• 한국기계가공학회지
• /
• 제15권6호
• /
• pp.77-82
• /
• 2016

When drilling through Inconel 601 nickel-chromium-based alloys, a large amount of cutting oil is required to prevent tools from wear and fracturing due to heat buildup resulting from the high temperature resistance and toughness of this alloy. However, cutting oil supply has become a factor compromising the machining environment, and this has caused attention to shift to a more environmentally friendly cutting fluid supply system called minimum quantity lubrication (MQL). Our aim in this study was to find a more efficient drill processing method using MQL, and to verify its performance. To that end, we proposed a sealed cover, a step feed, and POSS-type cutting oil as measures to increase the effectiveness of MQL in view of the cutting force and tool wear, and established an improvement in efficiency using the proposed measures.

• 대한치과교정학회지
• /
• 제31권2호통권85호
• /
• pp.271-281
• /
• 2001

치아에 부착된 bracket이 교정선을 따라 이동할때 필연적으로 bracket과 교정선, 결찰재 사이에 마찰력이 발생된다. 이에 저자는 동일한 bracket내에서 교정선의 종류, 결찰방법, 건조와 타액상태에 따른 마찰력 차이, 타액의 윤활제로서의 기능을 살펴보기 위해 본 연구를 시행하게 되었다. 본 실험에 사용된 bracket은 .18" ${\times}$ .025" slot의 상악 견치용 standard edgewise bracket(RMO. USA)이며, 교정선은 .016" , .016" ${\times}$ .022" 크기의 Cobalt-chromium(Elgiloy : RMO. USA), Nickel-titanium(Ni-Ti) (ORTHOLLOY : Goldstar Cable Co. KOREA), Beta- titanium(TMA : ORMCO Co., USA)의 2가지 형태의 3종을 이용하여 활주할 때의 마찰력을 만능시험기(Instron, M 1000 EC)를 사용하여 계측하여 다음과 같은 결론을 얻었다. 1. 각각의 동일조건하에서 교정선의 재질에 따른 마찰력은 Co-Cr, Ni-Ti, ${\beta}$-Ti순으로 증가하였다. 단, 타액상태에서 elastomeric으로 결찰한 .016" 군에서는 예외이다. 2. 각 조건하(건조/타액상태, .016" /.016" ${\times}$.022" ) 에서 결찰방법에 따른 마찰력은 elastomeric보다 stainless steel결찰에서 더 크게 나타났다(p<0.05). 3. 각각의 교정선과 결찰방법에서 타액 유무에 따른 마찰력은 stainless steel로 결찰한 .016" Co-Cr, Ni-Ti, ${\beta}$-Ti는 타액상태에서 감소하나, stainless steel로 결찰한 .016" ${\times}$.022" Co-Cr, Ni-Ti, ${\beta}$-Ti는 타액상태에서 증가하였다(p<0.05). 4. 각 조건하(건조/타액상태, elastomeric/stainless steel 결찰) .016" 과 .016" ${\times}$.022" 교정선 사이의 마찰력은 .016" ${\times}$.022" 교정선에서 증가하였다(p<0.05).

• 수산해양기술연구
• /
• 제27권2호
• /
• pp.132-140
• /
• 1991

오스테나이트계 스테인레스강 SUS316, SUS321 보다 용접성, 내식성 및 극저온인성이 양호하며 기존의 재료보다 고가 첨가 원소인 크롬과 니켈의 함유량을 절감한 새로운 강종의 개발을 목표로 연구를 수행한 결과, 다음과 같은 결론을 얻었다. 1) Trans-Varestraint 시험에 의하여 용해 제조강과 수입개의 고온 균열 감수성을 비교 평가한 결과, SUS321 수입재와 SuS321에 대응하여 개발한 강종 사이의 응고 균열 감수성이 거의 동등 내지는 용해 제조강의 고온 균열 저항력이 우수하였다. 따라서 Creq/Nieq의 값 1.43~1.48의 범위에서 합금 설계한 강종 M-1~M-9의 고온 균열 저항력은 기존의 문헌에 의한 테이타와 비교한 결과, 우수함을 알 수 있었다. 2) 샤르피(Charpy V notch) 표준 시험편에 의한 극저온 및 상온에서의 인성을 조사한 결과, 용해 제조강 M-1~M-9의 인성은 양호하였으며 특히 SUS321 수입재와 SUS321 대체재로서 개발한 M-7~M-9의 인성은 수입재의 그것보다 훨씬 높은 값을 나타내었다. 3) JIS G 0574에 의한 입계 부식 감수성을 조사한 결과, 입계 부식 감수성을 낮추기 위해서는 티타늄의 첨가가 매우 유효함을 알 수 있었다. 특히 SUS321 수입재와 SUS321 대응 강종(M-7~M-9)의 내식성은 수입재보다 개발 강종의 내식성이 훨씬 우수하였다. 4) 이상의 고온 균열 감수성과 극저온 및 상온에서의 인성, 내식성을 종합적으로 검토한 결과, 스테인리스강의 고가 첨가 원소인 크롬과 니켈의 첨가량을 절감할 수 있었다. 상기와 같은 관점에서 본 연구 수행에 의하여 새로운 합금 설계 개념에 의거, 새로운 강종의 개발과 생산 원가의 절감 그리고 제품의 품질 향상에 기여할 수 있는 기준을 확립할 수 있었다.

• 대한소아치과학회지
• /
• 제27권2호
• /
• pp.274-282
• /
• 2000

소아의 유구치 수복에 흔히 사용하는 stainless steel crown은 주성분으로 $70\sim90%$의 니켈과 $5\sim15%$의 크롬을 함유하고 있다. 이 중 니켈 자체가 일으킬 수 있는 allergy반응이나 발암성등의 부작용이 성인에서는 활발하게 연구되고 있으며, 특히 니켈이 포함된 합금을 이용한 보철물 주변에 병원성이 있는 니켈내성 Enterococci가 존재한다는 보고가 있어 성인과는 구강환경이 다른 소아에서도 stainless steel crown 주변에 니켈내성균주가 존재하는지를 확인하고자 이 실험을 시행하였다. 유구치에 stainless steel crown(Anatom primary crown, Sankin)을 6개월 이상 장착한 환자 15명과 유구치 협면에 치아우식증이 없는 환자 15명의 치은열구액에서 채취한 시료를 BHI 한천배지, 니켈배지 및 Bile-esculin azide(BEA) 한천 배지에 도말하였다. BEA한천배지에서 자란 enterococci를 니켈내성정도를 확인하기위해 3, 5, 10, 30, 50mM 니켈배지에 접종한후 성장상태를 관찰하였다. 실험군에서는 BHI 한천배지에서 507,350개의 균주가 분리되었으며, 이 중 니켈내성세균(3mM)은 53,864 균주였다. 대조군에서는 BHI 한천배지에서 414,590 균주가, 니켈내성세균(3mM)은 37,523 균주가 분리되었다. BEA한천배지에서는 실험군의 경우 95개가 분리되었으며, 대조군에서는 20개의 균주만이 분리되었다. BHI 한천배지에서 분리된 총 균주 수를 100으로 놓았을 때 3mM 니켈배지에서 분리된 균주는 실험군에서는 10.62%, 대조군에서는 9.05%를 차지하여 두 군간에 뚜렷한 차이는 없었으며, 3mM 니켈배지에서 자란 총 균주 수와 BEA 한천배지에서 배양된 enterococci를 3mM 니켈배지로 옮겨 배양했을 때와 비교하면, 실험군에서 0.13%, 대조군에서 0.03%로 모두 1%이하의 분포를 차지하였다.

• 대한치과기공학회지
• /
• 제31권2호
• /
• pp.45-52
• /
• 2009

Esthetic restorations have been widely used in dental practice, although many studies have focused on the development and improvement of all ceramic restorations. The success of esthetic restorations depends primarily on an optimal bond strength between various veneered ceramics and core materials for esthetic restorations. The purpose of this study was to compare the shear bond strength between various veneered ceramics and core materials for esthetic restorations. 30 metal cores and 20 zirconia cores were fabricated and divided into five groups according to veneered ceramic materials such as Creation porcelain powder, Cercon Ceram Kiss, and IPS e.max ZirPress. Thirty spacimens were prepared using Creation porcelain powder, veneered 3mm height and 3mm in diameter, over the metal cores (n=10). Twenty specimens were prepared using Cercon Ceram Kiss and Zirpress, veneered 3mm height and 3mm in diameter, over the zirconia cores (n=10). The shear bond strength test was performed in a universal testing machine with a crosshead speed of 1mm/min. Ultimate shear bond strength data were analyzed with One-way ANOVA and the Scheffe's test (p=.05). Within the limits of this study, the following conclusions were drawn: The mean shear bond strengths (MPa) were: 18.44 for Uni metal VH/Creation (NCUC); 18.72 for Heraenium/Creation (NCHC); 16.23 for Wirobond C/Creation (NCWC); 13.88 for Zirconia core/$110{\mu}m$ $Al_2O_3$ sandblasting/Cercon Ceram Kiss (ZS110P); 14.61 for Zirconia core/No surface treatment/IPS e.max ZirPress (ZNTH). The mean shear bond strength for NCUC (Uni metal VH/Creation), NCHC (Heraenium/Creation) and NCWC (Wirobond C/Creation) were significantly superior to ZS110P (Zirconia core/$110{\mu}m$ $Al_2O_3$ sandblasting/Cercon Ceram Kiss) and ZNTH(Zirconia core/No surface treatment/IPS e.max ZirPress) (p<0.05).

• The Journal of Advanced Prosthodontics
• /
• 제9권3호
• /
• pp.170-175
• /
• 2017

PURPOSE. The aim of the present study was to evaluate the fracture resistances of zirconia, cast nickel-chromium alloy (Ni-Cr), and fiber-composite post systems under all-ceramic crowns in endodontically treated mandibular first premolars. MATERIALS AND METHODS. A total of 36 extracted human mandibular premolars were selected, subjected to standard endodontic treatment, and divided into three groups (n=12) as follows: cast Ni-Cr post-and-core, one-piece custom-milled zirconia post-and-core, and prefabricated fiber-glass post with composite resin core. Each specimen had an all-ceramic crown with zirconia coping and was then loaded to failure using a universal testing machine at a cross-head speed of 0.5 mm/min, at an angle of 45 degrees to the long axis of the roots. Fracture resistance and modes of failure were analyzed. The significance of the results was assessed using analysis of variance (ANOVA) and Tukey honest significance difference (HSD) tests (${\alpha}=.05$). RESULTS. Fiber-glass posts with composite cores showed the highest fracture resistance values ($915.70{\pm}323N$), and the zirconia post system showed the lowest resistance ($435.34{\pm}220N$). The corresponding mean value for the Ni-Cr casting post and cores was reported as $780.59{\pm}270N$. The differences among the groups were statistically significant (P<.05) for the zirconia group, as tested by ANOVA and Tukey HSD tests. CONCLUSION. The fracture resistance of zirconia post-and-core systems was found to be significantly lower than those of fiber-glass and cast Ni-Cr post systems. Moreover, catastrophic and non-restorable fractures were more prevalent in teeth restored by zirconia posts.

• The Journal of Advanced Prosthodontics
• /
• 제9권2호
• /
• pp.110-117
• /
• 2017

PURPOSE. This laboratory study assessed the effect of different dentin cleaning procedures on shear bond strength of resin cements for recementing prosthesis. MATERIALS AND METHODS. A $4{\times}4$ flat surface was prepared on the labial surface of 52 maxillary central incisors. Metal frames ($4{\times}4{\times}1.5mm$) were cast with nickel-chromium alloy. All specimens were randomly divided into 2 groups to be cemented with either Panavia F2.0 (P) or RelyX Ultimate (U) cement. The initial shear bond strength was recorded by Universal Testing Machine at a crosshead speed of 0.5 mm/min. Debonded specimens were randomly allocated into 2 subgroups (n = 13) according to the dentin cleaning procedures for recementation. The residual cement on bonded dentin surfaces was eliminated with either pumice slurry (p) or tungsten carbide bur (c). The restorations were rebonded with the same cement and were subjected to shear test. Data failed the normality test (P < .05), thus were analyzed with Mann Whitney U-test, Wilcoxon signed rank test, and two-way ANOVA after logarithmic transformation (${\alpha}=.05$). RESULTS. The initial shear bond strength of group P was significantly higher than group U (P = .001). Pc and Uc groups presented higher bond strength after recementation compared to the initial bond strength. However, it was significant only in Pc group (P = .034). CONCLUSION. The specimens recemented with Panavia F2.0 provided higher bond strength than RelyX Ultimate cement. Moreover, a tungsten carbide bur was a more efficient method in removing the residual resin cement and increased the bond strength of Panavia F2.0 cement after recementation.

• The Journal of Advanced Prosthodontics
• /
• 제8권3호
• /
• pp.224-228
• /
• 2016

PURPOSE. This study aimed to investigate whether dentin surface preparation with diamond rotary instruments of different grit sizes affects the shear bond strength of resin-bonded restorations. MATERIALS AND METHODS. The buccal enamel of 60 maxillary central incisors was removed with a low speed diamond saw and wet ground with silicon carbide papers. The polished surfaces of the teeth were prepared with four groups of rotary diamond burs with super-coarse (SC), coarse (C), medium (M), and fine (F) grit sizes. Following surface preparation, 60 restorations were casted with nickel-chromium alloy and bonded with Panavia cement. To assess the shear bond strength, the samples were mounted on a universal testing machine and an axial load was applied along the cement-restoration interface at the crosshead speed of 0.5 mm/min. The acquired data was analyzed with one way ANOVA and Tukey post hoc test (${\alpha}=.05$). RESULTS. The $mean{\pm}SD$ shear bond strengths (in MPa) of the study groups were $17.75{\pm}1.41$ for SC, $13.82{\pm}1.13$ for C, $10.40{\pm}1.45$ for M, and $7.13{\pm}1.18$ for F. Statistical analysis revealed the significant difference among the study groups such that the value for group SC was significantly higher than that for group F (P<.001). CONCLUSION. Dentin surface roughness created by diamond burs of different grit sizes considerably influences the shear bond strength of resin bonded restorations.

• The Journal of Advanced Prosthodontics
• /
• 제7권5호
• /
• pp.343-348
• /
• 2015

PURPOSE. The purpose of this study was to evaluate the bond strength of composite resin on the fracture surface of metal-ceramic depending on the repair systems and surface roughening methods. MATERIALS AND METHODS. A total of 30 disk specimens were fabricated, 15 of each were made from feldspathic porcelain and nickel-chromium base metal alloy. Each substrate was divided into three groups according to the repair method: a) application of repair system I (Intraoral Repair Kit) with diamond bur roughening (Group DP and DM), b) application of repair system I with airborne-particle abrasion (Group SP and SM), and c) application of repair system II (CoJet Intraoral Repair System, Group CP and CM). All specimens were thermocycled, and the shear bond strength was measured. The data were analyzed using the Kruskal-Wallis analysis and the Mann-Whitney test with a significance level of 0.05. RESULTS. For the porcelain specimens, group SP showed the highest shear bond strength ($25.85{\pm}3.51MPa$) and group DP and CP were not significantly different. In metal specimens, group CM showed superior values of bond strength ($13.81{\pm}3.45MPa$) compared to groups DM or SM. CONCLUSION. Airborne-particle abrasion and application of repair system I can be recommended in the case of a fracture localized to the porcelain. If the fracture extends to metal surface, the repair system II is worthy of consideration.

• 대한치과보철학회지
• /
• 제40권6호
• /
• pp.590-596
• /
• 2002

The resin : metal interface is at the basis of most bonding failures in resin-bonded prosthesis. Although debonding has been a problem with adhesive fixed partial dentures, various dentists classify them as long-term restorations. The advantages of resin-bonded fixed partial dentures include minimal tooth reduction and the possibility of rebonding. if resin-bonded protheses can be easily rebounded, it is of clinical importance to know if the lutingagents rebond as well the second time as they did originally. Several retentive systems for resin-to-metal bonding have recommended. Treatments such as electrolytic etching and silicone coating, despite the good result of bond strength, have proved to be time-consuming and technique-sensitive. Therefore a simple and more reliable method is desirable. This study evaluated the effect of metal surface treatments on the rebond strength of panavia 21 cement to a nickel-chromium(Ni-Cr) alloy. The samples were received the following surface treatments : Group No.1 (control or served as the control) treatment with sandblasting with 50um aluminum oxide and ultrasonically cleaned for 10minutes in double-deionized water, Group No.2 were no surface treatments. Group No.3 were treated with metal primer. Group No.4 were treated with sandblasting as previously described, and then metal priming. From the analysis of the results, the following conclusions were drawn. 1. Sandblasting and metal priming appears to be an effective method for treatment of metal after accidental debonding. 2. Group without surface treatment had significantly lower bond strengths compared with other groups. 3. The combination of sandblasting and metal priming may not develop superior bonding strengths compared with other techniques that used the Ni-Cr alloys. 4. Combination of cohesive and adhesive failures were the most common type observed. The results support the use of sandblasting as a viable procedure when rebonding accidentally lost adhesive partial denture. We concluded that sandblasting and metal priming of metal surface before bonding could provide the adequate bond strength during rebonding of resin-bonded fixed partial denture.