• Title/Summary/Keyword: Nitrogen pressure

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The Effect of Chamber Pressure and Nitrogen Flow Rate on Deposition Characteristics of $(Ni_{0.8}Fe_{0.2})_{20}Ag_{80}$ Thin Films

  • Oh, T.S.;Choo, W.K.
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1997.06a
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    • pp.275-280
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    • 1997
  • We have investigated the deposition characteristics of (Ni0.8Fe0.2)20Ag80 thin films as a function of chamber pressure and nitrogen flow rate with scanning electron microscopy(SEM), atomic force microscopy(AFM), XRD and $\alpha$-step. The deposition rate of these film is decreased with increasing the chamber pressure and the nitrogen flow rate. With raising the chamber pressure, the growth mode of thin film is changed from island growth to columnar one, which is probably due to energy of atom. Contrary, the nitrogen flow rate is raised, growth mode is changed from columnar to island one. According to the XRD patterns, the preferred orientation is inhibited as the nitrogen flow rate is kept above 10 sccm, but that is nearly independent on the chamber pressure. When the chamber pressure decrease or the nitrogen flow rate increase, phase separation into permoally and silver is occured.

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The Effect of Initial Partial Pressure of Nitrogen on the Manufacturing of Reaction-Bonded Silicon Nitride (반응결합 질화규소의 제조의 있어서 초기 질소분압의 영향)

  • 이근예;이준근;오재희
    • Journal of the Korean Ceramic Society
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    • v.21 no.1
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    • pp.51-59
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    • 1984
  • In this paper mechanical properties of reaction-bonded silicon nitride are studied with the variation of initial nitrogen partial pressure. At 1, 25$0^{\circ}C$ the amount of nitridation and the nucleation of nitride increase linearly with the nitrogen partial pressure increase. After the nitridation is completed the density of nitride and modulus of rupture at room temperature are increased with the amount of nitridation. When the partial pressure of nitrogen is 0.5 atm the specimen show the optimum properties that is the highest density of nitride and modulus of rupture. Also the microstructure of $\alpha$-matte is deveoped very well at that pressure of nitrogen which contributes to the strength development of specimen. It is shown that with proper control of initial partial pressure of nitrogen high strength silicon nitride body can be manufactured for dynamic applications.

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Effect of pressure and temperature on bulk micro defect and denuded zone in nitrogen ambient furnace

  • Choi, Young-Kyu;Jeong, Se-Young;Sim, Bok-Cheol
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.26 no.3
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    • pp.121-125
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    • 2016
  • The effect of temperature and pressure in the nitrogen ambient furnace on bulk micro defect (BMD) and denuded zone (Dz) is experimentally investigated. It is found that as pressure increases, Dz depth increases with a small decrease of BMD density in the range of temperature, $100{\sim}300^{\circ}C$. BMD density with hot isostatic pressure treatment (HIP) at temperature of $850^{\circ}C$ is higher than that without HIP while Dz depth is lower due to much higher BMD density. As the pressure increases, BMD density is increased and saturated to a critical value, and Dz depth increases even if BMD density is saturated. The concentration of nitrogen increases near the surface with increasing pressure, and the peak of the concentration moves closer to the surface. The nitrogen is gathered near the surface, and does not become in-diffusion to the bulk of the wafer. The silicon nitride layer near the surface prevents to inject the additional nitrogen into the bulk of the wafer across the layer. The nitrogen does not affect the formation of BMD. On the other hand, the oxygen is moved into the bulk of the wafer by increasing pressure. Dz depth from the surface is extended into the bulk because the nuclei of BMD move into the bulk of the wafer.

Characterization of Nitrogen Gas Crossover in PEM Fuel Cell Stacks (고분자 연료전지 스택에서 질소 크로스오버 특성에 관한 연구)

  • Baik, Kyung-Don;Kim, Min-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.33 no.3
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    • pp.207-214
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    • 2009
  • Crossover of nitrogen from cathode to anode is inevitable in typical membranes used in PEM fuel cells. This crossovered nitrogen normally accumulates in the hydrogen recirculation system at anode side channels. Excessive buildup of nitrogen in the anode side lowers the relative hydrogen concentration and finally affects the performance of fuel cell stack. So it is very important to analysis the nitrogen gas crossover at various operating conditions. In this study, characterization of nitrogen gas crossover in PEM fuel cell stack was investigated. The mass spectroscopy (MS) has been applied to measure the amount of the crossovered nitrogen gas at the anode exit. Results show that nitrogen gas crossover rate was affected by current density, anode and cathode stoichiometric ratio and operating pressure. Current density, anode stoichiometric ratio and anode operating pressure do not affect nitrogen crossover rate but anode exit concentration of nitrogen. Cathode pressure and stoichiometric ratio largely affect the nitrogen crossover rate.

The Study on Emission Spectrum Characteristics of Atmosphere Pressure Plasma (상압 플라즈마의 광 방출 스펙트럼 특성조사에 관한 연구)

  • Park, Sung-Jin
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.27 no.2
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    • pp.77-83
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    • 2013
  • In this study, we aimed to determine the optical properties of the plasma used for the dry cleaning method. The optical properties of the atmospheric pressure plasma device were measured through the degree of ionization of hydrogen or nitrogen gas by ionized atmospheric gas. The degree of ionization of hydrogen or nitrogen is closely associated with surface modification. We observed through our experiments that argon gas, an atmospheric gas, caused an increase in the ionization of nitrogen gas, which has similar ionization energy. This type of increase in nitrogen gas ions is believed to affect surface modification. The results of our study show that the pressure of argon gas and the partial pressure of argon and nitrogen gases lead to different results. This important result shows that argon ions can affect the ionization of nitrogen gas.

Effects of Pressure on the Breakdown Characteristics of Cryogenic Liquid and Gaseous Nitrogen (극저온 액체 및 기체 질소의 압력에 따른 절연파괴 특성)

  • 백승명;정종만;김상헌
    • Progress in Superconductivity and Cryogenics
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    • v.4 no.2
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    • pp.1-4
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    • 2002
  • Electrical properties of liquid nitrogen ($LN_2$) and gaseous nitrogen($GN_2$) have become of great interest again since the discovery of high temperature superconductors . It is very important from a point of superconducting apparatus protection to elucidate breakdown characteristics in $LN_2$ and $GN_2$ at atmospheric and pressurized conditions Therefore. this paper studies the effect of pressure on the breakdown characteristics in $LN_2$ and $GN_2$. Af high voltage is applied to electrode system with uniform and non-unform field in various gap length. And Breakdown voltages of $LN_2$ and $GN_2$ are investigated under AC voltage for Pressure ranging from 0 and 0.5 MPa. This research presented basis information of electrical insulation design for liquid nitrogen immersed HTS power apparatus.

Extinguishing of Oil Fire by Water Mist Suppression System Using Compressed Inert Gas (불활성 압축가스를 이용한 미세물분무 소화시스템의 유류화재 소화특성)

  • Shin, Chang-Sub;Jeon, Go-Un;Kim, Ki-Whan
    • Journal of the Korean Society of Safety
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    • v.25 no.6
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    • pp.109-114
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    • 2010
  • Water mist fire suppression system is environmental system and needs a flange pump to jet water. In this research, high pressure Nitrogen cylinder is used as a pressurizing source instead of flange pump, and also we tried to find the possibility of using compressed Nitrogen as a fire suppression agent. As a result, it was possible to design water mist fire suppression system with Nitrogen cylinder and suppress oil fire effectively. With DK1.58 nozzle, the optimum Nitrogen pressure was 80bar and the pressure was stable during water mist spray. However, jet of Nitrogen was not effective fire suppression agent when it was dually used with water mist because water mist has blown away, and it is efficient way to use compressed Nitrogen as a pressurizing source only.

Effect of Nitrogen Gas Pressure on the Property of TiN-Coated Layer of High Speed Steel by Arc ion Plating (AIP 법에서 질소가스 압력이 고속도강의 TiN 코팅층 성질에 미치는 영향)

  • Kim, Hae-Ji;Joun, Man-Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.25 no.7
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    • pp.124-130
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    • 2008
  • The effect of nitrogen gas pressure in arc ion plating on surface properties of the TiN-coated high speed steel(SKH51) is presented in this paper. The surface roughness, micro-particle, micro-hardness, coated thickness, atomic distribution of TiN, and adhesion strength are measured fur various nitrogen gas pressures. It has been shown that the nitrogen gas pressure has a considerable effect on the surface roughness, adhesion strength, atomic distribution of TiN, and surface deposition of TiN of the high speed steels but that it has little influence on the micro-hardness and coated thickness.

Effect of Nitrogen Gas Pressure on the Mechanical Properties of Polymer Composite Materials (고분자 복합재료의 기계적 물성에 미치는 질소기압의 영향)

  • Kim, Bu-An;Hwang, Hyun-Young;Kang, Suk-Jun;Moon, Chang-Kwon
    • Journal of Power System Engineering
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    • v.20 no.5
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    • pp.14-19
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    • 2016
  • This study is about the effect of nitrogen gas pressures during manufacturing process on the mechanical properties of composite materials. $TiO_2$/epoxy resin nanocomposites and carbon fiber reinforced epoxy resin(CFRP) composites were fabricated under various nitrogen gas pressures. Tensile strength test, vicker's hardness test and fracture surface observation were carried out to investigate the effect of nitrogen gas pressure. As a result, the tensile strength of nanocomposite and CFRP composites showed clearly increasing tendency by a change in the nitrogen gas pressure up to 3.0 atm and then the tensile strength decreased a little. However, the vicker's hardness of $TiO_2$/epoxy nanocomposites showed same hardness values regardless of the nitrogen gas pressures.

Construction of High-Pressure Pressurized Liquid Nitrogen Supply Facilities (고압의 가압식 액체질소 공급 설비 구축)

  • Shin, Minkyu;Oh, Jeonghwa;Kim, Seokwon;Ko, Youngsung;Chung, Yonggahp
    • Journal of Aerospace System Engineering
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    • v.14 no.5
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    • pp.26-32
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    • 2020
  • In this study, a facility was constructed to supply liquid nitrogen to simulate combustion instability in a liquid rocket combustor. The pressurization and supply performances were predicted and verified through different experiments. The liquid nitrogen supply system was composed of a pressurized supply system, and a dome regulator was used to adjust the pressure of the pressurant. A cavitation venturi was used to control the mass flow rate of liquid nitrogen. The condition of liquid nitrogen supply was a mass flow rate of 2.55 kg/s and the venturi inlet pressure was above 100 bar. Based on the initial experiment, it was observed that the predicted amount of the pressurant was not sufficiently supplied and the target pressure was not supplied due to a drop in tank pressure. Through the modification of the established facilities, the target mass flow rate was successfully supplied and the cryogenic liquid nitrogen supply facility was verified.