• Title/Summary/Keyword: Optimum Curing time

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Improvement of Polyimide/Epoxy Adhesion Strength from the Modification of Polyimide Surface and Epoxy Adhesive (폴리이미드 표면개질과 에폭시접착제 개질을 통한 폴리이미드/에폭시의 접착력 향상)

  • Kim, Seong-Hun;Lee, Dong-U;Jeong, Gyeong-Ho
    • Korean Journal of Materials Research
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    • v.9 no.1
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    • pp.65-72
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    • 1999
  • In order to minimize flexible printed circuit(FPC), which is used in computer, communication, medical facility, aviation space industry, it is required to improve the interfacial adhesion of polymide/epoxy or polyimide/polyimide consists of FPC. In this study, it was considered to improve the adhesion strength of polyimide/epoxy joint by introducing functional group on polyimide film and improving mechanical property of epoxy. Functional group on polyimide film was introduced by changing polyimide film surface to polyamic acid in KOH aqueous solution. The optimum conditions for surface modification were the concentration of 1M KOH and treatment time of 5min. Also, the optimum adhesion strength of polyimide/epoxy joint was obtained using rubber modified epoxy and polyamic acid as a base resin and curing agent of epoxy adhesive, respectively. The degree of surface modification of polyimide film examined with contact angle measurement of FTIR, thus modification of polyimide to polyamic acid was identified. Fracture surface of plymide/epoxy joint was analyzed by scanning electron microscopy, and modified polyamic acid reimidezed to polymide as increasing curing temperature.

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Optimum Treatment Parameters for Photodynamic Antimicrobial Chemotherapy on Streptococcus mutans Biofilms (Streptococcus mutans biofilm에 대한 광역동 치료의 최적조건에 관한 연구)

  • Choi, Seojung;Park, Howon;Lee, Juhyun;Seo, Hyunwoo;Lee, Siyoung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.42 no.2
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    • pp.151-157
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    • 2015
  • The purpose of this study was to evaluate the effects of Photochemotherapy using a combination of erythrosine and standard halogen dental curing lights on the viability of Streptococcus mutans in the biofilm phase. To investigate the optimum treatment parameters, the researchers controlled the concentration of erythrosine, light irradiation time and the treatment time of erythrosine. The higher concentration of erythrosine (0, 10, 20, 40, 80 M) in the presence of light irradiation created greater effects in reducing the viability of S. mutans. The results showed a statistically significant difference among the antimicrobial effects in 20, 40, 80 M erythrosine. The higher irradiation time of light (0, 5, 15, 30, 60, 75s) in the presence of erythrosine showed greater effects in reducing the viability of S. mutans. There was statistically significant difference in 30, 60, 75 seconds. The higher treatment time of erythrosine (0, 1, 2.5, 5min) in the presence of erythrosine created greater effects on reduction of S. mutans viability. Statistically significant differences were found between 2.5 and 5 minutes of erythrosine treatment time. The results of this study showed that the photochemotherapy on S. mutans using erythrosine and the halogen dental curing lights conventionally used in dental clinics is effective in the condition of 20-40 M erythrosine concentration, irradiation time over 30 seconds, and erythrosine treatment time over 2.5 minutes.

A Study on the Chlorination and Resin Shrink Resist Finish of Wool (양모직물의 염소화/수지 방축 가공에 관한 연구)

  • Lee, Min Koo;Lee, Jae Ho;Jang, Byung Ho
    • Textile Coloration and Finishing
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    • v.3 no.2
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    • pp.1-9
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    • 1991
  • In order to improve the shrink resistance of wool, the fabric was treated with D.C.C.A.(Di-chloro Isocyanuric Acid) and Hercosett. The results obtained as follows, 1. The optimum condition for the shrink resistance of wool fabric was Hercosett concentration of about 2.0~2.5%(o.w.f), pH of 7, the curing temperature of about $140^{\circ}C$, and curing time of 3 minutes. 2. The physical properties with the experimental conditions, such as the tensile strength, bending strengh, crease recovery, tearing strengh were confirmed by measurements.

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Study of the Scorch/Cure time Relationships (스코치/가황시간의 상관관계에 관한 연구)

  • Ryou, Jin-Ho;Kim, Chang-Hee;Oh, Taeg-Su
    • Elastomers and Composites
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    • v.31 no.1
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    • pp.33-42
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    • 1996
  • NR, NBR, and CR rubber were prepared by mixing filler in various ratios. Their vulcanization characteristics and thermal properties were studied. Vulcanization characteristics were investigated using cure curve that had been obtained from oscillating disk rheometer study. The Arrhenius law is known to describe the relationship between cure time and temperature of most elastomers. Curing could be done by the addition of sulfur, peroxides, and proper acceleratores. The optimum cure time that affects desirable values of modulus and tensile strength of the vulcanizate is taken as t90 as measured by a rheometer. Rubbers were cured in the rheometer at temperatures ranging from $130^{\circ}C\;to\;180^{\circ}C$ in order to check the validity of the curing system used. A linear relationship between ln(ts2) and ln(t90) was found for all elastomers. The term sensitivity has been used to describe the relationship between a change of ts2 to the corresponding change of t90 due to an increment of temperature. This is related to the formula of the compound.

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Characteristics of Strength Development of Ultra-High Performance Concrete according to Curing Condition (초고성능 콘크리트의 양생 조건에 따른 강도 발현 특성)

  • Park, Jong-Sup;Kim, Young-Jin;Cho, Jeong-Rae;Jeon, Se-Jin
    • Journal of the Korea Concrete Institute
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    • v.25 no.3
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    • pp.295-304
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    • 2013
  • Ultra-High Performance Concrete (UHPC) has recently been one of the most active research fields in Korea as well as in foreign countries, because it can contribute to a longer life and economic efficiency of structures. Although precast-type UHPC fabricated in a factory is preferable in terms of quality control and reduction of construction period, there exist, even in the precast structure, some parts that need to be cast in-place such as the joints between precast segments. In the cast-in-place UHPC, however, it is probable that an optimum curing condition can hardly be realized in contrast to the factory production. In this study, therefore, the trend of compressive strength development of UHPC was experimentally investigated by assuming various inferior curing conditions that may be anticipated at a construction site. Concrete specimens were fabricated and cured under different conditions with the variables such as curing temperature, delay time before the initiation of curing, duration of curing time and moisture condition. The strengths were compared with those of the specimens cured by standard high temperature steam. Through the analysis of the test results, some minimum requirements for curing have been proposed that are required when the UHPC is cast in-place. It is expected, through this study, that practical use of UHPC in construction sites can be increased.

The Effects of Glycerol Aftertreatment for Low-Formaldehyde Finishing (Glycerol 후처리에 의한 Free-formaldehyde 발생 억제 효과)

  • Choi Suk-Chul;Kim Ho-Jung
    • Journal of the Korean Society of Clothing and Textiles
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    • v.10 no.2
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    • pp.59-67
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    • 1986
  • To control the amounts of formaldehyde released from the cotton fabric finished with N-methylol compounds, glycerol was used as a formaldehyde-scavenging agent. It was observed the effects of catalysts and curing conditions when aftertreated with glycerol on melamine resin finished fabric. The effects of Different processes of glycerol treatment, and different resins, urea resin and melamine resin, were compared. The conclusions obtained from the results are as follows: 1) It was shown hatt the aftertreatment with glycerol (treated without catalyst) was more effective than treated with catalysts in controlling free formaldehyde. 2) The optimum curing temperature and curing time for the glycerol aftertreatment without adversely affecting the other properties of fabric was about $160^{\circ}C$, 3 min. 3) According to the increase of glycerol concentration in both aftertreatment and simultaneous treatment the amounts of free formaldehyde was reduced. The rate of decrease was manifest within the limits of $6\%$ in the case of simultaneous treatment with glycerol ana resins, and $3\%$ in the case of glycerol aftertreatment on resin finished fabrics. 4) Dry wrinkle recovery angle was decreased the increase of glycerol concentration. Melamine resin had a little adverse effect than urea resin, particulary glycerol aftertreatment. 5) The breaking strength was increased with the increase of glycerol concentration.

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Experimental study on the strength behavior of cement-stabilized sand with recovered carbon black

  • Chhun, Kean Thai;Choo, Hyunwook;Kaothon, Panyabot;Yune, Chan-Young
    • Geomechanics and Engineering
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    • v.23 no.1
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    • pp.31-38
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    • 2020
  • Soil-cement stabilization is a type of ground improvement method which has been used to improve the engineering properties of soil. The unconfined compression test is the commonly used method to evaluate the quality of the stabilized soil due to its simplicity, reliability, rapidity and cost-effectiveness. The main objective of this study was to evaluate the effect of recovered carbon black (rCB) on the strength characteristic of cement-stabilized sand. Various rCB contents and water to cement ratios (w/c) were examined. The unconfined compression test on stabilized sand with different curing times was also conducted for a reconstituted specimen. From the test result, it was found that the compressive strength of cement-stabilized sand increased with the increase of the rCB content up to 3% and the curing time and with the decrease of the w/c ratio, showing that the optimum rCB concentration of the tested stabilized sand was around 3%. In addition, a prediction equation was suggested in this study for cement-stabilized sand with rCB as a function of the w/c ratio and rCB concentration at 14 and 28 days of curing.

Effect of Curing Period on Photocatalytic Effect of TiO2 Nanotubes-reinforced Cement Paste (양생기간이 TiO2 나노튜브 보강 시멘트 페이스트의 광촉매 효과에 미치는 영향)

  • Liu, Jun-Xing;Jin, Da-hyung;Bae, Sung-chul
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.11a
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    • pp.172-173
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    • 2021
  • With the development of nano-reinforcement technology and the increasing concern for environmental issues, TiO2 nanomaterials have received wide attention as an additive besides carbon nanomaterials that can be used to enhance the mechanical properties of cement-based materials. Also, TiO2-based materials can allow cement-baned materials with photocatalytic capability, providing a potentially effective approach to reduce environmental problems. In this work, compressive strength, splitting tensile strength, and degradation of methylene blue solution were used as target to assess the effect of TiO2 nanotubes on the mechanical strength and photocatalytic effect of hardened cement paste at different curing time. According to the strength results, the optimum amount of TiO2 was identified as 0.5% of the weight of cement. Meanwhile, the TiO2 nanotubes-reinforced specimen exhibited better photocatalytic effect in the early stage of curing.

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Cure Characteristics, Mechanical Properties, Abrasion Property and Thermal Properties of EVM/EPM Blends Containing Flame Retardants

  • Sung, Il Kyung;Lee, Won Ki;Park, Chan Young
    • Elastomers and Composites
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    • v.52 no.2
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    • pp.105-113
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    • 2017
  • The curing behavior, mechanical properties, hot-air aging resistance, abrasion properties,thermal properties, etc., of EVM/EPM/APP (ammonium polyphosphate)/DPER (dipentaerythritol)/EG (expandable graphite) and EVM/EPM/ATH (aluminium trihydroxide) flame retarding systems in ethylene vinyl acetate rubber (EVM) blends with EPM (ethylene propylene rubber) were sequentially examined. For both flame retarding systems, the torque values increased with the content of EPM rubber and with the vulcanization time. As the content of EPM rubber increased, the scorch time became shorter, whereas the optimum cure time followed an increasing trend. For the EVM/EPM/APP/DPER/EG flameretarding system, as the content of EPM rubber increased, the hardness did not change,whereas the tensile strength and elongation at break decreased. A hot-air aging resistance test at $150^{\circ}C$ showed that the heat resistance decreased with the EPM content regardless of the kinds and contents of flame retardants. As the EPM content increased, the abrasion rate became higher and the abrasion resistance of the EVM/EPM/APP/DPER/EG flame retarding systems exceeded that of the EVM/EPM/ATH flame retarding counterparts. In comparison with the EVM/EPM/ATH flame retarding systems, the thermal stability of the EVM/EPM/APP/DPER/EG flame retarding system showed an increasing tendency.

TEMPERATURE TRANSMISSION OF PAC UNIT THROUGH DENTIN (상아질을 통한 플라즈마 아크 광중합기의 온도 전달)

  • Park, Ho-Won;Kim, Ji-Hun
    • Journal of the korean academy of Pediatric Dentistry
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    • v.30 no.4
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    • pp.707-714
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    • 2003
  • Plasma Arc Curing(PAC) units operate at relatively high intensity and claimed to result in optimum properties of composite resin in a short curing time, so the interest of pediatric dentists about PAC units have been increased recently. But PAC units used for polymerizing restorative resins produce heat during operation. The purpose of this study was to evaluate temperature transmission through dentin of various depths using two types of PAC units(Flipo, Q-Lux plasma 100). The results from the present study can be summarized as follows : 1. When PAC be used continuously, temperature on tip was increased as curing times, and Q-Lux showed greater temperature rising(p<0.001). 2. Compared temperature transmission as dentin depth, temperature rising rate was decreased as dentin thickened(0.5, 1.0, 1.5, 2.0mm)(p<0.05). 3. Compared temperature transmission as resin depth, temperature rising rate was also decreased as resin thickened(1.0, 2.0mm)(p<0.05).

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