• Title/Summary/Keyword: Particle loss

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Effect of Precipitants and Precipitation Conditions on Synthesis of β-Ga2O3 Powder (침전제의 종류 및 침전 공정의 변화가 β-Ga2O3 분말 합성에 미치는 영향)

  • Hwang, Su Hyun;Choi, Young Jong;Ko, Jeong Hyun;Kim, Tae Jin;Jeon, Deok Il;Cho, Woo Suk;Han, Kyu Sung
    • Korean Journal of Materials Research
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    • v.24 no.4
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    • pp.214-220
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    • 2014
  • In this research, a precipitation method was used to synthesize ${\beta}-Ga_2O_3$ powders with various particle morphologies and sizes under varying precipitation conditions, such as gallium nitrate concentration, pH, and aging temperature, using ammonium hydroxide and ammonium carbonate as precipitants. The obtained powders were characterized in detail by XRD, SEM, FT-IR, and TG-DSC. From the TG-DSC result, GaOOH phase was transformed to ${\beta}-Ga_2O_3$ at around $742^{\circ}C$, and weight loss percent was about 14 % when $NH_4OH$ was used as a precipitant. Also, ${\beta}-Ga_2O_3$ formed at $749^{\circ}C$ and weight loss percent was about 15 % when $(NH)_2CO_3$ was used as a precipitant. XRD results showed that the obtained $Ga_2O_3$ had pure monoclinic phase in both cases. When $(NH)_2CO_3$ was used as a precipitant, the particle shape changed and became irregular. The range of particle size was about $500nm-4{\mu}m$ based on various concentrations of gallium nitrate solution with $NH_4OH$. The particle size was increased from $1-2{\mu}m$ to $3-4{\mu}m$ and particle shape was changed from spherical to bar type by increasing aging temperature over $80^{\circ}C$.

Solid Particle Erosion Properties of Hot-Dip Aluminized Economizer Steel Tube (용융 알루미늄 도금된 절탄기 강재 튜브의 고상입자 침식 특성)

  • Park, Il-Cho;Han, Min-Su
    • Corrosion Science and Technology
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    • v.20 no.6
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    • pp.384-390
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    • 2021
  • In this paper, durability evaluation and surface damage mechanism were investigated through solid particle erosion (SPE) test after applying hot-dip aluminizing (HDA) technology for the purpose of maintenance of marine economizer tube. Damaged surface shape was analyzed using SEM and 3D microscope. Compositional changes and microstructure of the HDA layer were analyzed through EDS and XRD. Durability was evaluated by analyzing weight loss and surface damage depth after SPE. HDA was confirmed to have a two-layer structure of Al and Al5Fe2. HDA+HT was made into a single alloy layer of Al5Fe2 by diffusion treatment. In the microstructure of HDA+HT, void and crack defect were induced during the crystal phase transformation process. The SPE damage mechanism depends on material properties. Plastic deformation occurred in the substrate and HDA due to ductility, whereas weight loss due to brittleness occurred significantly in HDA+HT. As a result, the substrate and HDA showed better SPE resistance than HDA+HT.

A Study on the Estimation Method of Loss Ratio in Dredged Fills (준설매립토의 유실율 평가방법 정립에 관한 연구)

  • Kim, Seog-Yeol;Choi, Hyo-Pum;Park, Jae-Eock;Kim, Seung-Wook
    • Journal of the Korean GEO-environmental Society
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    • v.3 no.1
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    • pp.67-77
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    • 2002
  • Volume change of the dredged soils is composed of the volume loss of soil particle flowing over an outflow weir with water and settlement due to both the self-weight consolidation in reclaimed layer and the desiccation at the surface of reclaimed layer. In order to estimate the amount of soil particles flowing over an outflow weir with water, the evaluation procedure of loss ratio of the dredged soils is proposed in the present study based on the Marsal's modified breakage theory and the results of hydrometer analyses. To verify a validity of the proposed procedure, evaluated loss ratio is compared with results from the other existing methods. The model test results and those of field test were compared and analyzed. Also, the variation of soil loss ratio was examined through the model test in the lab.

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A Study on the SVR Optimal Placement in Distribution System with Distributed Generators (분산전원이 연계된 배전 계통의 SVR 최적 설치위치 선정)

  • Lee, Hyun-Ok;Huh, Jae-Sun;Kim, Chan-Hyeok;Kim, Jae-Chul
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.27 no.11
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    • pp.69-75
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    • 2013
  • This paper proposes a new algorithm for the optimal placement of a step voltage regulator(SVR) in distribution system with Distributed Generators(DG) using a Particle Swarm Optimization(PSO). The objective function of this algorithm is to find optimal placement for minimum loss while maintaining each node voltage fluctuations within upper and lower limits. In the objective function of proposed algorithm, the deviations to reference voltage and the distribution loss are considered. To verify effectiveness of the proposed method, simulation is implemented using MATLAB.

A Study on the Surface Deterioration Evaluation of Epoxy Resin Coating as Anticorrosive Material of Concrete Water Tank Using Ozone($O_3$) (오존 정수처리 음용수조 구조물에 사용하는 에폭시 수지 방수.방식재의 표면특성 평가)

  • 오상근;강효진;곽규성
    • Proceedings of the Korea Concrete Institute Conference
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    • 2003.11a
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    • pp.513-518
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    • 2003
  • Recently, advanced systems for water treatment are introduced for water quality improvement. One of those systems is water treatment method using ozone($O_3$). For it has strong oxidizing energy, it is necessary to have materisl stability against $O_3$. In this paper, epoxy resin specimens using as anticorrosive material of concrete structure for drink water are used to serve as a material of deterioration evaluation. It is to be studied weight loss, surface corrosion of specimens, ingredient analysis of floating particle, a solute of chemical ingredient by way of accelerated ozone testing. As the results of experiment, specimen weight is decreased. The surface of specimen is eroded heavily and showed a loss of gloss and floating particle, and in the stability for drinking water, harmful ingredient is not detected in the water.

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Study on the Effect of Particles Injected Into the Head/Disk Interface (헤드-디스크 인터페이스에 주입되는 입자의 영향에 대한 연구)

  • Han Je-Hee;Lee Rae-Jun;Kim Dae-Eun;Kang Tae-Sik;Cho Keung-Youn
    • 정보저장시스템학회:학술대회논문집
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    • 2005.10a
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    • pp.179-183
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    • 2005
  • Particles in the HDD can cause serious damages such as scratches and thermal asperity(TA) at the head/disk interface(HDI). Accordingly, particles cause data loss including physical and electrical damages. To improve the reliability of head-disk interface, understanding the damage characteristics at the HDI due to particle interactions is required. The materials such as $A1_2O_3$, TiC and aluminum were used in this experiment. The size and hardness of particles injected into the HDI are closely relevant to surface damage caused the data loss on the disk and head. In this paper, a variety of scratches were analyzed using scanning electron microscope(SEM) and atomic force microscope(AFM). In order to analyze defects of very small size on the disk, optical surface analyzer(OSA) was also used.

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The Firing of Slag Containing Batch (광재 조합물 소성에 관한 연구)

  • 박기형;송한식;천성순;김종희
    • Journal of the Korean Ceramic Society
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    • v.15 no.4
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    • pp.185-192
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    • 1978
  • The effects of slag prticle size, $Na_2SO_4$ addition and sulphide in slag to the foam formation was investigated. This investigation showed that the slag particle size and the amount of $Na_2O$ had produced effects on the size of the foam, foam distribution and firing temperatures. In addition to that the amount of sulphide loss during the firing was controlling factor for the foam formation. The smaller slag particles and higher firing temperatures increased the loss of sulphide in the slag. The addition of $Na_2SO_4$ in the slag batch was likely to inhibit the foam formation. The larger slag particles resutled in the larger foam size and tended to be increasing the batch firing temperature. The main constituents of slag formed glass consisted of wallstonite and glassy phase. It is believed that the controlling the slag particle size and the amount of $Na_2SO_4$ in the slag batch will probably be main factors in foam formation.

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Microwave Characteristics of Ferroxplana-Silicone Rubber Composite (Ferroxplana-Silicone Rubber 복합체의 마이크로파 특성)

  • 박효열;김근수;김태옥
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.53 no.8
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    • pp.401-406
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    • 2004
  • In this experimentation, we investigated the characteristics of electromagnetic wave absorption of ferroxplana powder and silicone rubber composite. Ferroxplana was prepared by flux method at low temperature. The crystallization, magnetic properties and particle morphology of the obtained ferroxplana powder were investigated by using XRD, VSM and SEM. The particle size of ferroxplana powder was 2∼4$\mu\textrm{m}$ at the ratio of R=26, The coercivity and saturation magnetization of ferroxplana powder increased slightly with increase of temperature, The magnetic loss was the main factor of electromagnetic wave absorption of ferroxplana powder and silicone rubber composite, The maximum reflection loss of composite was about -l5dB below 4GHz.

Effect of Coal Properties on Combustion Characteristics in a Pulverized Coal Fired Furnace (미분탄 연소로에서 연소특성에 미치는 석탄특성에 관한 연구)

  • Lee, Byoung-Hwa;Song, Ju-Hun;Lee, Cheon-Sung;Chang, Young-June;Jeon, Chung-Hwan
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.33 no.10
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    • pp.737-747
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    • 2009
  • This study is to investigate the effect of the moisture, volatile matter and particle size in the coal on the pulverized coal combustion characteristics using CFD. The results show that as the moisture content in coal increases, flame temperature decreases because of heat loss driven from latent heat of vaporization and reduction of heating value. As the volatile matter content in the coal increases, the temperature in the region near the burner increases, while the temperature in rear region of boiler decreases. The solution to keep the temperature in the rear region of boiler is suggested that particle size is needed to be larger. As the particle size increases, the temperature in the rear region of boiler show tendency to increase, for combustion burning time of coal could be extended.

Evaluation of The Wear Characteristics on The White Metal Bearing in a Low Speed Two-Stroke Marine Diesel Engine (저속 2행정 박용 기관에서의 LO 입자 오염도에 따른 베어링 마모 특성 평가)

  • Ahn, Y.H.;Kim, D.Y.;Kim, Y.C.;Park, D.J.
    • Proceedings of the Korean Society of Marine Engineers Conference
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    • 2005.11a
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    • pp.21-22
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    • 2005
  • A study on the wear characteristics of the white metal(Sn-base alloy) bearing as a function of particle contamination level was conducted in order to establish control criteria of the lubricant in the 2-stroke marine diesel engine. Particle contamination level of the lubricants ranged from NAS 10 to 12 for the experiments. Bar-on-plate type wear test was performed using reciprocating wear tester. Based on this study it was found that there was no noticeable difference in weight loss of the white metal for NAS10 and NAS11(particle contamination level). Surface roughness of the white metal bearing after the wear test of 8hrs for the highly contaminated lubricant(NAS12 level) was up to $6{\mu}m$ in Rmax whilst that of the less contaminated lubricants(NAS10 & 11) was less than $1.5{\mu}m$ in Rmax.

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