• 대한전기학회논문지:전기물성ㆍ응용부문C
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• 제54권5호
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• pp.198-205
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• 2005

Many precedent investigations hate been made for the reliable assessment of the insulation state of large power apparatus for which partial discharge detection is one of tile plausible way. In this work, experimental investigations have been carried out to make the comparison on the PD(partial discharge) pattern analysis related to the five different types of artificial defects such as SFMP (Single Free Moving Particle), MFMP (Multi Free Moving Particle), Void, CFP (Conductor-Fixed Protrusion), EP (Enclosure Protrusion). For each PD pattern, PD detection has been done by tee different types of PD sensors such as HFCT(High Frequency Current Transformer), AE(Acoustic Emission) and UHF(Ultra High Frequency). And, in addition, frequency spectrum by the UHF sensor has been also made for each defect respectively. As a result, it is observed that the possibility of obtaining PD pattern based on PRPD(Phase Resolved Partial Discharge) in connection with the defects tinder investigation is dependant on the type of the sensor while the spectrum analysis is always successful to be achieved for every defect. Therefore, it could be suggested that the nature of PD source can be identified more distinctively when the conventional PRPDA is combined with spectrum analysis.

• 한국전기전자재료학회논문지
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• 제20권10호
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• pp.907-911
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• 2007

This paper dealt with the frequency spectrum analysis of acoustic signal produced by partial discharge (PD) in insulation oil and the positioning of PD occurrence to apply in diagnosis of oil insulated transformers. Three types of electrode system ; the needle-plane, the plane-plane, and the wire-wire structure were assembled to simulate partial discharges in oil insulated transformers. A low-noise amplifier and a decoupling circuit were designed to detect acoustic signal with high sensitivity The frequency spectrum of the acoustic signal were 50 kHz ${\sim}$ 260 kHz in the needle-plane, 50 kHz ${\sim}$ 250 kHz in the plane-plane, and 45 kHz${\sim}$195 kHz in the wire-wire electrode system. Their peak frequencies were 145 kHz, 130 kHz and 114 kHz, respectively The position of PD occurrence was calculated by the time difference of arrival (TOA) using three acoustic emission (AE) sensors, and we could find the position within the error of 1 % in the experimental apparatus.

• 한국자기학회지
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• 제4권4호
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• pp.307-312
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• 1994

(Fe, Co)/(Pd, Pt, Cu, Ag)로 이루어진 금속 다층박막에 대한 자기광학 Kerr 효과(${\theta}_{k}$) 스펙트럼을 박막내에서 빛의 다중간섭 이론을 적용하여 계산하였고, 그 결과를 보고된 실험값과 비교하였다. Co/Pd 다층막의 경우, ${\theta}_{k}$ 스펙트럼의 조성에 따른 파장 의존성에 대한 계산값이 서로 잘 일치하였으며, Fe/Cu 및 Fe/Ag 다층막에 있어서는 Cu와 Ag의 광흡수단 영역에서 다층막 고유의 새로운 peak가 나타나는 실험현상을 계산결과로 설명이 가능하였다. 그러나 Co/Pt 다층막의 경우에는 실험으로 측정된 300 nm파장 영역에서의 거대한 자기 광학 효과를 다중간섭이론으로는 설명할 수 없었으며, 이는 Co 또는 Pt 고유의 광학정수가 다층막을 이루면서 변화되어 나타나는 현상으로 생각된다.

• Bulletin of the Korean Chemical Society
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• 제19권9호
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• pp.942-947
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• 1998

The >$^13C$ NMR spectrum of >$^13CO$ adsorbed on Pd particles varies dramatically depending on dispersion. The spectrum of highly dispersed Pd particles supported on silica is a powder pattern ∼800 ppm wide with a first moment of 410 ppm. A low dispersion sample has a motionally narrowed line centered at 750±30 ppm and only ∼85 ppm full width at half height (FWHH). Over several years, high dispersion samples show an increase in the intensity near 750 ppm. These observations are interpreted as an increase of mobile bridging CO on high dispersion Pd surfaces of particles which resulted from smoothing of the metal particle surfaces in the presence of CO.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2002년도 하계학술대회 논문집 C
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• pp.1655-1657
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• 2002

Ultra-wide bandwidth (UWB), narrow bandwidth (single frequency), and a combination of both technologies have been studied for the ultra-high frequency (UHF) partial discharge (PD) monitoring system as a detection scheme. We have experimentally compared those detection methods using a mock-up of 362 kV class single phase gas-insulated switchgear (GIS) and a stable PD source. A rolling-ball type PD cell that produces PDs of about 10 pC, is placed at one end of the GIS. An internal UHF PD sensor was attached several meters away from the PD source. The PD spectrum was measured up to 3 GHz. A useable bandwidth of more than 1 GHz was used to measure UWB signals from the PD. To simulate the narrow bandwidth scheme a bandwidth of 100 kHz centered at several different frequencies was used.

• 한국ITS학회 논문지
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• 제7권6호
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• pp.101-109
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• 2008

본 논문은 클러스터링 기법을 도입하여 기존에 제안된 가중치 협력 스펙트럼 시스템에서 실질적으로 구하지 못했던 Pd를 구하고, 새로운 가중치 생성 알고리즘을 통하여 1차 사용자 신호의 감지 성능을 향상시키는 방법을 제안하였다. 유사한 채널을 같는 CR 사용자를 클러스터링 기법을 이용하여 그룹화하여 각각의 사용자로부터 획득한 센싱 결과를 토대로 Pd를 계산하였다. 또한, 각 클러스터의 검출확률의 제곱 합을 이용하여 가중치(Wj(n+1))를 생성하였다. 이는 기존의 방식보다 센싱 성능이 우수하였으며, 특히 1차 사용자의 신호가 갑자기 사라졌을 경우 신호가 없는 상황에서의 검출 확률인 false alarm rate가 낮아지는 결과를 보였다. 컴퓨터 모의실험을 통하여 이를 검증한다.

• 한국전기전자재료학회논문지
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• 제26권4호
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• pp.309-314
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• 2013

This paper dealt with the radiated electromagnetic wave detection of partial discharge (PD) in oil for insulation diagnostics of oil-immersed transformers. Three types of electrode system were fabricated to simulate the insulation defects that could occur in oil-immersed transformers. Frequency components of radiated electromagnetic wave in oil was measured by broadband bi-conical antennas of 300 MHz~2 GHz and a spectrum analyzer of 9 kHz~3 GHz. Frequency component of electromagnetic waves from PD in oil were highly distributed at 500 MHz. From the result, a narrow-band monopole antenna with the center frequency of 500 MHz was fabricated. We could detect PD signal in insulation oil without an influence of external noise by a measurement system which consists of the prototype monopole antenna, a LNA (Low Noise Amplifier), an oscilloscope and a spectrum analyzer.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1999년도 하계학술대회 논문집 E
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• pp.2028-2030
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• 1999

In this paper, partial discharge(PD) was generated under the two types of needle -plane electrodes in the air. Using a monopole antenna to detect the radiated electromagnetic waves by stream of charge between the electrodes. the progress of partial discharge was studied. To analyze the progress of PD, statistical re-search was introduced. It was executed by personal computer and it can be possible to visualize the progress of PD. The t-test was used for lower voltage applied. The population of background noise spectrum and applied voltage spectrum showed the difference. The new method was introduced to analyze the spectrum. According tho the magnitude of applied voltage, the different statistical methods were used. The results obtained from this work will provide the useful information on partial discharge in time to come.

• 대한화학회지
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• 제36권5호
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• pp.679-684
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• 1992

$trans-[Pd(en)_2Cl_2](ClO_4)-2$ (en = ethylenediamine)와 purine 염기인 Guanine, Adenine 또는 pyrimidine 염기인 Uracil anion을 반응시켜 새로운 팔라듐(IV) 착물을 얻었다. 착물의 중심금속과 각 리간드의 조성비는 $C{\cdot}H{\cdot}N$ 원소 분석으로써 확인하였으며 리간드의 배위자리 등 착물의 구조는 적외선 흡수 스펙트럼 및 $^1H-NMR,\; ^{13}C-NMR$로써 조사하였다. Guanine 또는 Adenine 착물을 purine계 염기가 N7 자리에 배위되었고 출발물질로부터 하나의 en 리간드가 이탈하고 두 $ClO_4^-$가 배위된 $[Pd(en)L_2(ClO_4)_2](ClO_4)_2{\cdot}(en)$ (L = Guanine, Adenine) 구조이다. Uracil 착물은 en과 $ClO_4^-$의 이동없이 Uracil anion의 N1 자리가 배위된 $[Pd(en)_2(Urac)_2](ClO_4)_2$ (Urac = Uracil anion) 구조의 착물로 추정되었다.

• BMB Reports
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• 제34권6호
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• pp.551-558
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• 2001

We extended the measurable time scale of DNA dynamics to submicrosecond using a long-lifetime metal-ligand complex, $[Ru(phen)_2(dppz)]^{2+}$ (phen=1,10-phenanthroline, dppz=dipyrido[3,2-a:2',3'-c]phenazine) (RuPD), which displays a mean lifetime near 350 ns. We partially characterized the fluorescence resonance energy transfer (FRET) in calf thymus DNA from RuPD to nile blue (NB) using frequency-domain fluorometry with a high-intensity, blue light-emitting diode (LED) as the modulated light source. There was a significant overlap of the emission spectrum of the donor RuPD with the absorption spectrum of the acceptor NB. The F$\ddot{o}$rster distance ($R_0$) that was calculated from the spectral overlap was $33.4\;{\AA}$. We observed dramatic decreases in the steady-state fluorescence intensities of RuPD when the NB concentration was increased. The intensity decays of RuPD were matched the closest by a triple exponential decay. The mean decay time of RuPD in the absence of the acceptor NB was 350.7 ns. In a concentration-dependent manner, RuPD showed rapid intensity decay times upon adding NB. The mean decay time decreased to 184.6 ns at $100\;{\mu}M$ NB. The FRET efficiency values that are calculated from the mean decay times increased from 0.107 at $20\;{\mu}M$ NB to 0.474 at $100\;{\mu}M$ NB concentration. The use of FRET with a long-lifetime metal-ligand complex donor is expected to offer the opportunity to increase the information about the structure and dynamics of nucleic acids.