revealed that the grain size and oxide distributions of the ODS steels can be changed by heat treatment, which significantly affected the strengths at elevated temperature. Therefore, the high temperature strength of dual phase ODS steel can be enhanced by a proper heat treatment process with a good combination of ferrite grains, nano-oxide particles, and grain boundary sliding.

Effect of Mo Addition on the Sinterability and Mechanical Properties of TiB$_2$-Fe Cermets (TiB$_2$-Fe 서메트의 소결성 및 기계적성질에 미치는 Mo첨가의 영향)

  • 최덕순
    • Journal of the Korean Ceramic Society
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    • v.36 no.5
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    • pp.471-477
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    • 1999
  • Fe and Fe-Mo binder were used to produce TiB2 based cermet by a pressureless sintering. The densification behaviour of TiB2-Fe-Mo cermet during liquid-phase sintering in argon was studied in relation to binder phase charactertics. The effects of Mo addition and sintering condition on the sintering behaviour and mechanical properties were also investigated. TiB2-based cermets with Fe-Mo binder composition showed a better sinterability than the cermets with only Fe binder. In TiB2-Fe-Mo cermet higher densities in the wide temperature range were obtained and also fully densified sintered cermet were obtained at 1873K The enhancement in the densification phenomenon of TiB2-Fe-Mo system can be explained by improved liquid phase wettability associated with the roles of Mo components as solute atoms. When Fe-Mo binders were used cermets with a finer grain size and enhanced mechanical properties wereproduced and new phases such as Fe2B and Mo2FeB2 were observed in the sintered cermet. The highest bending strength was obtained from the 20vol% Fe-Mo cermet and these hardness-fracture toughness combination in the wide binder compositions is better than that of TiB2-Fe cermet. In order to improve mechanical properties microstructure control with high purity powders is desirable because high purity powders prevent the formation of Fe2B and Mo2FeB2 phase which comsume the ductile binder phase.

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A Single-Phase Active Power Filter Control with Load Current Estimation Method (부하전류 추정기법에 의한 단상능동전력필터 제어)

  • 곽상신;이무영;최연호;임성운;권우현
    • The Transactions of the Korean Institute of Power Electronics
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    • v.5 no.4
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    • pp.335-342
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    • 2000
  • A new control method for a single-phase active power filter, based on a load current estimation using a DC capacitor voltage of active power filter without sensing nonlinear load current, is proposed in this paper. Because the method proposed can remove the load current sensor in comparison with a conventional method sensing the load current and DC capacitor voltage together, it can make the active power filter easy installation, low cost, small size with no performance detriment. In addition, sample-hold technique and proportional control method is adopted to control the DC capacitor voltage and as no delay element such as LPF or PI control in the conventional method is used, the transient response is fast and good. Operation of a single-phase active power filter which consist of eight mode is explained according to utility voltage, compensation current and switch state, and compensation characteristics of active power filter using proposed method is verified by experiment.

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An Effective Control Scheme for Battery Charger System in Electric Vehicles

  • Nguyen, Cong-Long;Lee, Hong-Hee
    • Proceedings of the KIPE Conference
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    • 2012.07a
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    • pp.232-233
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    • 2012
  • This paper presents an effective control scheme for an electric vehicle battery charger where a symmetrical bridgeless power factor-corrected converter and a buck converter are cascaded. Both converters have been popular in industries because of their high efficiency, low cost, and compact size, hence combining these converters makes the overall battery charging system strongly efficient. Moreover, this charger topology can operate at universal input voltage and attain a desired battery current and voltage without ripple. In order to achieve a unity input power factor and zero input current harmonic distortion, the proposed control scheme adopts duty ratio feed-forward control technique in both current and voltage control loop. Additionally, in the current loop, its reference is created by a phase-locked loop (PLL) block, leading to a pure sinusoidal input current although the input voltage waveform is being distorted. The feasibility and practical value of the proposed approach are verified by simulation and experiment with an 110V/60Hz ac line input and 1.5kW-72V dc output of the battery charging system.

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Static bending study of AFG nanobeam using local stress-and strain-driven nonlocal integral models

  • Yuan Tang;Hai Qing
    • Advances in nano research
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    • v.16 no.3
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    • pp.265-272
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    • 2024
  • In this paper, the problem of static bending of axially functionally graded (AFG) nanobeam is formulated with the local stress(Lσ)- and strain-driven(εD) two-phase local/nonlocal integral models (TPNIMs). The novelty of the present study aims to compare the size-effects of nonlocal integral models on bending deflections of AFG Euler-Bernoulli nano-beams. The integral relation between strain and nonlocal stress components based on two types nonlocal integral models is transformed unitedly and equivalently into differential form with constitutive boundary conditions. Purely LσD- and εD-NIMs would lead to ill-posed mathematical formulation, and Purely εD- and LσD-nonlocal differential models (NDM) may result in inconsistent size-dependent bending responses. The general differential quadrature method is applied to obtain the numerical results for bending deflection and moment of AFG nanobeam subjected to different boundary and loading conditions. The influence of AFG index, nonlocal models, and nonlocal parameters on the bending deflections of AFG Euler-Bernoulli nanobeams is investigated numerically. A consistent softening effects can be obtained for both LσD- and εD-TPNIMs. The results from current work may provide useful guidelines for designing and optimizing AFG Euler-Bernoulli beam based nano instruments.

Morphological control and electrostatic deposition of silver nanoparticles produced by condensation-evaporation method (증발-응축법에 의해 발생된 은(silver) 나노입자의 구조제어 및 전기적 부착 특성 연구)

  • Kim, Whidong;Ahn, Ji Young;Kim, Soo Hyung
    • Particle and aerosol research
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    • v.5 no.2
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    • pp.83-90
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    • 2009
  • This paper describes a condensation-evaporation method (CEM) to produce size-controlled spherical silver nanoparticles by perturbing coagulation and coalescence processes in the gas phase. Polydisperse silver nanoparticles generated by the CEM were first introduced into a differential mobility analyzer (DMA) to select a group of silver nanoparticles with same electrical mobility, which also enables to make a group of nanoparticles with elongated structures and same projected area. These silver nanoparticles selected by the DMA were then in-situ sintered at ${\sim}600^{\circ}C$, and then they were observed to turn into spherical shaped nanoparticles by the rapid coalescence process. With the assistance of modified converging-typed quartz reactor, we can also produce the 10 times higher number concentration of silver nanoparticles compared with a general quartz reactor with uniform diameter. Finally, the spherical silver nanoparticles with 30 nm were electrostatically deposited on the surface of silicon substrate with the coverage rate of ~4%/hr. This useful preparation method of size-controlled monodisperse silver nanoparticles developed in this work can be applied to the various studies for characterizing the physical, chemical, optical, and biological properties of nanoparticles as a function of their size.

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Compliance Control of DD Manipulator using Ultrasonic Motor (초음파 모터를 사용한 DD 매니퓰레이터의 컴플라이언스 제어)

  • Kim, Dong-Ok;Sin, Duck;Kim, Won-Bae;Sung, Do-Saing;Kim, Young-Dong
    • Proceedings of the KIPE Conference
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    • 1996.06a
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    • pp.47-51
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    • 1996
  • In this paper, we propose a method for compliance control of a SCARA type 2-freedom direct drive(DD) manipulator. Each joint of the manipulator is driven by a travelling ultrasonic motor(USM). The travelling USM has good some characteristics over conventional servo motors such as compact size, light weight, silent motion, high torque and high speed response. By controlling the elasticity and viscosity of robot joints, a robot can work in compliance with external environment. we control the elastic coefficient and the viscous coefficient of joint by adjusting the phase difference of the motor power. And we contemplate transient response of USM with adjusting the elastic coefficient and the viscous coefficient. To use the result, we can control the robot to reach its goal with compliance motion. It remains for further research to develop the impedance control of USM.

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Effects of the Variables related to the Health Action Process Approach Model on Physical Activity: A Systematic Literature Review and Meta-analysis (신체활동에 대한 건강행동과정접근모델(Health Action Process Approach Model) 관련 변인의 효과: 체계적 문헌고찰 및 메타분석)

  • Choi, Yun;Yang, Sook Ja;Song, Hye Young
    • Research in Community and Public Health Nursing
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    • v.29 no.3
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    • pp.359-370
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    • 2018
  • Purpose: The purpose of this study is to identify effects of the variables of Health Action Process Approach (HAPA) Model on physical activity. Methods: This study has conducted a systematic literature review and meta-analysis. Sixteen articles were searched through electronic databases (PsycINFO, PubMed, CINAHL, Web of science, Science Direct, RISS, KMBASE, KoreaMed, KISS, DBpia) and additional journals from 2000 to July, 2017. To estimate the effect size (ES), the meta-analysis of the studies was performed by using Comprehensive Meta-Analysis programs. Results: The overall effect size of the variables of HAPA on physical activity was median (ES=.28). Of the core variables of HAPA model, action control (ES=.43) showed the largest effect size, followed by coping self-efficacy (ES=.31) and planning (ES=.31).Additional variables were identified as preparatory behavior (ES=.39) and past physical activity (ES=.24). Through the moderator effect analysis, the effect size was higher in the volitional phase than in the motivational phase, and higher in the healthy group than in the patient group. The higher the proportion of males and the lower the age, the larger the effect size. Conclusion: This finding shows empirical evidence that all core variables of the HAPA model are useful for predicting physical activity. We propose the use of the HAPA model to develop physical activity promotion intervention.