• Bulletin of the Korean Chemical Society
• /
• v.29 no.8
• /
• pp.1575-1578
• /
• 2008

• Analytical Science and Technology
• /
• v.13 no.3
• /
• pp.378-384
• /
• 2000

This Study has been carried out to develop a method of analysis of 8 permitted synthetic food colors [including Brilliant Blue FCF(B1), Indigocarmine (B2), Fast green FCF(G3), Amaranth (R2), Erythrosine (R3), Allura red (R40), Tartrazine (Y4), Sunset Yellow FCF (Y5)] in Korean foods by HPLC. After adjusting to 0.5% HCl, each of the food colors extracted was eluted by Sep-pak $C_{18}$ cartridge. Eluates were then determined by high performance liquid chromatograph with a UV-VIS detector. Recoveries of the 8 synthetic food colors were found to be 81.2-98.0% for soft drinks, 80.6-96.1% for candy, 79.8-96.3% for chewing gum, 76.5-91.7% for cereals, 79.9-93.8% for ice cream and 78.6-94.7% for jelly, respectively. The detection limits were $0.05-0.1{\mu}g/g$.

• Journal of Internet Computing and Services
• /
• v.6 no.3
• /
• pp.17-30
• /
• 2005

A PAK(Password-Authenticated Key Exchange) protocol is used as a protocol to provide both the mutual authentication and allow the communication entities to share the session key for the subsequent secure communication, using the human-memorable portable short-length password, In this paper, we propose distributed key exchange protocols applicable to a smartcard using the MTI(Matsumoto, Takashima, Imai) key distribution protocol and PAK protocol. If only one server keeps the password verification data which is used for password authentication protocol. then It could easily be compromised by an attacker, called the server-compromised attack, which results in impersonating either a user or a server, Therefore, these password verification data should be distributed among the many server using the secret sharing scheme, The Object of this paper Is to present a password-based key exchange protocol which is to allow user authentication and session key distribution, using the private key in a smartcard and a password typed by a user. Moreover, to avoid the server-compromised attack, we propose the distributee key exchange protocols using the MTI key distribution protocol, And we present the security analysis of the proposed key exchange protocol and compare the proposed protocols with the existing protocols.

• Journal of the Korean Chemical Society
• /
• v.43 no.4
• /
• pp.438-446
• /
• 1999

The optimum analytical method of aldehydes, ozone by-products, was established by reverse phase liquid chromatography. Six aldehydes including formaldehyde, acetaldehyde, acrolein, propionaldehyde, butylaldehyde and benzaldehyde, and one ketone including acetone were selected as aldehyde test samples through preliminary experiments. Such analytical conditions as the pH of citrate buffer solution, reaction temperature, reaction time, and concentration of DNPH, the component and composition of desorption solvent were optimized. As the result, pH 3.0 of citrate buffer solution, 40$^{\circ}C$ of reaction temperature, 15 minutes of reaction time, and 0.012% of DNPH concentration were chosen as optimum conditions. Aldehydes-DNPH derivatives in water were concentrated on $C_18$ Sep-Pak cartridge and followed by elution of their derivatives fraction with THF/ACN(70/30) mixture, and showed recoveries of the range from 87 to 107%. Separation condition on Nova-Pak $C_18$ column with low pressure gradient elution from ACN/MeOH/water(30/10/60) of an initial condition to 80% ACN of a final condition was found to give a good resolution within 20 minutes of run time. 86% to 103% of recovery for aldehydes using this method was similar to that for aldehyde using EPA Method 554 which is ranged from 84% to 103%.

• KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
• /
• v.26 no.2
• /
• pp.53-60
• /
• 2020

A concept of household container to create and keep the modified atmosphere (MA) beneficial for fresh produce mix was devised and tested under typical chilled storage conditions of 3℃. The container system containing mixed products is initialized by applying weak hypobaric condition (0.9 atm) and subsequently injecting CO₂ gas at an appropriate low level (0.03 atm). The passive atmosphere modification by produce respiration is then induced to reach a target until gas diffusion tube of proper dimension starts to open. The design was made to attain quasi-steady state mass balance of O₂, CO₂ and N₂ to maintain the desired MA through the storage. Interrupted opening for taking out or placing some products was to reinitialize the loop of control logic. The developed concept was tested by the container which held commodities of spinach, pak choi, oyster mushroom, peeled onion, strawberry and cut carrot. The target optimum MA of 11% O₂ and 10% CO₂ (0.11 and 0.10 atm, respectively) was set to avoid injurious range of O₂ and CO₂ concentrations for any commodities. The developed container system could work to reach and maintain beneficial MA of 0.10-0.12 atm O₂ and 0.07-0.10 atm CO₂ close to the target during the storage contributing to quality retention of products measured in weight loss, chlorophyll content of spinach, ascorbic acid content of pak choi, color of onion, texture of oyster mushroom, bacterial count of strawberry and carotenoids of carrot. The container system shows potential to improve current preservation practice of fresh produce mix on consumers' level.

• Proceedings of the Korea Information Processing Society Conference
• /
• 2017.04a
• /
• pp.1001-1002
• /
• 2017

2차원 바코드는 1차원 바코드의 데이터 용량의 한계를 극복하여 최근 많이 사용되고 있다. 복잡한 환경에서 바코드의 인식을 위해서는 바코드 영역 검출이 중요한 단계이다. 본 논문에서는 딥러닝 기법을 이용하여 QR코드 검출 시스템을 구현한다. 실험은 실생활에서 카메라로 촬영한 바코드 영상을 이용한다.

• Journal of the Korean Mathematical Society
• /
• v.34 no.1
• /
• pp.167-179
• /
• 1997

In the study of a manifold M, the exterior algebra $\Lambda^* M$ plays an important role. In fact, the de Rham cohomology theory gives many informations of a manifold. Another important object in the study of a manifold is its Clifford algebra (Cl(M), generated by the tangent space.

• Journal of the Society of Disaster Information
• /
• v.2 no.1
• /
• pp.39-52
• /
• 2006

In this paper, an analytical and experimental study was performed in order to determine the effects of interaction between vehicle and structure. Results presented in the paper show that analytical method including moving load effect can investigate the trend of structural response due to dynamic interaction between vehicle and structure. The wheel tracking machine fitted with 2-axle test vehicle can demonstrate more accurate dynamic interaction between vehicle and structure than the wheel tracking machine fitted without 2-axle test vehicle.

• The Korean Journal of Food And Nutrition
• /
• v.15 no.2
• /
• pp.97-103
• /
• 2002

Five citrus juices were separated into a ascorbate and phenolic portion using rep-pak C$\_$18/ cartridge, respectively, in order to elucidate the nitrite scavenging effect and N-nitrosodimethylamine(NDMA) formation in model system. The nitrite scavenging effect of ascorbate portion from citrus juices, in the different pH, when added with 5ml were 79.9 ∼98.6% under the condition of pH 2.5. 48.5∼86.3% at pH 4.2 and lower than 35.2% at pH 6.0. The nitrite scavenging effect was excellent phenolic portion rather than ascorbate portion. Particularly, the effect was more 2 times than ascorbate portion under the reaction condition of pH 6.0. When added the phenolic portion in the reaction mixture, NDMA formation was inhibited 92.8% or more in kum quat, mandarin orange and sweet orange juices. But the ascorbate portion was a negative response of the inhibition of NDMA formation. The inhibition on NDMA formation in citrus juice may be due to phenolic compounds were reacted.

• Korean Journal of Clinical Laboratory Science
• /
• v.55 no.4
• /
• pp.261-268
• /
• 2023

[¹⁸F]Fluorocholine is a radiopharmaceutical used non-invasively in positron emission tomography to diagnose parathyroid adenoma, prostate cancer, and hepatocellular carcinoma by evaluating the choline metabolism. In this study, a radiolabeling method for [¹⁸F]fluorocholine was optimized using a solid phase extraction (SPE) cartridge. [¹⁸F]Fluorocholine was labeled in two steps using an automated synthesizer. In the first step, dibromomethane was reacted with [¹⁸F]KF/K2.2.2/K₂CO₃ to obtain the intermediate [¹⁸F]fluorobromomethane. In the second step, [¹⁸F]fluorobromomethane was passed through a Sep-Pak^Ⓡ Silica SPE cartridge to remove the impurities and then reacted with N,N-dimethylaminoethanol (DMAE) in a Sep-Pak^Ⓡ C18 SPE cartridge to label [¹⁸F]fluorocholine. The reaction conditions of [¹⁸F]fluorocholine were optimized. The synthesis yield was confirmed according to the number of silica cartridges and DMAE concentration. No statistically significant difference in the synthesis yield of [¹⁸F]fluorocholine was observed when using four or three silica cartridges (P>0.05). The labeling yield was 11.5±0.5% (N=4) when DMAE was used as its original solution. On the other hand, when diluted to 10% with dimethyl sulfoxide, the radiochemical yield increased significantly to 30.1±5.2% (N=20). In conclusion, [¹⁸F]Fluorocholine for clinical use can be synthesized stably in high yield by applying an optimized synthesis method.