• Journal of the Korean Wood Science and Technology
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• v.46 no.5
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• pp.511-526
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• 2018

Effects of heat treatment on the characteristics of Royal paulownia (Paulownia tometosa) wood were investigated. The results were compared with those of Suwon silver poplar (Populus tementiglandulosa) and Korean red pine (Pinus densiflora) woods. The wood samples of the three species were treated at $160^{\circ}C$, $180^{\circ}C$, $200^{\circ}C$ and $220^{\circ}C$ in an electric furnace for 2 hours. The changes of color, density, mass loss, and relative crystallinity were investigated before and after heat treatment. The lightness ($L^*$) decreased rapidly from $200^{\circ}C$ in all species. There were no change in red-green chromaticity($a^*$) and yellow-blue chromaticity($b^*$) of Royal paulownia and poplar woods with increasing temperature. Whereas, yellow-blue chromaticity($b^*$) of Korean red pine wood decreased sharply from $200^{\circ}C$. Royal paulownia wood showed appreciable color change(${\Delta}E^*$) after heat treatment above $180^{\circ}C$. Poplar and pine woods, however, presented significant color change from $160^{\circ}C$. Color change of the three wood species increased rapidly with increasing temperature. Mass loss of the three wood species by heat treatment was the highest in the Royal paulownia wood and the lowest in the pine wood. Mass loss and relative crystallinity increased and density decreased slightly with increasing temperature. Consequently, it is revealed that Royal paulownia wood showed considerable differences in the temperature of color change, weight loss and change of relative crystallinity compared to the other wood species.

• Journal of the Korean Wood Science and Technology
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• v.19 no.1
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• pp.71-80
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• 1991

This study was carried out to investigate replaceable species with the conventional sounding board sitka spruce. by comparing the dynamic properties such as density, dynamic Young's modulus and internal friction Dynamic Young's modulus. internal friction of longitudinal and radial direction measured in free mass-free boundary condition for facile vibration analysis and measured by forced vibration method. Dynamical properties of four species were measured on squared plate specimen that the four edges were hung vertically by threads and driven magnetically through an iron piece glued on the specimen, by the use of condenser microphone as vibration transducer, and analyzed by FFT analyzer. The results obtained were as follows: 1. Chaldni method using aluminum powder was proper to identify the vibration mode in the plate vibration and it was possible to verify the resornance mode. 2. It was considered that it was necessary to investigate the influence of adhesive part on the plate vibration when the sounding board was made by two or three small board adhesion. 3. It was considered that plate vibration method, which was a superior to the vibration test of beam, was suitable for selecting suounding board because dynamic Young's modulus and internal friction show different order according to longitudinal and radial direction. 4. Paulownia tomentosa Thunb.) Steudel has been considered to be replaceable species with sitka spruce because it has high dynamic Young's modulus compared with low density, low internal friction, and K value of Paulownia tomentosa (Thunb.) Steudel is greater than that of sitka spruce.

• Journal of Conservation Science
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• v.24
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• pp.75-83
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• 2008

In order to assess antifungal activity of a wooden storage box, which was made of Paulownia tomentosa and used for keeping ancient documents, antifungal activity of volatile organic compounds emitted from the box was investigated along with qualitative analysis on major substances of the compounds. After collecting floating microorganisms inside air tester, the fungal activity was assessed by counting the number of colonies growing on TSA media. Compared to the control which collected 85 colonies from outdoor, 72 colonies were observed showing reduction rate of 14.82%. Through GC/MS and TDS system analysis, limonene was detected from the volatile organic compounds as characteristic features. When the fungal activity was assessed through fumigation by adding natural biocide BI and BII containing eugenol and anethole as major substances, both biocides showed a strong fungal activity with respectively 92.6%(inside the box) and 99.9%(outdoor) of reduction rate. Although these results didn't clarify antifungal activity of the volatile organic compounds emitted from the Paulownia-wood storage box and their functional components, it was at least confirmed that there is application possibility of natural biocide to use for preservation of ancient documents with increased efficiency in controlling pests of wooden storage boxes.

• Journal of the Korean Wood Science and Technology
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• v.44 no.5
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• pp.760-766
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• 2016

This study explored the effects of heating temperature and laminae thicknesses on the time required to heat the center of air-dried Paulownia tomentosa, Pinus sp., Abies sp., and Larix sp. laminae to $56^{\circ}C$, which is a minimum core temperature of wood packaging materials defined by ISPM 15 standard, and maintain for 30 minutes in dry heat treatment schedule. Heating times were different among wood species and were Pinus sp. ${\geq}$ Abies sp. > Paulownia tomentosa > Larix sp. in decreasing order. The differences in heating times of some species were significantly different statistically, but were not different enough in practical terms to warrant heating four species separately. Heating times decreased as heating temperature increased and followed approximately power-function relationship. Also, heating times increased linearly with increasing laminae thickness. These relationships make it possible to calculate intermediate heating times relative to experimentally observed heating times. The results of this study will serve as a guideline for heat sterilization of Chinese laminae species to meet heat treatment requirements for protection against invasive pests.

• Journal of the Korean Wood Science and Technology
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• v.47 no.3
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• pp.299-310
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• 2019

This study was carried out to investigate the effect of heat-treatment and particle size on the crystalline properties of the wood cellulose. The color of wood flours was changed from light yellow in control sample to dark yellow or deep brown by heat treatment at $100^{\circ}C$ to $200^{\circ}C$. Relative crystallinity of the heat treated wood cellulose decreased with decreasing particle size from wood chips to 200 mesh, and there was little change in the crystal width. As the temperature was increased, relative crystallinity of the wood increased and crystal width was not changed. As a result of the FT-IR analysis, it was confirmed that the peaks were gradually decreased at -OH elongation as the heat-treated temperature was increased. The lignin C-H bending of $1425cm^{-1}$ and the hemicellulose C-H bending of $1370cm^{-1}$ did not change with the increase of the heat treatment temperature. In addition, it was revealed that C-C stretching of carbohydrate near $1031cm^{-1}$ decreased with increasing heat treatment temperature. Consequently, it is suggested that particle size and heat treatment affected the crystalline properties of wood cellulose.

• Journal of the Korean Wood Science and Technology
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• v.30 no.2
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• pp.87-94
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• 2002

This study was carried out to evaluate bending property on principal domestic species such as sargent cherry(Prunus sargentii), bitter wood(Picrasma quassioides), horn beam(Carpinus laxiflora), cork oak(Quercus variabilis), birch(Betula schmidtii), painted maple(Acer mono), basswood(Tilia amurensis), red pine(Pinus densiflora), pitch pine(Pinus rigtda), royal pawlonia(Paulownia tomentosa) by microwave heating. In this study, radius of curvature(ROC) for bending process was classified by radius of curvature(ROC) of bending plate such as 4 cm, 6 cm, and 10 cm, and thickness of metal-strap(TMS) was 0.6 mm and 0.8 mm. Bending process was successfully operated for 100 percent in bitter wood, horn beam, birch and painted maple. On the other hand, there was a success rate of 58 percent in sargent cherry and 83 percent in cork oak and 29 percent in basswood and 8 percent in royal pawlonia which is the worst bending property. All specimens of basswood and royal pawlonia were broken at 4 cm of ROC. Success rate of bending property was shown 44 percent in red pine and 56 percent in pitch pine. TMS has an effect on only drying speed in drying process than difficulty and facility of bending property. It was considered that the thinner TMS in drying process is the faster in drying speed of bent wood.

• Journal of the Korean Wood Science and Technology
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• v.35 no.1
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• pp.17-26
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• 2007

This study was conducted to investigate the effects of End-coating (CO) treatment and Vapor-dam (V) treatment on the air circulating oven drying characteristics of green stock (Paulownia tomentosa) for drum. The reduction of the weight of specimens was greatly displayed in order of control (C-NC) treatment, End-coating (C-CO) treatment, Vapor-dam (V-NC) treatment and Vapor-dam/End-coating (V-CO) treatment after the beginning of drying. The V-CO treated specimen showed smoother temperature gradient compared with the V-NC treated specimen throughout whole drying stage and there was little temperature gradient between the inner and outer part of the cylindrical stock. The C-CO treated specimen showed higher value of vapor pressure in both the inner and outer part of the cylindrical stock until the middle stage of drying, while after the middle stage of drying only the inner part of the cylindrical stock presented higher value compared with the C-NC treated specimen. The distribution of the absolute vapor pressure of the V-CO treated specimen was similar to that of the V-NC treated specimen during the initial stage of drying. However, the former showed a large distribution in order of the hollow, the outer part, the inner part of the cylindrical stock after the initial stage of drying, which was entirely different model of distribution from that of the V-NC treated specimen. Surface checks and ring failures were not observed for all of the specimens, while end checks were severely occurred for the C-NC treated specimen and the V-NC treated specimen.