• Environmental Engineering Research
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• v.11 no.5
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• pp.257-265
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• 2006

The purpose of research is to mix the fly ash from municipal solid waste incinerator in the recycled Polypropylene and to recycle. The specimen was produced by mixing 20 wt.% of MSWI fly ash at maximum in the recycled Polypropylene and the particle size analyzer, DSC, TGA, SEM and UTM instruments were used to analyze the physical chemical properties of the specimen. As a result of measurement, the average particle size of MSWI fly ash was $18.08\;{\mu}m$. In TGA analysis, the temperature of specimen S-5 at 50% of weight decrease was risen by $7^{\circ}C$ higher than specimen S-1. In UTM measurement, specimen S-2 showed the maximum strength for tensile strength and specimen S-3 showed the maximum strength for flexural strength. But, impact strength was decreased according to the increasing proportion of MSWI fly ash. In conclusion, when the proper amount of MSWI fly ash was added to the recycled Polypropylene, thermal endurance, tensile strength and flexural strength could be increased, but impact strength was decreased.

• Analytical Science and Technology
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• v.8 no.4
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• pp.411-418
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• 1995

A method for the direct determination of elemental content in each of aerosol particles by inductively coupled plasma atomic emission (ICP-AES) or mass spectrometry (ICP-MS) is described. This method is based upon the introduction of diluted aerosol into an ICP and the measurement of either the flash emission intensities of an atomic spectral line or ion intensities. A pulse-height analyzer is used for the measurement of the distribution of the elemental content. In order to calibrate the measuring system, monodisperse aerosols are used. The potentials of the method are shown by demonstrating the copper emission signals from the aerosols generated at a small electric switch, a study of the relation between the decreasing rate of particle number density and particle size, and measurements of calcium contents in the individual biological cells.

• Bulletin of the Korean Chemical Society
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• v.30 no.7
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• pp.1505-1515
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• 2009

A new method to semicontinuously determine $PM_{2.5}$ ionic species with a short time resolution is described in detail. In this system, a particle collection section (mixing part, particle collection chamber, and air/liquid separator) was developed. A Y-type connector was used to mix steam and an air sample. The particle collection chamber was constructed in the form of a helix coil and was cooled by a water circulation system. Particle size growth occurred due to the high relative humidity and water absorbed particles were efficiently collected in it. Liquid samples were drained out with a short residence time (0.08-0.1 s). The air/liquid separator was also newly designed to operate efficiently when the flow rate of the air sample was 16.7 L $min^{-1}$. For better performance, the system was optimized for particle collection efficiency with various types of test aerosols such as ($NH_4)_2SO_4,\;NaCl,\;NH_4HSO_4,\;and\;NH_4NO_3$. The particle collection efficiencies were almost 100% at different concentration levels in the range over 500 nm in diameter but 50-90% in the range of 50-500 nm under the following experimental conditions: 15 coil turns, a water flow rate for steam generation of 0.65 mL $min^{-1}$, and an air sample flow rate of 16.7 L $min^{-1}$. Finally, for atmospheric applications, chemical compositions of $PM_{2.5}$ were determined with a time resolution of 20 min on January 11-24, 2006 in Seoul, Korea, and the chemical characteristics of $PM_{2.5}$ ions were investigated.

• KIEE International Transactions on Electrophysics and Applications
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• v.4C no.2
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• pp.39-44
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• 2004

The present paper gives a review of the recent development of a differential mobility analyzer (DMA) available for both particle size measurements and production of monodisperse particles in the nanometer range. Operating principles of a general DMA are introduced as well as characteristics of highly functional DMAs such as those capable of classifying particles in a measurement range as broad as 1-1000nm at low pressures. Some examples of DMA applications are also described.

• Journal of the Korean Ceramic Society
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• v.55 no.3
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• pp.275-284
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• 2018

In the ball milling process of ceramic powders, according to economic considerations for industrial applications, it is very important to quickly determine the optimum process condition with the maximum grinding efficiency. However, it is still difficult to determine the optimum condition for a ball mill with respect to the various process parameters, such as the rotational speed and the milling time. Ball milling was carried out at the same starting conditions with given amounts of alumina powders, balls and water, and was conducted slower or faster or a critical rotational speed was just determined by observing the angular position of the slurry in a semi-translucent polyethylene laboratory container. With respect to the different rotational speeds, which were slower or faster than the critical rotational speed, the particle size distribution of the grained powders and the acoustic intensity caused by cascading of the balls led to various behaviors. From the results of the particle size distribution and the acoustic signal analysis in the ball milling, there was one rotational speed that made the finest milled powder with maximum acoustic intensity. As a result, there was a correlation between the ground particle size and the acoustic intensity, which yields the interpretation that it can be possible in-situ to determine the optimum condition of ball milling by acoustic signal without repeated measurement efforts.

• Journal of Korean Society for Atmospheric Environment
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• v.20 no.E2
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• pp.53-59
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• 2004

The roadway tunnels in urban areas give rise to problems such as a localized air pollution. Here, we report the results of a case study of an urban roadway tunnel measurement. The size-resolved particle sampling was carried out with a two 2-stage filter pack samplers and an Andersen impactor sampler at the center of Buk-Ak tunnel in November 2001. Particle Induced X-ray Emission (PIXE) was applied to determine the elemental composition of size-resolved particles divided into soluble and insoluble fractions. The Thermal/Optical Reflectance (TOR$^{(R)}$) method was also employed in analyzing of elemental carbon (EC) and organic carbon (OC). Mass concentrations of fine (< 1.2 ${\mu}{\textrm}{m}$) and coarse (> 1.2 ${\mu}{\textrm}{m}$) particles are 165 and 48 $\mu\textrm{g}$ m$^{-3}$ , respectively. Total elemental mass concentration (the sum of insoluble coarse, soluble coarse, insoluble fine, and soluble fine) is found to be 24$\mu\textrm{g}$ m$^{-3}$ and comprises only 11 % of total particle mass concentration. The concentrations of EC, OC, and mass show the clear dependency on particle size with the maximum between 0.1 and 0.43 ${\mu}{\textrm}{m}$ aerodynamic diameters. Total carbon (sum of EC and OC) accounts for approximately 70% of mass concentration.n.

• Korean Journal of Soil Science and Fertilizer
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• v.32 no.3
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• pp.274-278
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• 1999

Determination of soil texture, particularly the clay fraction, is an important measurement in most researches related with soil. In this study micro-pipette method For soil particle size analysis was compared with the standard hydrometer method. Micro-pipette method can eliminate the need for bulky laboratory equipment and long settling times associated with the standard hydrometer or pipette method. In the results of this investigation, the particle size data obtained with micro-pipette method were in good agreement with those found using standard hydrometer method. And with this method one person could run analysis much larger numbers of soil sample per day than with hydrometer method in relatively small laboratory space.

• Journal of the Korean Institute of Gas
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• v.2 no.2
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• pp.55-60
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• 1998

In this study, we investigated the dust explosion characteristics by determining minimum ignition energy and explosion limit for this experiment, we used pine-tree dust which was used widely for the filler of thermosetting resin. The experiment was accomplished according to the variation of discharge gap, dust concentration, particle size and humidity. The result of this experiment are as follows; (1) The relation between the discharge gap and ignition energy was that ignition energy decreased according as the discharge gap became small, but increased when the discharge gap was below 4mm and suddenly became infinite when the discharge gap was below. So, we knew that this infinite value was limit discharge gap. (2) When the dust concentration increase and the particle size became microscopic it was easy to explore and in the same particle size, if the humidity increase the minimum ingnition energy decreased.

• Mass Spectrometry Letters
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• v.2 no.2
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• pp.57-60
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• 2011

As background significantly affects measurement accuracy and a detection limit in determination of the trace amounts of uranium, it is necessary to determine the impurities in the Lexan detector film for single particle measurements by thermal ionization mass spectrometry coupled with fission track technique (FT-TIMS). We have prepared various micro sizes of the blank Lexan detector film using a micromanipulation technique for uranium measurements by TIMS. Few tens of fg of uranium background with no remarkable dependency on the film sizes were observed in the blank Lexan films with the sizes from $50{\times}50\;{\mu}m^2$ to $300{\times}300\;{\mu}m^2$. Based on the determination of the uranium background in the Lexan film, any background correction is necessary in the isotopic analysis of a uranium single particle with micron sizes when the particle bearing Lexan film is dissected with less than $300{\times}300\;{\mu}m^2$ size. The isotopic analysis of a uranium particle in U030 standard material using TIMS was carried out to verify the applicability of the Lexan film to the single particle analysis with high accuracy and precision.

• Journal of the Korean Ceramic Society
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• v.53 no.1
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• pp.7-12
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• 2016

In this paper, we have developed a simple, new and economical carbonation method to synthesize a pure form of aragonite needles using dolomite raw materials. The obtained aragonite Precipitated Calcium Carbonate (PCC) was characterized by XRD and SEM, for the measurement of morphology, particle size, and aspect ratio (ratio of length to diameter of the particles). The synthesis of aragonite PCC involves two steps. At first, after calcinated dolomite fine powder was dissolved in water for hydration, the hydrated solution was mixed with aqueous solution of magnesium chloride at $80^{\circ}C$, and then $CO_2$ was bubbled into the suspension for 3 h to produce aragonite PCC. Finally, aragonite type precipitated calcium carbonate can be synthesized from natural dolomite via a simple carbonation process, yielding product with average particle size of $30-40{\mu}m$.