• Title/Summary/Keyword: One-pot

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Characterization of a Unique New Strain Named the NFRDI N°1 Rotifer Strain, a Brackish Brachionus Rotifer Collected from a South Korea Coastal Lagoon

  • Jung, Min-Min
    • Fisheries and Aquatic Sciences
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    • v.14 no.4
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    • pp.333-337
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    • 2011
  • A new and a unique Brachionus rotifer was found in Hwajinpo coastal lagoon in Gangwon Province, South Korea. This Brachionus certainly originated from the wild rather than from aquaculture stations because Hwajinpo coastal lagoon has been under rigorous control as a military protected area and therefore could not have been contaminated by aquaculture stations. The new strain was identified as Brachionus rotundiformis based upon its morphological characteristics. The parthenogenetic female of this new rotifer strain typically shows characters similar to those of B. rotundiformis, such as the pot shape of the body, rounded dorsal plate compared with flattened ventral plate, elliptical mictic egg, four frontal spines, six pointed occipital spines, non-nodal foot, two toes, trophi typical of the Brachionus genus with five uncus plates resembling comb teeth, one wide symmetrical manubrium and ramus, and no stiffened spine as is seen in freshwater Brachionus rotifers. Moreover, its lorica was rather small in size compared with other common rotifer strains that serve as live-food organisms (Guam, Thai, and Bali strains). This new and unique Korean brackish rotifer, a B. rotundiformis strain, was therefore named the National Fisheries Research and Development Institute (NFRDI) $N^{\circ}1$ rotifer strain.

The historical study of Lamb Cooking in Korea (우리나라 양육(羊肉) 조리법(調理法)의 역사적(歷史的) 고찰(考察))

  • Kim, Tae-Hong
    • Journal of the Korean Society of Food Culture
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    • v.9 no.1
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    • pp.23-41
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    • 1994
  • In this study kinds of Lamb cooking and preservation and the ingredients of lamb cooking are surveyed through the references written from 1670 to 1943. The lamb cooking found in the literature totaled to more than 53. They can be classified into fourteen different groups according to their processing features which as follows: Salnum and Pyunyuk(boiled and slices of boiled), Kui(roasted), Chim(steamed), Whe(raw meat), Hounjae(smoking), Po(dried), Juk(gruel), Tang(soup), Sundae(stuffed small interstines), Jokpyun(jellied foot), Jungol(happiness pot), Sikhae(salt+meat+malt), Oumjang(salted meat), Kunjo(dried). Korean lamb cooking methods were primarily adopted from Mogolia in late Korea Dynasty but they had unique characteristics different from Mongolian ones. Furthermore, they were creatively applied to other meat cooking such as beef, pork and dog. About twenty one ingredients were mainly used in lamb cooking, including fresh meat, ribs, breast, heart, liver and the like. In particular, most popularly used ones were fresh meat and the heart in internal organs, which coincide with the main ingredients in beef cooking of today. The number of seasoning used in lamb cooking was twelve and especially salt, vineger, ginger and stone leek were most commonly used ones. Fourteen other addition were put into lamb cooking and the rice(Korean) wine was the most frequently used addition.

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The controllable fluid dash pot damper performance

  • Samali, Bijan;Widjaja, Joko;Reizes, John
    • Smart Structures and Systems
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    • v.2 no.3
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    • pp.209-224
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    • 2006
  • The use of smart dampers to optimally control the response of structures is on the increase. To maximize the potential use of such damper systems, their accurate modeling and assessment of their performance is of vital interest. In this study, the performance of a controllable fluid dashpot damper, in terms of damper forces, damper dynamic range and damping force hysteretic loops, respectively, is studied mathematically. The study employs a damper Bingham-Maxwell (BingMax) model whose mathematical formulation is developed using a Fourier series technique. The technique treats this one-dimensional Navier-Stokes's momentum equation as a linear superposition of initial-boundary value problems (IBVPs): boundary conditions, viscous term, constant Direct Current (DC) induced fluid plug and fluid inertial term. To hold the formulation applicable, the DC current level to the damper is supplied as discrete constants. The formulation and subsequent simulation are validated with experimental results of a commercially available magneto rheological (MR) dashpot damper (Lord model No's RD-1005-3) subjected to a sinusoidal stroke motion using a 'SCHENK' material testing machine in the Materials Laboratory at the University of Technology, Sydney.

Facile Synthesis of Dendritic Benzyl Chlorides from Their Alcohols with Methanesulfonyl Chloride/$Et_3N$ (덴드리틱 벤질 클로라이드의 효율적인 합성)

  • Lee, Jae-Wook;Han, Seung-Choul;Kim, Hee-Joo;Kim, Jung-Hwan;Lee, Un-Yup;Kim, Byoung-Ki;Sung, Sae-Reum;Kang, Hwa-Shin;Kim, Ji-Hyeon;Huh, Do-Sung
    • Polymer(Korea)
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    • v.31 no.5
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    • pp.417-421
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    • 2007
  • A successful rapid synthesis of dendritic benzyl chlorides from dendritic benzyl alcohols using methanesulfonyl chloride/$Et_3N$ as activating agents was described. In this method, each dendritic benzyl chloride can be prepared in one pot: no isolation of intermediate mesylated dendrons is required. The key steps in the syntheses of dendritic benzyl chlorides were the mesylation of the hydroxymethyl group followed by the chlorination by in-situ generated triethylammonium chloride.

Green Synthesis of Ag Thin Films on Glass Substrates and Their Application in Surface-Enhanced Raman Scattering

  • Cho, Young Kwan;Kim, In Hyun;Shin, Kuan Soo
    • Bulletin of the Korean Chemical Society
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    • v.34 no.10
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    • pp.2942-2946
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    • 2013
  • Nanostructured Ag thin films could be facilely prepared by soaking glass substrates in ethanolic solutions containing $Ag_2O$ powders at an elevated temperature. The formation of zero-valent Ag was corroborated using X-ray diffraction and X-ray photoelectron spectroscopy. The deposition of Ag onto a glass substrate was readily controlled simply by changing the reaction time. Due to the aggregated structures of Ag, the surface-enhanced Raman scattering spectra of benzenethiol could be clearly identified using the Ag-coated glass. The enhancement factor at 514.5 nm excitation estimated using benzenethiol reached $1.0{\times}10^5$ while the detection limit of rhodamine 6G was found to be as low as $1.0{\times}10^{-13}$ M. Since this one-pot fabrication method is eco-friendly and is suitable for the mass production of diverse Ag films, it is expected to play a significant role in the development of surface plasmon-based analytical devices.

New Antibiotics Produced by Streptomyces melanosporofaciens II. Antimicrobial Activities and Isolation, Purification, and Structure Determination of the Active Compound (Streptomyces melanosporofaciens가 생산하는 새로운 항생물질 II. 물질의 항균활성과 황성물질의 분리.정제 및 구조결종)

  • 김시관;김상석;김근수;정영륜;김창한
    • Microbiology and Biotechnology Letters
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    • v.19 no.3
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    • pp.235-241
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    • 1991
  • - A phthalic acid derivative and basic macrolide antibiotics, with antimicrobial activity against Gram positive bacteria and phytopathogenic fungi, respectively, were found to be produced by a strain 88-GT-161 identified as being a variety of Streptomyces melanosporofaciens. This paper describes an isolation procedure of the active compounds produced by this strain, their in vitro and in vivo (pot test) antimicrobial activites, and structure determination of one of the compounds, bis (2-ethylhexyl) phthalate, a phthalic acid derivative antibiotic. This compounds, upon cornparision with authentic bis (2-ethylhexyl) phthalate, dioctyl phthalate, revealed a difference in antimicrobial activity even though physico-chemical properties of these two compounds seemed indentical. This is the first report that dioctyl phthalate is biosynthetically produced by a Streptomyces sp. and shows antimicrobial activity.

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Reduction of floating Dross in the Zinc Bath (도금욕 부유드로스의 감소)

  • Chang, Seky
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 1999.05a
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    • pp.97-97
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    • 1999
  • Dross formation in the zinc bath is inevitable under any condition as long as coating process on steel strip continues. Thus, bath aluminum and temperature are precisely managed to suppress the increase of dross. Also, excessive dross for normal coating process is generally eliminated physically by bubbling and skimming. Total amount of dross in the bath can be sometimes high enough to cause coating defect. On the other hand, local concentration of dross can make coating defect even with satisfactory level of total amount of dross. Reduction of dross in the bath was attempted by using ceramic foam filter made of mainly alumina. Dross in molten zinc was almost reduced to the levels of solubility of iron and aluminum in molten zinc at $450~460^{\circ}C$. Their solubility levels were confirmed by thermodynamic calculations or DEAL program. Two kinds of filters were tested for dross reduction. One was #20 ppi, porous per inch, and the other #30 ppi filter. Both were effective in reducing the bath dross to the solubility levels at the static state. Bath iron was reduced by 24 wt% and 19 wt% with #20 filter, and by 35 wt% and 29 wt% with #30 filter for GI and GA pot, respectively. Also, ceramic foam filter did not make any harm to the zinc bath composition after filtering test.

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Synthesis of Naphthacenone Derivatives Using a Michael Reaction (Michael 반응을 이용한 Naphthacenone 유도체의 합성)

  • Rho, Young S.;Yoo, Jin H.;Park, Si H.;Cho, In H.;Kwon, Yoon J.
    • Journal of the Korean Chemical Society
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    • v.40 no.7
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    • pp.519-525
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    • 1996
  • 3-Carbomethoxy-1(3H)-isobenzofuranone(9) underwent condensation with ${\alpha}{\beta}-unsaturated$, esters 3a-b to produce the corresponding naphthacene-6,7-diones 11a-b with high yields in one pot procedure. Among the naphthacene-6,7-diones formed, compound 11a without an ethyl group at C-9 position was oxidized to give the naphthacene-5,12-dione 13a, while compound 11b containing the ethyl group was oxidized to give a 3:2 mixture of the naphthacene-5,7,12-trione 12b and naphthacene-5,12-dione 13b under the same experimental conditions.

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One-pot synthesis of gold trisoctahedra with high-index facets

  • Kim, Do Youb;Choi, Kyeong Woo;Im, Sang Hyuk;Park, O Ok;Zhong, Xiao-Lan;Li, Zhi-Yuan
    • Advances in materials Research
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    • v.1 no.1
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    • pp.1-12
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    • 2012
  • There have been many efforts on the generating metal nanocrystals enclosed by high-index facets for the use as highly active catalysts. This paper describes a facile synthesis of Au trisoctahedra with high-index facets. In brief, the Au trisoctahdra were prepared by reduction of $HAuCl_4$ in N,N-dimethylformamide (DMF) containing poly (vinyl pyrrolidone) (PVP) and trace amount of $AgNO_3$. The Ag ions in the reaction solution played a critical role in controlling the trisoctahedral shape of the final product by underpotential deposition (UPD) on the Au surfaces. The as-prepared Au trisoctahedra were single crystal and enclosed by high-index {441}, {773} and {331} facets.

The Synthesis of CuInS2 Nanoparticles by a Simple Sonochemical Method

  • Park, Jae-Young;Park, Jong-Pil;Hwang, Cha-Hwan;Kim, Ji-Eon;Choi, Myoung-Ho;Ok, Kang-Min;Kwak, Ho-Young;Shim, Il-Wun
    • Bulletin of the Korean Chemical Society
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    • v.30 no.11
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    • pp.2713-2716
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    • 2009
  • $CuInS_{2}$ nanoparticles were synthesized by a simple sonochemical method; First, Cu nanoparticles were prepared from $CuInS_{2}$ in methanol solution by a one pot reaction through the sonochemistry under multibubble sonoluminescence (MBSL) conditions. Second, the resulting Cu nanoparticles were treated with $InCl_3{\cdot}4H_2O$ and $CH_3CSNH_2$ (thioacetamide) at the same MBSL conditions to synthesize $In_2S_3$-coated Cu nanoparticles in methanol solution. Then, they were transformed into $CuInS_{2}$ (CIS) nanoparticles of 20 $\sim$ 40 nm size in diameter by thermal heating at 300 ${^{\circ}C}$ for 2 hr. The prepared CIS nanoparticles, of which band gap is 1.44 eV, were investigated by X-ray diffractometer, UV-Vis spectrophotometer, inductively coupled plasma spectrometer, and high resolution-transmission electron microscope.