• Journal of Environmental Science International
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• v.6 no.2
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• pp.183-187
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• 1997

Organophosphate pesticides were extracted with 70% acetone and then transferred to dichloromethane. Extracts were applied to open-column chromatography with florisil. The florial extract was analyzed by gas chromatography with nitrogen-phosphorus detector(GC/NPD). Recoveries of the 18 organophosphate pesticides were ranged from 88.7% to 100. 0% for the narrow-bore capillary GC(Ultra-21. The minimum detectable level of this analytical method was 0.019 - 0.035 mg/kg. Sample throughput(extraction, open-column chro- matography, and GC analysts) was decreased considerably (8h per sample).

• Bulletin of the Korean Chemical Society
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• v.35 no.10
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• pp.3115-3118
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• 2014

• Journal of the Korean Wood Science and Technology
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• v.48 no.6
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• pp.769-779
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• 2020

This study investigates the selective fractionation of lignin with uniform structures and lower molecular weight. Lignin solubilization was first performed using a solution of acetic acid (AA) and hydrogen peroxide (HP) (4:1, (v/v)) to form peracetic acid (PAA), which is a strong oxidant. After the PAA-induced solubilization that occurred at 80℃, totally soluble lignin was extracted by ethyl acetate (EA) and divided into organic- and water-soluble fractions. The EA fraction was then fractionated by open-column using three solutions (chloroform-ethyl acetate, methanol, and water) sequentially. With an increase in the solvent polarity during the fractionation step, the molecular weight of the lignin-derived compounds in the fraction increased. Remarkably, some lignin fractions did not have aromatic structures. These fractions were identified as carboxylic acid-containing polymers like poly-carboxylates. These results conclude that the selective production of lignin-derived polymers with specific molecular weight and structural characteristics could be possible through open-column fractionation.

• Journal of the Korean Society for Marine Environment & Energy
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• v.20 no.2
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• pp.63-75
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• 2017

In offshore environment, an accurate estimation of a wave-structure interaction has been an important issue for safe and cost effective design of fixed and floating offshore structures exposed to a harsh environment. In this study, a wave-structure interaction around a circular column was investigated with regular waves. To simulate 3D two-phase flow, open source computational fluid dynamics libraries, called OpenFOAM, were used. Wave generation and absorption in the wave tank were activated by the relaxation method, which implemented in a source term. To validate the numerical methods, generated Stokes 2nd-order wave profiles were compared with the analytic solution with deep water condition. From the validation test, grid longitudinal and vertical sizes for wave length and amplitude were selected. The simulated wave run-up and wave loads on the circular column were studied and compared with existing experimental data.

• Journal of the Korean housing association
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• v.26 no.6
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• pp.139-146
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• 2015

In this study, the plane type of main building relics of unified Silla period house site which excavated in Gyeongju city after 1990s was classified and the architectural characteristic of them was investigated. The chronology of building relics in Silla capital city site was mostly known as 8-9th century, and by standard of column arrangement, the plane types of them could be classified as grid type, front veranda-grid type, outer column type. The outstanding characteristic of plane is wide span and open front veranda. In most relics the span were over 4 meters, and inner foundations for small post and strip foundation were found between columns. The front veranda added type buildings were composited of enclosed main room and open front veranda, and column arrangement of them dose not fall into line in most case. Thus it thought that the structures of enclosed main room and open front veranda were independent. The interior space of enclosed main room were divided two rooms by partition wall in some case. In this case, one room is enclosed by wall, and the other room has open front side. This plane is considered for the pleasant life in cold winter and hot summer.

• 한국신재생에너지학회:학술대회논문집
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• 2006.11a
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• pp.9-14
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• 2006

Open loop or ground water heat pump systems are the oldest of ground-source systems. Standing column wells can be used as highly efficient ground heat exchanger in geo-thermal heat pump systems, where hydrological and geological conditions are suitable. These systems require some careful considerations for well design, ground water flow, heat exchanger selection etc This paper describes 9round water temperature variations, performances in heat ins and cool ing mode and the results of ground water analysis.

• Journal of the Korean Chemical Society
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• v.45 no.2
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• pp.143-148
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• 2001

In this study, open tubular capillary columns for ion charomatography were developed to analyze trace amount of ions in samples. When small I,D. capillary column length is 1.0~5.0 m. The capillary columns were made using fused silica capillary(I.D:50㎛) and DMEOHA latex particles. The new conductivity cell and suppressor were also developed and made for capillary column ion chromatography. When several anions(fluoride, nitrite, nitale,chlorate,phosphte, sulfate) were analyzed using these capillary columns. reproducible and good chromatograms were obtained.

• Proceedings of the KSR Conference
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• 2011.10a
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• pp.2409-2421
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• 2011

This paper will present hybrid tests to a one bay-one story steel frame structure under ground excitation. A structure used in this paper for hybrid test, to evaluate performance and behavior, is divided into two models; one is numerical model with one column element, and a truss or a beam element, the other is physical substructural model with one beam-column element. All tests considered one or three degrees of freedom to implement real-time hybrid test, and two control algorithms to control hardware are used; one using MATLAB/Simulink, the other using OpenSees, OpenFresco and xPCTarget. In addition, for real-time data communication between numerical and physical substructural models SCRAMNet was used. The results of hybrid tests were compared with one of numerical analysis of numerical model with fiber force-based beam-column elements using OpenSees. Real-time hybrid tests were implemented for the validation of control system with simple structure, and then it will be extended to hybrid test for higher nonlinear or complex structure later on.

• Disaster Prevention Review
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• v.13 no.2
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• pp.30-36
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• 2011

• Clinics in Shoulder and Elbow
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• v.22 no.1
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• pp.29-36
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• 2019

Background: The execution of fibular allograft augmentation in unstable proximal humerus fractures (PHFs) was technically demanding. In this study, the authors evaluated the clinical and radiographic outcomes after tricortical iliac allograft (TIA) augmentation in PHFs. Methods: We retrospectively assessed 38 PHF patients treated with locking-plate fixation and TIA augmentation. Insertion of a TIA was indicated when an unstable PHF showed a large cavitary defect and poor medial column support after open reduction, regardless of the presence of medial cortical comminution in preoperative images. Radiographic imaging parameters (humeral head height, HHH; humeral neck-shaft angle, HNSA; head mediolateral offset, HMLO; and status of the union), Constant score, and range of motion were evaluated. Patients were grouped according to whether the medial column support after open reduction was poor or not (groups A and B, respectively); clinical outcomes were compared for all parameters. Results: All fractures healed radiologically (average duration to complete union, 5.8 months). At final evaluation, the average Constant score was 73 points and the mean active forward flexion was $148^{\circ}$. Based on the Paavolainen assessment method, 33 patients had good results and 5 patients showed fair results. The mean loss of reduction was 1.32 mm in HHH and 5.02% in HMLO. None of the parameters evaluated showed a statistically significant difference between the two groups (poor and not poor medial column support). Conclusions: In unstable PHFs, TIA augmentation can provide good clinical and radiological results when there are poor medial column support and a large cavitary defect after open reduction.