• 한국표면공학회지
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• 제29권6호
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• pp.857-861
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• 1996

The influence of rf-plasma operation on the thin film formation containing small particles for Al-Li alloys mainly have been studied as a function of Ar gas pressure and plasma power by means of a 200kV transmission electron microscope (TEM). Under the non-plasma operation, the transition from continuous thin films to clusters of grape-like small particles occurred at Ar gas pressures above 20Pa. Particles were single crystals with clear crystal habit planes. Under the plasma operation, the influence of gas pressures on the film formation at a plasma power of 5W was also examined. Thin films containing particles below 30Pa and the films containing mainly particles above 40Pa were formed. The prominent change of the average particle size was not recognized. The increase of the plasma powers at 20Pa, which formed particles under non-plasma, suppressed growth of particles, and homogeneous films containing very small particles were fabricated. The electric conductivity showed slight decrease with an increase of plasma power.

• 펄프종이기술
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• 제36권2호
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• pp.33-38
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• 2004

Toner particles used in laser and xerographic printing process is fused on paper surface so strongly that they tend not to detach easily from the recylced paper surface during pulping. Furthermore, the removal efficiency of detached toner particles by conventional screening and flotation process has limitation due to the platy shape and large size of detached toner particles. It has been shown that the removal efficiency of toners in the screening process can be increased by agglomerating the toner particles with fatty alcohol. It is not possible, however, to remove small and platy toner particles by screening process. These small and platy toner particles should be removed by flotation process. In this study the effect of fatty alcohol that used for toner agglomeration on flotation efficiency has been examined. It was shown that flotation efficiency decreased when fatty alcohol was used most probably due to its effect of reducing hydrophobicity of toner particles.

• 한국신재생에너지학회:학술대회논문집
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• 한국신재생에너지학회 2009년도 추계학술대회 논문집
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• pp.305-305
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• 2009

The carbon nano-structured materials could be applied to the fields of advanced fillers, templates, electrode materials, sensor, storage, and absorption materials. The polyacrylonitrile (PAN) based carbon nano-particles provide the remarkable properties of high specific surface area, large pore volume, chemical inertness, and good mechanical stability. In this study, well-defined carbon nano-particles were obtained through pyrolysis of polyacrylonitrile based particles. The precursor nano-particles were prepared by modified aqueous dispersion polymerization using hydrophilic poly(vinyl alcohol) in a water/ N,N-dimethylformamide mixture media. Synthesized precursor nanoparticles have relatively monodisperse particles ranging 80 ~ 250nm. Stable spherical particles are obtained without coagulum or secondary particles in our system. The characteristic of the carbon nanoparticles were investigated in terms of surface area, morphology, and size distribution.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2009년도 9th International Meeting on Information Display
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• pp.1220-1223
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• 2009

The effect of silver (Ag) nano-particles on OLEDs was investigated by using a finite difference time domain (FDTD) tool. The proposed OLEDs employed Ag nanoparticles thermally deposited in a high vacuum on a cathode. The emission rate of the exciton was improved by 1.8 fold compared to the conventional OLEDs without Ag nano-particles. Less spacing between the dipole source and the Ag nano-particles resulted in a larger emission rate of the exciton in the OLED with nano-particles. The size of the Ag nano-particles was proportional to the emission rate of the exciton in a range of nano-meter scale of nano-particles. The enhancement of the emission rate of the exciton due to Ag nano-particles caused the improvement in the efficiency of the proposed OLED.

• Journal of Magnetics
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• 제20권1호
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• pp.21-25
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• 2015

Fine Nd-Fe-B-type particles were prepared by ball milling of different types of Nd-Fe-B precursor materials, such as die-upset magnet, HDDR-treated material, and sintered magnets. Coercivity dependence on the grain and particle size of the powder was investigated. Coercivity of the milled particles was reduced as the particle size decreased, and the extent of coercivity loss was dependent upon the precursor material. Coercivity loss in the finely milled particles was attributed to the surface oxidation. The extent of coercivity loss in the fine particles was closely linked to grain size of the precursor materials. Coercivity loss was more profound for the fine particles with larger grain size. Contrary to the fine particles from the sintered magnets with larger grain size the fine particles (~10 um) from the die-upset magnet and HDDR-treated material with much finer grain size still retained high coercivity (> 10 kOe for die-upset magnet, > 4 kOe for HDDR-treated material).

• Asian Journal of Atmospheric Environment
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• 제6권2호
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• pp.83-95
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• 2012

China has been a top producer and exporter of refined lead products in the world since the year 2000. After the phasing-out of leaded gasoline in the late 1990s, non-ferrous metallurgy and coal combustion have been identified as potential major sources of aerosol lead in China. This paper presents the single particle analytical results of ambient aerosol particles collected near a lead smelter using a scanning electron microscopy- energy dispersive x-ray spectroscopy (SEM-EDX). Aerosol particle samples were collected over a 24-hour period, starting from 8 pm on 31 May 2002, using a high volume TSP sampler. For this near source sample, 73 particles among 377 particles analyzed (accounting for 19.4%) were lead-containing particles mixed with other species (S, Cl, K, Ca, and/or C), which probably appeared to be from a nearby lead smelter. Lead-containing particles of less than $2{\mu}m$ size in the near source sample were most frequently encountered with the relative abundances of 42%. SEM-EDX analysis of individual standard particles, such as PbO, PbS, $PbSO_4$, $PbCl_2$, and $PbCO_3$, was also performed to assist in the clear identification of lead-containing aerosol particles. Lead-containing particles were frequently associated with arsenic and zinc, indicating that the smelter had emitted those species during the non-ferrous metallurgical process. The frequently encountered particles following the lead-containing particles were mineral dust particles, such as aluminosilicates (denoted as AlSi), $SiO_2$, and $CaCO_3$. Nitrate- and sulfate-containing particles were encountered frequently in $2-4{\mu}m$ size range, and existed mostly in the forms of $Ca(NO_3,SO_4)/C$, $(Mg,Ca)SO_4/C$, and $AlSi+(NO_3,SO_4)$. Particles containing metals (e.g., Fe, Cu, and As) in this near source sample had relative abundances of approximately 10%. Although the airborne particles collected near the lead smelter contained elevated levels of lead, other types of particles, such as $CaCO_3$-containing, carbonaceous, metal-containing, nitrates, sulfates, and fly-ash particles, showed the unique signatures of samples influenced by emissions from the lead smelter.

• International Journal of Aeronautical and Space Sciences
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• 제16권2호
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• pp.247-253
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• 2015

The components of an aero-engine gas path cannot be monitored in a timely way due to a lack of real-time monitoring technologies. As an attempt to address this problem, we have conducted research on a condition monitoring technology based on the charging characteristics of particles in an aero-engine gas path, and emphatically analyze the formation of particles in an aero-engine gas path, the charging mechanism of carbon particles and the factors that influence the charge quantity and polarity. The verification experiments are performed on the simulated experiment platform and a turbo-shaft engine test bench. The results show the carbon particles' carry charge, and an obvious change in the total electrostatic charge level in the aero-engine gas path due to the increased carbon particles produced by burning or abnormal metal particles; the charge number is related to the size of particles, and the bigger carbon particles carry a negative charge and metal particles carry a positive charge; the change in engine power can lead to an obvious change in the level of electrostatic charge in the gas path, and the change in electrostatic charge results from the extra carbon particles formed in the rich-oil burning process. The research provides a reference for establishing the baseline of electrostatic charge while the engine runs on different power. The study also demonstrates the validity of the electrostatic monitoring technology and establishes a base for developing the application of electrostatic monitoring technology in aero-engines.

• 한국대기환경학회지
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• 제12권3호
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• pp.289-296
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• 1996

Effects of crustal species on the characteristics of ambient particles were studied by applying a gas-particle equilibrium model, SCAPE, to the measurements at Kosan, Cheju Island during the spring and summer, 1994. Two cases were simulated; the measured composition was used without any modification (case 1), and the metal ion concentrations originated from crust were subtracted from the measured particle composition (case 2). Total suspended particles (TSPs) were collected by an automatic high volume tape sampler during spring period and by high volume samplers during summer period. The fine particles, PM 2.5, and gaseous volatile species were collected using a filter pack smapler during summer period. The water soluble ion concentrations were analyzed from all the particle samples. According to the simulation results, the effect of crustal elements on the chemical composition of particles is negligible for both TSP particles and PM 2.5 particles. Acidity of particles measured at Kosan, however, is affected by the change of the concentrations of crustal species, stronger effects for TSP particles than for PM 2.5 particles during summer, and stronger effects during summer than spring for TSP particle. The average pH decrease due to the absence of crustal species was about 0.10 for PM 2.5 particle during summer and 1.51 and 0.85 for TSP particles during summer spring, respectively. Water contents of PM 2.5 particles for both cases are comparable to each other. Estimated water content of TSP particles for case 2 is higher than that for case 1 by about 4 $\sim 6 \mum/m^3$ because salts of metal ions are not hygroscopic.

• 천문학회보
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• 제42권2호
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• pp.48.3-49
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• 2017

Interplanetary space of the solar system contains a large number of dust particles, referred to as Interplanetary Dust Particles (IDPs) cloud complex. They are observable through meteors and zodiacal lights. The relative contribution of possible sources to the IDPs cloud complex was an controversial topic, however, recent research (Yang & Ishiguro, 2015 and references therein) suggested a dominance of cometary origin. In this study, we numerically investigated the orbital evolution of cometary dust particles, with special concerns on different evolutionary tracks and its consequences according to initial orbits, size and particle shape. The effect of dust particle density and initial size-frequency distribution (SFD) were not decisive in total cloud complex mass and mass supply rate, when these physical quantities are confined by observed zodiacal light brightness and dust particle SFD at 1 au. We noticed that, if we assume the existence of fluffy aggregates discovered in the Earth's stratosphere and the coma of 67P/Churyumov-Gerasimenko, the required mass supply rate decreases significantly. We also found out that close encounters with planets (mostly Jupiter) are the dominating factor of the orbital evolution of dust particles, as the result, the lifetime of cometary dust particles are shorter than Poynting-Robertson lifetime (around 250 thousand years). As another consequence of severe close encounters, only a small fraction of cometary dust particles can be transferred into the orbit < 1 au. This effect is significant for large size particles of ${\beta}$ < 0.01. The exceptional cases are dust particles ejected from 2P/Encke and active asteroids. Because they rarely encounter with Jupiter, most dust particles ejected from those objects are governed by Poynting-Robertson effect and well transferred into the orbits of small semimajor axis. In consideration of the above effects, we directly estimated probability of mutual collisions between dust particles and concluded that mutual collisions in the IDPs cloud complex is mostly ignorable, except for the case of large sized particles from active asteroids.

• Asian Journal of Atmospheric Environment
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• 제6권4호
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• pp.275-280
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• 2012

To understand the effect of aerosols on the growth and physiological conditions of trees in forests, it is important to know the state of aerosols that are deposited on the surface of the leaves or needles. In this study, we developed methods of visualization of submicron-sized aerosols that were artificially deposited from the gas-phase or liquid phase onto tree leaves or needles in trees. Firstly, we used field-emission scanning electron microscopy (FE-SEM) to observe black carbon (BC) particles that were artificially sprayed onto the leaves or needles. The distribution of BC particles deposited on the leaves and needles were distinguished based on the size and morphological features of the particles. The distribution and agglomerates size of BC particles differed between two spraying methods of BC particles employed. Secondly, we tried to visualize gold (Au) particles that were artificially sprayed onto the leaves using energy dispersive X-ray spectrometry (EDX) coupled to FE-SEM. We detected the Au particles based on the characteristic X-ray spectrum, which was secondarily generated from the Au particles. In contrast to the case of BC particles, the Au particles did not form agglomerates and were uniformly distributed on the leaf surfaces. The present results show that our methods provide useful information of adsorption and/or behavior of fine particles at the submicron level on the surface of the leaves.