• Title/Summary/Keyword: Particle Size Measurement

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Measurement of the Particle Current Changes Associated with the Flatness of Deflector Mesh Surface in Particle Beam Mass Spectrometer System

  • Kim, Dongbin;Kim, TaeWan;Jin, Yinhua;Mun, Jihun;Lim, In-Tae;Kim, Ju-Hwang;Kim, Taesung;Kang, Sang-Woo
    • Applied Science and Convergence Technology
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    • v.25 no.2
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    • pp.25-27
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    • 2016
  • The surface flatness of metal meshes in a deflector of particle beam mass spectrometer (PBMS) required ideally flat, and this can specify the particle trajectories which goes through the detector. In this research, charged particle current was measured using the different surface roughness deflectors. NaCl particles were generated monodispersed in its size by using differential mobility analyzer and the whole processes were followed the way calibrating PBMS. The results indicate that the mesh surface morphology in the deflector can affect to the particle size and the concentration errors, and sensitivity of PBMS.

Effect of Concentration and Surface Property of Silica Sol on the Determination of Particle Size and Electrophoretic Mobility by Light Scattering Method (광산란법에서 실리카 졸의 농도 및 표면특성이 입자 크기 및 전기영동 이동도 측정결과에 미치는 영향)

  • Cho, Gyeong Sook;Lee, Dong-Hyun;Kim, Dae Sung;Lim, Hyung Mi;Kim, Chong Youp;Lee, Seung-Ho
    • Korean Chemical Engineering Research
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    • v.51 no.5
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    • pp.622-627
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    • 2013
  • Colloidal silica is used in various industrial products such as chemical mechanical polishing slurry for planarization of silicon and sapphire wafer, organic-inorganic hybrid coatings, binder of investment casting, etc. An accurate determination of particle size and dispersion stability of silica sol is demanded because it has a strong influence on surface of wafer, film of coatings or bulks having mechanical, chemical and optical properties. The study herein is discussed on the effect of measurement results of average particle size, sol viscosity and electrophoretic mobility of particle according to the volume fraction of eight types of silica sol with different size and surface properties of silica particles which are presented by the manufacturer. The measured particle size and the mobility of these sol were changed by volume fraction or particle size due to highly active surface of silica particle and change of concentration of counter ion by dilution of silica sol. While in case the measured sizes of small particles less than 60 nm are increased with increasing volume fraction, the measured sizes of larger particles than 60 nm are slightly decreased. The mobility of small particle such as 12 nm are decreased with increase of viscosity. However, the mobility of 100 nm particles under 0.048 volume fraction are increased with increasing volume fraction and then decreased over higher volume fraction.

Uranium Isotopic Ratio Analysis of U-Bearing Particulates By SIMS in CIAE

  • Yonggang, Zhao
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2004.02a
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    • pp.257-259
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    • 2004
  • In this paper measurement method of uranium isotope ratio of uranium-bearing particles in swipe samples was introduced; Swipe sample screening program was proposed on the basis of studying various destructive assay and non-destructive assays. Scanning electron microscope(SEM) equipped with an energy dispersive X-ray fluorescence(XRF) system was applied to locate the deposited uranium-containing particles on the graphite support, particle's composition and size can be identified. Some isotope ratio results were compared with those of other bulk analytical methods; By measuring the same prepared sample, we got the U-particle isotopic ratio data similar to those from IAEA NWAL, indicating that our operation parameters and experimental conditions are viable and can be used for measurement of U-particle isotopic ratio from swipe samples.

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Application of Fluorescence/Scattering Technique to the Measurement of Spray Droplet Size in GDI Injector (직접 분사식 가솔린 인젝터 분무의 입경 측정에 형광/산란광법의 적용)

  • Kwak, Soo-Min;Ryu, Kyeong-Hun;Choi, Bong-Seok;Kim, Duck-Jool
    • Proceedings of the KSME Conference
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    • 2000.11b
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    • pp.353-358
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    • 2000
  • To achieve the requirement for high fuel economy and low emissions, the research for GDI engines is recently very brisk in the whole world. This study was performed to measure distribution of average particle size in non-evaporating spray. The 2-D fluorescence/scattering images of fuel spray were captured simultaneously by visualization system composed of a laser sheet, a doubling prism, optical filters, and an ICCD camera. Using the ratio of the two light intensities, particle size distribution was obtained. The SMD measured by fluorescence/scattering technique was compared with it obtained by PDA. The experimental results show that the spray structure of GDI injector and temporal SMD distribution.

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Characteristics of Aerosol Mass Concentrations and Size Distribution Measured at Anheung, Korea (서해안 안흥에서 관측된 에어로솔의 농도 변화 및 크기분포 특성)

  • Lee, Kwon-Ho;Lee, Kyu-Tae;Kim, Jung-Ho;Mun, Gwan-Ho;Ahn, Joon-Mo
    • Journal of Korean Society for Atmospheric Environment
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    • v.34 no.5
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    • pp.677-686
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    • 2018
  • An intensive measurement was conducted to study the mass and number concentrations of atmospheric aerosols in Anheung ($36.679^{\circ}N$, $126.186^{\circ}E$), the west coastal measurement site of Korea during December 2017~April 2018. To evaluate relationships between the aerosols and meteorological parameters, comparisons of Optical Particle Counter (OPC) measured data and Auto Weather System (AWS) data were performed. Measured PM mass concentrations are $PM_{10}=42.814{\pm}30.103{\mu}g/m^3$, $PM_{2.5}=29.674{\pm}25.063{\mu}g/m^3$, $PM_1=28.958{\pm}24.658{\mu}g/m^3$, respectively. The PM ratios showed that the $PM_{10}$ concentrations contained about 67.8% of $PM_{2.5}$, while most part of $PM_{2.5}$ was $PM_1$ (about 97.1%). Timely collocation with AWS data were performed, exploring relations with the PM concentrations. PM concentrations can be explained by wind direction and relative humidity conditions. The significant reductions of fine particles in mass and number concentrations may attribute to actions on particle growth and wet removal. In these results, we suppose that the aerosol concentrations and size distributions are affected by inflow direction and air mass sources from the origin.

Characteristics of Nano-particle Emitted by Auto-ignited Engine with ULSD, Bio-diesel and DME Fuel and Effects of Oxidation Catalyst on Its Reduction (디젤연소가능 청정연료(ULSD, Bio-Diesel, DME)엔진의 극미세입자 정량화 및 촉매 영향)

  • Lee, Jin-Wook;Bae, Choong-Sik;Schonborn, Alessandro;Ladommatos, Nicos
    • Transactions of the Korean Society of Automotive Engineers
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    • v.17 no.3
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    • pp.81-89
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    • 2009
  • In this experimental study, the effects of clean alternative fuels compatible with diesel combustion on nano-sized particle emission characteristics were investigated in a 0.5L auto-ignited single-cylinder engine with a compression ratio of 15. Because the number concentration of nano-sized particles emitted by automotive engine, that are suspected of being hazardous to human health and environment, might increase with engine fuel considerably and recently attracted attention. So a ultra-low sulfur diesel(ULSD), BD100(100% bio-diesel) and Di-Methyl Ether(DME) fuels used for this study. And, as a particle measuring instrument, a fast-response particle spectrometer (DMS 500) with heated sample line was used for continuous measurement of the particle size and number distribution in the size range of 5 to 1000nm (aerodynamic diameter). As this research results, we found that this measurements involving the large proportion of particles under size order of 300nm and number concentration of $4{\times}10^9$ allowed a single or bi-modal distribution to be found at different engine load conditions. Also the influence of oxygen content in fuel and the catalyst could be a dominant factor in controlling the nano-sized particle emissions in auto-ignited engine.

Vertical Change in Extinction and Atmospheric Particle Size in the Boundary Layers over Beijing: Balloon-borne Measurement

  • Chen, Bin;Shi, Guang-Yu;Yamada, Maromu;Zhang, Dai-Zhou;Hayashi, Masahiko;Iwasaka, Yasunobu
    • Asian Journal of Atmospheric Environment
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    • v.4 no.3
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    • pp.141-149
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    • 2010
  • Aerosol size and number concentration were observed in the atmospheric boundary layer over Beijing (from near the ground to 1,200 m) on March 15 (a clear day) and 16 (a dusty day), 2005. The results were further compared with lidar measurements in order to understand the dependency of extinction on the particle size distribution and their vertical changes. The boundary layer atmosphere was composed of several sub-layers, and a dry air layer appeared between 400 and 1,000 m under the influence of dust event. In this dry air layer, the concentration of the fine-mode particles (diameter smaller than $1.0\;{\mu}m$) was slightly lower than the value on the clear day, while the concentration of coarse-mode particles (diameter larger than $1.0\;{\mu}m$) was remarkably higher than that on the clear day. This situation was attributed to the inflow of an air mass containing large amounts of Asian dust particles and a smaller amount of fine-mode particles. The results strongly suggest that the fine-mode particles affect light extinction even in the dusty atmosphere. However, quantitatively the relation between extinction and particle concentration is not satisfied under the dusty atmospheric conditions since laser beam attenuates in the atmosphere with high concentration of particles. Laser beam attenuation effect becomes larger in the relation between extinction and coarse particle content comparing the relation between extinction and fine particle content. To clarify this problem technically, future in situ measurements such as balloon-borne lidar are suggested. Here extinction was measured at 532 nm wavelength. Measurements of extinction at other wavelengths are desired in the future.

Phase Doppler Measurements and Probability Density Functions in Liquid Fuel Spray (연료분무의 위상도플러 측정과 확률밀도함수의 도출)

  • 구자예
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.18 no.4
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    • pp.1039-1049
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    • 1994
  • The intermitternt and transient fuel spray have been investigated from the simultaneous measurement of droplet sizes and velocities by using Phase/Doppler Particle Analyzer(PDPA). Measurement have been done on the spray axis and at the edge of the spray near nozzle at various gas-to-liquid density ratios(.rho./sub g//.rho./sub l/) that ranges from those found in free atmospheric jets to conditions typical of diesel engines. Probability density distributions of the droplet size and velocity were obtained from raw data and mathematical probability density functions which can fit the experimental distribations were extracted using the principle of maximum likelihood. In the near nozzle region on the spray axis, droplet sizes ranged from the lower limit of the measurement system to the order of nozzle diameter for all (.rho./sub g/ /.rho./sub l/) and droplet sizes tended to be small on the spray edge. At the edge of spray, average droplet velocity peaked during needle opening and needle closing. The rms intensity is greatly incresed as the radial distance from the nozzle is increased. The probability density function which can best fit the physical breakage process such as breakup of fuel drops is exponecially decreasing log-hypebolic function with 4 parameters.

Measurement of Particle Deposition Velocity toward a Horizontal Semiconductor Wafer Using a Wafer Surface Scanner (Wafer Surface Scanner를 이용한 반도체 웨이퍼상의 입자 침착속도의 측정)

  • Bae, G.N.;Park, S.O.;Lee, C.S.;Myong, H.K.;Shin, H.T.
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.5 no.2
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    • pp.130-140
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    • 1993
  • Average particle deposition velocity toward a horizontal semiconductor wafer in vertical airflow is measured by a wafer surface scanner(PMS SAS-3600). Use of wafer surface scanner requires very short exposure time normally ranging from 10 to 30 minutes, and hence makes repetition of experiment much easier. Polystyrene latex (PSL) spheres of diameter between 0.2 and $1.0{\mu}m$ are used. The present range of particle sizes is very important in controlling particle deposition on a wafer surface in industrial applications. For the present experiment, convection, diffusion, and sedimentation comprise important agents for deposition mechanisms. To investigate confidence interval of experimental data, mean and standard deviation of average deposition velocities are obtained from more than ten data set for each PSL sphere size. It is found that the distribution of mean of average deposition velocities from the measurement agrees well with the predictions of Liu and Ahn(1987) and Emi et al.(1989).

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Biocompatible Dispersion Methods for Carbon Black

  • Kim, Hwa;Park, Kwangsik;Lee, Moo-Yeol
    • Toxicological Research
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    • v.28 no.4
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    • pp.209-216
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    • 2012
  • The biological activity of particles is largely dependent on their size in biological systems. Dispersion in the aqueous phase has been both a critical impediment to and a prerequisite for particle studies. Carbon black has been used as a surrogate to investigate the biological effects of carbonaceous particles. Here, biocompatible methods were established to disperse carbon black into ultrafine and fine particles which are generally distinguished by the small size of 100 nm. Carbon black with a distinct particle size, N330 and N990 were suspended in blood plasma, cell culture media, Krebs-Ringer's solution (KR), or physiological salt solution (PSS). Large clumps were observed in all dispersion preparations; however, sonication improved dispersion - averaged particle sizes for N330 and N990 were $85.0{\pm}42.9$ and $112.4{\pm}67.9$ nm, respectively, in plasma; the corresponding sizes in culture media were $84.8{\pm}38.4$ and $164.1{\pm}77.8$ nm. However, sonication was not enough to disperse N330 less than 100 nm in either KR or PSS. Application of Tween 80 along with sonication reduced the size of N330 to less than 100 nm, and dispersed N990 larger than 100 nm ($73.6{\pm}28.8$ and $80.1{\pm}30.0$ nm for N330 and $349.5{\pm}161.8$ and $399.8{\pm}181.1$ nm for N990 in KR and PSS, respectively). In contrast, 1,2-dipalmitoyl-sn-glycero-3-phosphocholine (DPPC) exhibited little effect. Electron microscopy confirmed the typical aciniform structure of the carbon arrays; however, zeta potential measurement failed to explain the dispersibility of carbon black. The methods established in this study could disperse carbon black into ultrafine and fine particles, and may serve as a useful model for the study of particle toxicity, particularly size-related effects.