• 제목/요약/키워드: Optical Microscopy

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Formation and Characterization of Silicon Carbide Whiskers by Acheson Method (에치슨법에 의한 탄화규소 휘스카의 성장과 특성분석)

  • 주한용;김형준
    • Journal of the Korean Ceramic Society
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    • v.27 no.1
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    • pp.136-146
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    • 1990
  • Whiskers of SiC were grown from the mixture of silica and graphite powders by Acheson method(direct heating method). The structrua, morphological and chemical characterizations have been performed by X-ray diffractometer(XRD), transmission electron microscopy(TEM), optical microscopy(OM), scanning electron microscopy(SEM), X-ray photoelectron spectroscopy(XPS) and energy dispersive spectrometer(EDS). The growth mechanism of SiC whiskers is also discussed.

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INVESTIGATION OF DOMAIN STRUCTURES IN $LiNbO_3$ SINGLE CRYSTALS GROWN BY CZOCHRALSKI METHOD

  • Do, Won-Joong;Kyung Joo;Shin, Kwang-Bo;Auh, Keun-Ho
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.06a
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    • pp.111-114
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    • 1998
  • Lithium Niobate {{{{ { LiNbO}_{ 3} }}}} single crystals grown by Czichralski method at the congruent composition, have ferroelectric microdomains. These microdomins were investigated by chemical etching with hydrofluoric acid (HF) AND NITRIC ACID ({{{{ { HNO}_{3 } }}}}), and by us ing optical microscopy, scanning electron microscopy and atomic force microscopy

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Inspection of Ceramic Coatings Using Nanoindentation and Frequency Domain Photoacoustic Microscopy

  • Steen, T.L.;Basu, S.N.;Sarin, V.K.;Murray, T.W.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.6
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    • pp.390-402
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    • 2006
  • The elastic properties and thickness of mullite environmental barrier coatings grown through chemical vapor deposition (CVD) on silicon carbide substrates were measured using frequency domain photoacoustic microscopy. In this technique, extremely narrow bandwidth surface acoustic waves are generated with an amplitude modulated laser source. A photorefractive crystal based interferometer is used to detect the resulting surface displacement. The complex displacement field is mapped as a function of source-to-receiver distance in order to extract the wavelength of the surface acoustic wave at a given excitation frequency, and the phase velocity is determined. The coatings tested exhibited spatial variations in thickness and mechanical properties. The measured surface wave dispersion curves were used to extract an effective value for the elastic modulus and the coating thickness. Nanoindentation was used to validate the measurements of the effective elastic modulus. The average elastic modulus measured through the coating thickness using nanoindentation is compared to the effective modulus found using the photoacoustic system. Optical microscopy is used to validate the thickness measurements. The results indicate that the photoacoustic microscopy technique can be used to estimate the effective elastic properties in coatings exhibiting spatial inhomogeneities, potentially providing valuable feedback for the optimization of the CVD growth process.

Single Shot White Light Interference Microscopy for 3D Surface Profilometry Using Single Chip Color Camera

  • Srivastava, Vishal;Inam, Mohammad;Kumar, Ranjeet;Mehta, Dalip Singh
    • Journal of the Optical Society of Korea
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    • v.20 no.6
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    • pp.784-793
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    • 2016
  • We present a single shot low coherence white light Hilbert phase microscopy (WL-HPM) for quantitative phase imaging of Si optoelectronic devices, i.e., Si integrated circuits (Si-ICs) and Si solar cells. White light interferograms were recorded by a color CCD camera and the interferogram is decomposed into the three colors red, green and blue. Spatial carrier frequency of the WL interferogram was increased sufficiently by means of introducing a tilt in the interferometer. Hilbert transform fringe analysis was used to reconstruct the phase map for red, green and blue colors from the single interferogram. 3D step height map of Si-ICs and Si solar cells was reconstructed at multiple wavelengths from a single interferogram. Experimental results were compared with Atomic Force Microscopy and they were found to be close to each other. The present technique is non-contact, full-field and fast for the determination of surface roughness variation and morphological features of the objects at multiple wavelengths.

Construction of Langmuir trough and optical properties of phenylhydrazone dye LANGMUIR-BLODGETT films by attenuated total reflection (LANGMUIR-BLODGETT 박막 증착장치 제작 및 전반사감쇠법에 의한 Phenylhydrazone)

  • 고해석
    • Proceedings of the Optical Society of Korea Conference
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    • 1990.02a
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    • pp.193-198
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    • 1990
  • We constructed Langmuir trough for the ultra-thin films (from a few tens {{{{ ANGSTROM }}) of nonlinear optical organic materials. Surface pressure - area isotherm for the tetracosanoic acid which is a fatty acids, was recorded and Langmuir -Blodgett films was deposited using it. The homogenity was investigated using scanning electron microscopy (SEM).

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Study on morphology and OPtical Characteristics of merocyanine dye LB films (Merocyanine dye LB막의 표면이미지 및 광학적 특성 연구)

  • Ryu, Kil-Yong;Park, Sang-Hyun;Park, Jae-Chul;Kwon, Young-Soo
    • Proceedings of the KIEE Conference
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    • 2005.11a
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    • pp.136-138
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    • 2005
  • Merocyanine dye (MD) has been extensively investigated due to its marked potential application to photo-electric devices. We fabricated the number of layers to control its optical characteristics using the Langmuir-Blodgett (LB) method. We evaluated the morphology and optical characteristics of MD LB films using Atomic Force Microscopy (AFM) and UV spectroscopy, PL spectroscopy. As a result, we obtained the quantitative morphology and optical characteristics of LB films from controlling the deposided layers.

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