• 제목/요약/키워드: Particles

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다단 임팩터(MOUDI)의 조대 입자 채취 특성 (Collection Characteristics of a MOUDI Cascade Impactor for Coarse Particles)

  • 배귀남;지준호;문길주
    • 한국대기환경학회지
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    • 제15권6호
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    • pp.799-804
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    • 1999
  • Particle collection characteristics of the MOUDI cascade impactor has been studied for coarse particles in the range of 2 to 20$mu extrm{m}$ in aerodynamic diameter. A vibrating orifice aerosol generator was empolyed to generate monodisperse test aerosols. The oleic acid and sodium chloride(NaCl) particles were used as test aerosols. Aluminum foil and Teflon filter were selected as impaction media. The sampling flow rate was changed from 25 to 35L/min. Particle collection efficiency for single stage was examined for liquid particles. The stage response was obtained experimentally for the cascade impactor composed of three stages and a backup filter. The results showed that most of particle collection efficiencies measured in this work are similar to the efficiency curves obtained by Marple et al.(1991). For particles less than cut-off size of the stage, the collection efficiencies of solid particles are similar to those of loquid particles. However, the collection efficiency of solid particles decreases with mereasing particle diameter for the particles greater than the actual cut-off size of the impactor. The particle collection efficiency increases with increasing sampling flow rate at the same particel size. However, the collection efficiency curves seem not to be greatly shifted with the flow rate. The stage responses obtained by direct measurements in this work are in good agreement with those derived from the collection efficiency curves for single stage.

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STUDIES FOR THE CHARACTER OF NANO-SIZED $TiO_2$ PARTICLE SYNTHESIZED BY MICRO-EMULSION METHOD AND GOLD-DEPOSITED $TiO_2$ PARTICLE

  • Jhun, Hyun-Pyo;Park, Jae-Kiel;Lee, Kyoung-Chul;Park, Jae-Eon
    • 대한화장품학회지
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    • 제22권2호
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    • pp.52-69
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    • 1996
  • Nano-Sized TiO$_2$ particles with diameter between 2 and 5 nm are synthesized in Water/Triton X-100/n-Hexane microemulsion. Particles show the amorphous structure and partially hydroxide form. The optical absorbance of particles appears at 250nm and band edge at 340nm. Gold metal is deposited on the surface of TiO$_2$ particles by reduction reaction of Au(III) ion with sodium hypophosphite. The size of gold-deposited particles is 20nm, and the optical absorbance appears at 270nm and at 550nm. So particles show the red color. The dense precipitation is formed by aggregation in the TiO$_2$ nano-sized particles of about 5nm size. But the bulky precipitation is formed by agglomeration phenomena in the gold-deposited particles of 20nm size. And also gold-deposited particles is easily dispersed by being re-dispersed in PEG/Water solution. This study has compared those things measuring the SPF characteristics of the cosmetics made of the synthesized particles. If the particle size is controlled appropriately, then the SPF value will be higher, or more colorless cosmetics will be made.

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Synthesis and Compaction Behavior of Monodispersed 3Y-ZrO2 Spherical Agglomerates

  • Choi, Hong-Goo;Yong, Seok-Min;Kim, Do Kyung
    • 한국세라믹학회지
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    • 제50권6호
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    • pp.434-438
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    • 2013
  • Monodispersed 3Y-$ZrO_2$ spherical agglomerates were synthesized by thermal hydrolysis process followed by crystallization processes (hydrothermal treatment and calcination). The crystallization process affected the properties of the final particles, such as the primary particle size, the agglomeration state, and the fraction of $ZrO_2$ monoclinic phase. The hydrothermal treated spherical particles were porous microstructures (weak agglomerates) composed of small primary particles with a size of 14 nm, but the calcined spherical particles had a dense microstructure due to the hard aggregation between primary particles. While the calcined particles had a low green density due to the hard aggregation, hydrothermal treated ones were soft agglomerates and had a deflection point at 50 MPa due to the rearrangement of secondary spherical particles and the filling of the interstices with the primary particles. Finally, the green density of hydrothermally treated $ZrO_2$ particles was 58% at 200 MPa.

레이저를 이용한 마이크로/나노 알루미늄 입자 생성과 점화 (Generation and ignition of micro/nano - aluminum particles using laser)

  • 이경철;여재익
    • 한국추진공학회:학술대회논문집
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    • 한국추진공학회 2012년도 제38회 춘계학술대회논문집
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    • pp.429-434
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    • 2012
  • 금속 연료로 사용되는 마이크로/나노 알루미늄 입자를 산화피막에 의한 점화 지연을 최소화 하는 점화 방법을 제시 하였다. 알루미늄 입자를 생성시킴과 동시에 가열하여 입자가 생성된 직후 산소와 접촉시 격렬한 산화 반응을 유도하여 점화를 시키는 방법이다. 1064 nm 파장의 Nd:YAG 펄스 레이저를 이용한 레이저 삭마(laser ablation)를 알루미늄 시편에 발생시켜 입자를 생성하였으며, 산란 기법(scattering method)을 이용하여 입자를 가시화하여 생성을 확인하였다. 10.6 ${\mu}m$ 파장의 $CO_2$ 연속 레이저를 사용하여 알루미늄 시편을 가열하고 생성된 입자의 점화 열원으로 사용하여 알루미늄 입자가 점화되고 연소되어 이동하는 궤적을 확인하였다.

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정제 제형 제조를 위한 포공영 추출물 함유 분말의 제조 및 평가 (Fabrication and Characterization of Taraxacum platycarpum Extract-loaded Particles for Tablet Dosage Form)

  • 진성규
    • 한국분말재료학회지
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    • 제26권3호
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    • pp.225-230
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    • 2019
  • To develop Taraxacum platycarpum extract (TP)-loaded particles for tablet dosage form, various TP-loaded particles composed of TP, dextrin, microcrystalline cellulose (MCC), silicon dioxide, ethanol, and water are prepared using a spray-drying method and fluid-bed-drying method. Their physical properties are evaluated using angle of repose, Hausner ratio, Carr's index, hardness, disintegrant time, and scanning electron microscopy. Optimal TP-loaded particles improve flowability and compressibility. Furthermore, 2% silicon dioxide gives increased flowability and compressibility. The formula of TP-loaded fluid-bed-drying particles at a TP/MCC/silicon-dioxide amount of 5/5/0.2 improves the angle of repose, Hausner ratio, Carr's index, hardness, and disintegrant time as compared with the TP-loaded spray-drying particles. The TP-loaded fluid-bed-drying particles considerably improve flowability and compressibility ($35.10^{\circ}$ vs. $40.3^{\circ}$, 0.97 vs. 1.17, and 18.97% vs. 28.97% for the angle of repose, Hausner ratio, and Carr's index, respectively), hardness (11.34 vs. 4.7 KP), and disintegrant time (7.4 vs. 10.4 min) as compared with the TP-loaded spray-drying particles. Thus, the results suggest that these fluid-bed-drying particles with MCC and silicon dioxide can be used as powerful particles to improve the flowability and compressibility of the TP.

경유자동차 입자상물질의 휘발성에 대한 실험적 연구 (Experimental Study of Volatility of Diesel Exhaust Particles)

  • Gwon Sun-Park;Lee Gyu-Won;Saito K.;Shinozaki O.;Seto T.
    • 한국대기환경학회:학술대회논문집
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    • 한국대기환경학회 2002년도 춘계학술대회 논문집
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    • pp.229-230
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    • 2002
  • Diesel exhaust particles are mostly sub-micrometer agglomerates composed of carbonaceous primary particles ranging from 10 to 80nm, but contain also adsorbed or condensed hydrocarbons, hydrocarbon derivatives, sulfur compounds, and other materials. If particles are primarily composed of volatile materials, they have different health impacts from solid particles. Thus, the analysis of the volatility of diesel particles is one of an important diesel research area. (omitted)

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THREE-BODY ABRASIVE WEAR IN A BALL-CRATERING TEST WITH LARGE ABRASIVE PARTICLES

  • Stachowiak, G.B.;Stachowiak, G.W.
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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    • pp.199-200
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    • 2002
  • Three-body abrasive wear resistance of mild steel, low alloy steel (Bisalloy) and 27%Cr white cast iron was investigated using a ball-cratering test. Glass beads, silica sand, quartz and alumina abrasive particles with sizes larger than $100{\mu}m$ were used to make slurries. It was found that the wear rates of all three materials tested increased with time when angular abrasive particles were used and were rather constant when round particles were used. This increase in wear rates was mainly due to the gradual increase in ball surface roughness with testing time. Abrasive particles with higher angularity caused higher ball surface roughness. Mild steel and Bisalloy were more affected by this ball surface roughness changes than the hard white cast iron. Generally, three-body rolling wear dominated. The contribution of two-body grooving wear increased when the ball roughness was significant. More grooves were found when round particles were used or the size of the particles was decreased.

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Core-Shell Polymerization with Hydrophilic Polymer Cores

  • Park, Jong-Myung
    • Macromolecular Research
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    • 제9권1호
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    • pp.51-65
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    • 2001
  • Two-stage emulsion polymerizations of hydrophobic monomers on hydrophilic seed polymer particles were carried out to make core-shell composite particles. It was found that the loci of polymerization in the second stage were the surface layer of the hydrophilic seed latex particles, and that it has resulted in the formation of either eccentric core-shell particles with the core exposed to the aqueous phase or aggregated nonspherical composite particles with the shell attached on the seed surface as many small separated particles. The driving force of these phenomena is related to the gain in free energy of the system in going from the hydrophobic polymer-water interface to hydrophilic polymer-water interface. Thermodynamic analysis of the present polymerization system, which was based on spreading coefficients, supported the likely occurrence of such nonspherical particles due to the combined effects of interfacial free energies and phase separation between the two polymer phases. A hypothetical pathway was proposed to prepare hydrophilic core-hydrophobic shell composite latex particles, which is based on the concept of opposing driving and resistance forces for the phase migration. It was found that the viscosity of the monomer-swollen polymer phase played important role in the formation of particle morphology.

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오사카만에서 부유토사의 확산특성에 대한 침강속도의 중요성 (Importance of the Settling Velocity on the Suspended Solids Diffusion in Osaka Bay)

  • 김종인
    • 한국해양공학회지
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    • 제16권5호
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    • pp.41-48
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    • 2002
  • Numerical experiments are conducted using a three-dimensional baroclinic equation model and a Lagrangian method for clarifying the effect of th settling velocity on the suspended solids diffusion caused by the dredging and the reclamination works. Diffusion characteristics of the neutral particles and the weighting particles is experimented by the Lagrangian particles trajectory model, The results show that the diffusion characteristics of the suspended solids is effected by the settling velocity classified by the particles size in the density layered semi-closed bay. To estimate exactly the diffusion characteristics of the suspended solids and the contaminant with weight the three-dimensional baroclinic equation model and the three-dimensional Lagrangian particles trajectory model considering the settling velocity of the particle in the density layered semi-closed bay must be used.

Study on the Simulation for the Removal of Different Sized Particles in Suspension by Deep-Bed Filtration

  • Choo, Chang-Upp
    • International Journal of Safety
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    • 제4권1호
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    • pp.18-22
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    • 2005
  • A model was proposed for investigating the particle removal from suspension with particles of different sizes by deep-bed filtration, and the collection efficiency was predicted by computer simulation. Deposited particles on the pore surface may act as additional collector and reduce the pore size, which contribute to the improved collection efficiency with increase of deposition. Computer experiments for suspension of particles of three sizes and its equivalent size of mono particles were carried out and compared. The collection efficiency of suspension with poly-dispersed particles shows higher efficiency than that of suspension with mono-dispersed particles. Also the collection efficiency of smell particle of mixture is higher that that of same uniform size particles.