• 제목/요약/키워드: Partial melting

검색결과 164건 처리시간 0.024초

열처리 공정 변화에 따른 Bi2212/Ag ROSAT 선재의 임계 특성 (The Effect of Different Heat Treatment Processes on Critical Properties of Bi2212/Ag ROSAT Wire)

  • 오원석;장건익;김상철;하동우;오상수
    • Progress in Superconductivity
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    • 제9권1호
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    • pp.111-114
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    • 2007
  • We have investigated the effect of different heat treatment processes on electrical and magnetic properties of Bi2212/Ag ROSAT wire. The ROSAT wire was fabricated by stacking and arranging 12 filaments Bi2212/Ag tapes in triple rotation symmetry in a Ag tube. ROSAT wires have been prepared using a partial melting method with changing $T_{max}$ and $T_a$ in oxygen atmosphere. The highest critical current density($J_c$) at 65 K under 0 T was $21,158\;A/cm^2$ for wire prepared $890\;^{\circ}C(T_{max})$ and $840\;^{\circ}C(T_a)$, respectively. SEM results indicated that the wire prepared at $890\;^{\circ}C(T_{max})$ and $840\;^{\circ}C(T_a)$ showed better directional phases than the other samples. However the result of magnetic susceptibility measurement indicates that the wire prepared $890\;^{\circ}C(T_{max})$ and $835\;^{\circ}C(T_a)$ had better superconducting phases than the other samples. It was revealed that heat treatment temperature was important factor for superconducting properties of the ROSAT wire.

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지열부지의 저속도층을 탐지하기 위한 지진파의 응용성 (The Applicability of Seismic Waves to Detect a Low Velocity Body of the Geothermal Area)

  • 김소구
    • 지질공학
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    • 제4권3호
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    • pp.333-341
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    • 1994
  • Ray Method와 관측지진 자료에 의해서 지각구조 상부 Mantle을 연구하면서 저속도층이 탐지되었다. 우리는 한반도에서 부곡 온천 지역과 추가령 지구대를 통과하는 P파와 S의 도착 시간 지연을 관측했다. 현재 지열 탐사는 이 지역이 심부 저속도 물체는 "지연 암영"이라고 불리우는 높은 지열이상을 설명 해주고 있다. 우리는 하부지각의 부분 용융에 기인한 저속도 물체의 가설을 하부지각의 이차원 비등질 모델의 속도변화가 있음을 Ray Method(Cerveny and Psencik, 1983)에 의해서 분석 하였다.

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급속응고법으로 제작한 Zr기 수소저장합금의 전극특성 (The Electrode Characteristics of the Zr-based Hydrogen Absorbing Alloy Fabricated by the Rapid Solidification Process)

  • 한동수;정원섭;김인곤
    • 한국재료학회지
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    • 제9권4호
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    • pp.386-391
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    • 1999
  • The charge-discharge, the high-rate dischargeability, and the self discharge characteristics of the electrodes composed of rapidly solidified ZrV\ulcornerMn\ulcornerMo\ulcornerNi\ulcorneralloy, which has the form of partial substitution of Mn, Mo, Ni for V in $ZrV_2$ were studied. The alloys were prepared using Arc & RSP(Rapid Solidification Process) at the rotating roller speed of 2000 and 5000 rpm. Some of them were received heat treatment at$ 560 ^{\circ}C$ for 1 hour after the solidification to investigate the effect of the heat treatment. It was fond that cycle life was significantly improved by RSP, whereas discharge capacity, activation rte and high rate dischargeability were decreased compared with the conventional arc melting method. The capacity loss seems to be due to the loss of the crystallinity and the increase of the cycle life ascribed to the presence of the amporphous phase as well as the refined grain size of less than 0.2$\mu\textrm{m}$. Heat treatment of the alloy cooled at 2000 rpm improved the cycle life. In case of the alloys cooled at 5000 rpm, both the discharge capacity and the activation rate were significantly improved by the heat treatment.

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Y211 및 BaCO$_3$ 분말로 Screen Printing 법을 이용한 Cu-sheath의 YBCO 후막 제조 (Fabrication of Cu-Sheathed YBCO Thick Films by Screen Printing Method Using $Y_2$BaCu$O_5$ and BaC$O_3$ Powders)

  • 김경진;한상철;한영희;박병삼;정년호;윤희중;오제명;최희락;성태현
    • Progress in Superconductivity
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    • 제5권2호
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    • pp.132-135
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    • 2004
  • We fabricated YBCO thick films by using a screen printing method with $Y_2$BaCuO$_{5}$(Y211) and BaCO$_3$ powders on Cu-substrate in $N_2$ atmosphere. Cu-sheathed YBCO thick film process is more simple and economic than YBCO coated conductor methods. The heat treatment is performed in the range of 860 - 875 $^{\circ}C$ for 5 min in the tube furnace of $N_2$ atmosphere. The flow rate of $N_2$ gas is fixed 60 $m\ell$/min. Microstructure and phases of thick films were investigated by optical microscope, X-ray diffraction(XRD) and SEM. At heat-treatment temperature, the thick films were partially melted by liquid reaction between CuO of oxidized copper substrate and the powders screen-printed on Cu-sheath. During the heat-treatment procedure, YBCO superconducting grains nucleate.e.

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Physicochemical Properties of Gamma-Irradiated Corn Starch

  • Lee, Yong-Jin;Kim, Sun-Young;Lim, Seung-Taik;Han, Sag-Myung;Kim, Hye-Mi;Kang, Il-Jun
    • Preventive Nutrition and Food Science
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    • 제11권2호
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    • pp.146-154
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    • 2006
  • Structural modification of corn starch by gamma irradiation was evaluated for under dry conditions at varied intensities from 0 to 40 kGy. Under scanning electron microscopy, the granule shape of corn starch was not significantly affected by the irradiation up to 40 kGy. In addition, X-ray diffraction and melting patterns of the irradiated starches were similar to those of the native starch, indicating that crystalline regions in the starch granules were not changed by irradiation. However, the pattern of gel permeation column chromatography showed a significant increase in partial hydrolysis of gamma irradiated starch samples. The degree of polymerization and the paste viscosity of irradiated starch samples dose-dependently decreased significantly with irradiation, and increased solubility and clarity were observed in the irradiated starch solution. In addition, the degree of retrogradation decreased as irradiation dose increased. Irradiation of corn starch has advantages over the ordinary acid or the enzyme hydrolysis modification methods. It does not affect the granular shape and crystalline phase of starch during hydrolysis, and the process can be carried out in dry state.

고속 화염 용사를 통하여 형성된 다중벽 탄소 나노튜브 알루미늄 복합소재 코팅의 특성 평가 (Property Evaluation of HVOF Sprayed Multi-walled Carbon Nanotube Aluminum Composite Coatings)

  • 강기철;박형권;이창희
    • 한국표면공학회지
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    • 제45권1호
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    • pp.1-7
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    • 2012
  • Multi-walled carbon nanotube (MWCNT) aluminum composite powders were deposited to form coatings using a high velocity oxygen fuel (HVOF) spraying process. High thermal energy and contact with atmospheric oxygen were supplied as the MWCNT aluminum composite particles were exposed to a gas flow field at high temperature (${\sim}3.0{\times}10^3$ K) during HVOF spraying. As a result, the particles underwent full or partial melting and rapid solidification due to the high thermal energy, and the exposure to oxygen induced the interfacial reaction of MWCNTs within the particle. The electrical and mechanical properties of MWCNT aluminum composite coatings were evaluated based on microstructure analysis. Electrical resistivity, elastic modulus, and micro-hardness, of the MWCNT aluminum composite coatings were higher than those of pure aluminum coating. The contribution of MWCNTs to the aluminum matrix can be attributed to their high electrical conductivity, dispersion hardening and anchoring effects. The relationship among the properties and the interaction of the MWCNTs with the aluminum matrix is discussed.

Processed cheese 제조에 있어 polyphosphates 대체에 관한 연구 (Studies on the Replacement of Polyphophates in the Processed Cheese)

  • 안효일;이부웅
    • 한국식품영양과학회지
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    • 제11권1호
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    • pp.45-49
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    • 1982
  • 이상의 실험 결과에서 유화제나 증점제가 polyphosphates의 용도처럼 목적에 따라 다양한 경도의 변화를 가져오지 않는 것은 이들 화합물이 Bonell의 제시처럼 polyphosphates가 cheese내에서 단백질과의 완충 작용 및 원하는 texture형성을 하지 못하는 것으로 보인다. 더욱 중요한 것은 polyphosphates가 주는 특유한 processed cheese맛을 내지 못하는 것이다. 모래알같은 조직감을 주는 것은 균일하게 분산되지 않은 단백질이 화합되거나 결정화되기 때문인 것으로 보인다. 증점제나 유화제의 부분적 대치는 물성적으로 좋은 제품을 만들 수 있다. 이러한 결과는 체내에 흡수되어야 할 polyphosphates의 완전 대치는 process cheese의 전형적인 질을 고려한다면 불가능한 것으로 보여진다. 적은 비율의 유지방 cheese 제조에 있어 polyphosphate대치가 이러한 제품에선 현저한 영향을 미치지 않는 것으로 보인다.

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경상남도 울산지역 가대리화강암에 대한 암석화학적 연구 (Petrochemical Study of the Gadaeri Granite in Ulsan Area, Kyeongsang Province)

  • 최선규;위수민
    • 자원환경지질
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    • 제27권5호
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    • pp.459-467
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    • 1994
  • 울산지역에 분포하는 가대리 화강암체는 울산 철 텅그스텐 광화작용의 관계화성암으로서 전형적인 미문상조직을 보여주며, 칼크-알칼리 계열과 I-type화강암류의 지화학적 특성을 나타내고 있다. 가대리화강암은 물이 포화된 상태에서 0.5~2.0 kbar의 압력조건하에서 생성된 것으로 이는 천부에서의 분별결정에 기인된 것으로 화학성분의 분화는 대부분 알칼리 장석의 분별결정작용으로 이루어졌다. 경상분지 최남단에 분포하며 철광화작용과 관련된 미문상화강암체인 마산-김해 화강암체와 가대리화강암제는 미량성분의 화학조성을 비교해볼때 전혀다른 모마그마에서 분화되었음올 시사해준다.

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PVA/메틸셀루로스 블랜드의 상용성에 관한 연구 (Studies on the Compatability of the blend of PVA and Methyl cellulose)

  • 박준서;박장우
    • 한국포장학회지
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    • 제5권2호
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    • pp.1-8
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    • 1999
  • The state of compatability of poly(vinyl alcohol)(PVA) and methyl cellulose(MC), prepared by an aqueous solution casting, were investigated over the entire compositions by dynamical mechanical analyzer(DMA) and differential scanning calorimetry(DSC). The glass transition temperatures of the blends, estimated by DMA, indicate that the blends of PVA and MC showed a definite degree of partial miscibility by showing two glass transition temperatures below 80 wt % MC contents in the blends and one glass transition temperature above 80 wt % of MC contents. The DSC results show a depression of melting point and crystallization temperature of PVA in the blends containing more than 80 wt % MC. This indicates that a considerable compatibility in the blend above 80 wt % MC contents may be attribute to the presence of interaction of hydroxyl groups of component polymers through hydrogen bonding. The DMA study of the effect of plasticizer on the polymers showed that water was a good plasticizer for PVA and PEG400 for MC. The addition of water and PEG400 in the blends showed a synergic plasticizing effect on these blends, which resulted in the large extent of the improvement of the compatibility. The elongation of PVA, MC and blonds was found to increase with addition of PEG400 in the blends, but the tensile strength to decrease with addition of plasticizer.

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SHS법에 의한 티타늄 수소화물 합성 및 티타늄 분말 제조에 관한 연구 (A Study on the Synthesis of Titanium Hydride by SHS(Self-propagating High-temperature Synthesis) Method and the Preparation of Titanium Powder)

  • 하호;박승수;이희철
    • 공업화학
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    • 제5권2호
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    • pp.263-273
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    • 1994
  • SHS법에 의해 Ti-sponge(99.67%)를 수소화반응시켜 티타늄 수소화물을 합성한 다음, 이 분말을 탈수소시켜 티타늄 금속 분말을 제조하였다. 티타늄 수소화물 합성과정에서는 티타늄에 흡장된 수소의 양에 따라 티타늄 수소화물의 입도가 변하였으며, 수소의 압력이 높을수록, 연소파 전파 후 반응시간이 길수록 입도는 감소하였다. 탈수소 반응에서는 탈수소 시간이 길수록 탈수소된 티타늄 입자들이 소결 및 부분 용융되어 입도가 커지는 것으로 나타났다.

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