• Title/Summary/Keyword: Odor fingerprint

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Applicability Investigation for the Odor Source Tracking Approach using the Wind Field and the Fingerprinting (바람장 및 Fingerprint를 이용한 악취추적기법 활용가능성 평가)

  • Na, Kyung-Ho;Bak, Yong-Chul;Jang, Young-Gi
    • Journal of Korean Society for Atmospheric Environment
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    • v.23 no.1
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    • pp.1-13
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    • 2007
  • This study was carried out to evaluate the applicability of the odor source tracking using wind field and fingerprint as a solution tool. First of all, CALMET and HYSPLIT modeling system, and database of odor discharge companies were utilized to track odor from industrial complexes. Secondly, industrial odor fingerprint was made by listing on the 19 domestic industries, and compared with foreign data to assess the representative, and thus the similarity was 86.7%. On the modeling experiment, Sihwa industrial complex did not show any difference because the matching rates of day and night were 49.5% and 50.0%, respectively. However, the Banwol and Sihwa industrial complexes did show some differences due to odor facility density. Separately, in this study, odor samples were obtained from 10 odor discharging companies, located in the Sihwa and Banwol industrial complexes, They were compared with the results of odor tracking modeling. The matched companies were 4 of 10 by three cases of tracking, while the fingerprint and industry of odor monitoring networks and companies matched each other. Therefore, this study confirmed the approach applicability of source tracking system using the fingerprint.

Development of Standard Operating Procedures (SOPs), Standardization, TLC and HPTLC Fingerprinting of a Polyherbal Unani Formulation

  • Naaz, Arjumand;Viquar, Uzma;Naikodi, Mohammad Abdul Rasheed;Siddiqui, Javed Inam;Zakir, Mohammad;Kazmi, Munawwar Husain;Minhajuddin, Ahmed
    • CELLMED
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    • v.11 no.4
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    • pp.21.1-21.9
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    • 2021
  • Background: Unani System of Medicine (USM) has its origin to Greece. To ensure and develop the quality, authenticity of Unani drugs, standardization on modern analytical parameter is essential requirement for drugs. Objectives: The aimed of the present study was to develop a standard profile of "Qurṣ-e-Mafasil" by systematic study through authenticated ingredients, pharmacognostic identification followed by physicochemical, TLC, HPTLC fingerprinting analysis as per standard protocol. Material and Methods: In this study three batches of "Qurṣ-e-Mafasil" QM were prepared by standard method as per UPI had been followed by organoleptic properties of formulation such as appearance, color, odor, taste. Powder Microscopy and physicochemical studies were carried out such as Uniformity of weight, Friability, Disintegration time, hardness, LOD, ash vales and extractive values in like aqueous, alcohol & hexane. Further qualitative tests such as Thin-Layer Chromatography (TLC), and High-Performance Thin Layer Chromatography (HPTLC) studies were also carried out to develop fingerprint pattern of the alcoholic solvent extract of QM. Phytochemical screening was carried out in different solvent extracts such as alcoholic, aqueous and chloroform extracts to detect the presence phytoconstituents in the formulation QM. Heavy metals, Microbial Load Contamination and pesticidal residues were also determined. Results: Qurṣ-e-Mafasil showed tablet-like appearance, light brown colour, mild pungent odour and acrid taste. Uniformity of weight (mg), friability (rpm), and hardness (kg/cm) and disintegration time was ranged between (500 to 503), (0.0340 to 0.038), (8.40 to 8.67) and (4-5 minutes) respectively for the three batches. Loss in weight on drying at 105℃ was ranged between (8.3425 to 8.7346). Extracted values were calculated in distilled water ranged between (30.9091 to 31.4358), hexane (1.1419 to 1.4281), and alcohol (3.3352 to 3.3962). The ash values recorded were ranged between (3.7336 to 3.8378), and acid insoluble ash (0.5859 to 0.6112).

Characterization of Volatile Compounds in Donkey Meat by Gas Chromatography-Ion Mobility Spectrometry (GC-IMS) Combined with Chemometrics

  • Mengmeng Li;Mengqi Sun;Wei Ren;Limin Man;Wenqiong Chai;Guiqin Liu;Mingxia Zhu;Changfa Wang
    • Food Science of Animal Resources
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    • v.44 no.1
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    • pp.165-177
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    • 2024
  • Volatile compounds (VOCs) are an important factor affecting meat quality. However, the characteristic VOCs in different parts of donkey meat remain unknown. Accordingly, this study represents a preliminary investigation of VOCs to differentiate between different cuts of donkey meat by using headspace-gas chromatography-ion mobility spectrometry (HS-GC-IMS) combined with chemometrics analysis. The results showed that the 31 VOCs identified in donkey meat, ketones, alcohols, aldehydes, and esters were the predominant categories. A total of 10 VOCs with relative odor activity values ≥1 were found to be characteristic of donkey meat, including pentanone, hexanal, nonanal, octanal, and 3-methylbutanal. The VOC profiles in different parts of donkey meat were well differentiated using three- and two-dimensional fingerprint maps. Nine differential VOCs that represent potential markers to discriminate different parts of donkey meat were identified by chemometrics analysis. These include 2-butanone, 2-pentanone, and 2-heptanone. Thus, the VOC profiles in donkey meat and specific VOCs in different parts of donkey meat were revealed by HS-GC-IMS combined with chemometrics, whcih provided a basis and method of investigating the characteristic VOCs and quality control of donkey meat.