• 제목/요약/키워드: Nanoparticle Fabrication

검색결과 143건 처리시간 0.025초

전기방사법을 이용한 Ag 나노입자 분산 고분자 나노파이버와 Ag 나노파이버 제조 및 특성 평가 (Fabrication and Characterization of Ag Nanoparticle Dispersed Polymer Nanofiber and Ag Nanofiber Using Electrospinning Method)

  • 김희택;황치용;송한복;이근재;주연준;홍성재;강남기;박성대;김기도;좌용호
    • 한국분말재료학회지
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    • 제15권2호
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    • pp.114-118
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    • 2008
  • Functional nanomaterial is expected to have improved capacities on various fields. Especially, metal nanoparticles dispersed in polymer matrix and metal nanofiber, one of the functional nanomaterials, are able to achieve improvement of property in the electric and other related fields. In this study, the fabrication of metal (Ag) nanoparticle dispersed nanofibers were attempted. The Ag nanoparticle dispersed polymer nanofiber and Ag nanofiber were fabricated by electrospinning method using electric force. First, PVP/$AgNO_3$ nanofibers were synthesized by electrospinning in $18{\sim}22kV$ voltage with the starting materials (Ag-nitrate) added polymer (PVP; poly (vinylpyrrolidone)). Then Ag nanoparticle dispersed polymer nanofibers were fabricated to reduce hydrogen reduction at $150^{\circ}C$ for 3hr. And Ag nanofibers were synthesized by the decomposited of PVP at $300{\sim}500^{\circ}C$ for 3hr. The nanofibers were analyzed by XRD, TGA, FE-SEM and TEM. The experimental results showed that the Ag nanofibers could be applied in many fields as an advanced material.

C60 및 Si 초미립자 박막의 Laser 반응에 의한 가시광선발광 (Visible light emission from $C_60$ and Si nanoparticle film by laser process)

  • 김민성
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2000년도 추계학술대회 논문집
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    • pp.598-601
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    • 2000
  • We investigated the fabrication of Si nanoparticle and $C_{60}$ thin films by pulsed laser ablation. As a result, we observed visible green photoluminescence spectra in the Si/C$_{60}$ multilayer films after laser annealing. It is considered that this green photoluminescence is occurred from SiC particles, which is produced reaction of Si nanoparticles with $C_{60}$ via laser annealing.ing.

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PCL/TiO2 Nanoparticle 3차원 지지체 제조 및 특성 평가 (Fabrication and Characterization of PCL/TiO2 Nanoparticle 3D Scaffold)

  • 김정호;이옥주;;주형우;문보미;박현정;박찬흠
    • 폴리머
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    • 제38권2호
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    • pp.150-155
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    • 2014
  • Polycaprolactone(PCL)은 생분해성 고분자로 인장강도, 신장률, 충격강도 등의 기계적 물성이 우수하다. $TiO_2$ (titanium dioxide) nanoparticle은 친수성으로 밀도가 높고 생체적합성이 우수하다. 본 연구에서는 PCL과 $TiO_2$(titanium dioxide) nanoparticle을 이용하여 salt-leaching방법으로 3차원 다공성 지지체를 제작하였다. 제작한 지지체를 FESEM, FTIR, TGA, 압축강도 측정 등을 통해 물성을 분석하였다. $TiO_2$ nanoparticle에 의해 물흡수도와 팽윤도는 감소하였으나 압축강도는 증가하였다. CCK-8 assay를 통해 세포의 증식률을 확인한 결과, $TiO_2$ nanoparticle에 의한 세포 독성은 없는 것으로 확인되었다. 이러한 연구결과는 PCL/$TiO_2$ nanoparticle 지지체의 생체재료로 사용가능성을 제시하였다.

플라즈모닉 흡수체를 위한 금속 나노입자 주기구조 제작 기술 (Periodically Aligned Metal Nanoparticle Array for a Plasmonic Absorber and Its Fabrication Technique)

  • 최민정;류윤하;배규영;강구민;김경식
    • 한국광학회지
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    • 제28권6호
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    • pp.361-365
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    • 2017
  • 본 논문은 협대역의 플라즈모닉 흡수체 구현을 위한 금속 나노입자 주기구조 설계 및 제작에 관한 연구다. 제안된 플라즈모닉 흡수체의 상단 금속 나노입자는 주기적으로 홈이 파여있는 템플릿을 이용하여 전자빔 증착 후, 열처리하는 제작 기술로 형성하였다. 주기적 홈 템플릿 위에 제작된 금속 나노입자를, 따로 제작한 33 nm 두께의 $Al_2O_3$가 스퍼터 가공된 200 nm 두께의 금속 반사판-기판 상단에 옮기는 방법을 통해 플라즈모닉 흡수체를 제작하였다. 제작된 금속 나노입자는 평균 지름 46 nm, 주기 76 nm의 크기를 가졌다. 광학 측정 결과, 제작된 플라즈모닉 흡수체는 중심파장 572 nm, 반값전폭 109.9 nm의 플라즈모닉 공명 흡수를 나타내었다.

CIS 태양전지용 이원 화합물 $Cu_xSe$ 나노입자를 이용한 $Cu_xSe$ 박막 제조 (Fabrication of $Cu_xSe$ thin films by selenization of $Cu_xSe$ nanoparticles prepared by a colloidal process)

  • 김균환;안세진;윤재호;곽지혜;김도진;윤경훈
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2009년도 춘계학술대회 논문집
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    • pp.96-98
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    • 2009
  • This report summarizes our recent efforts to produce large-grained CIGS materials from porous nanoparticle thin films. In our approach, a $Cu_xSe$ nanoparticle colloid were first prepared by reacting a mixture of CuI in pyridine with $Na_2Se$ in methanol at reduced temperature. purified colloid was sprayed onto heated molybdenum-coated sodalime glass substrates to form thin film. After thermal processing of the thin film under a selenium ambient. $Cu_xSe$ colloid and thin film were characterized by scanning electron microscopy, x-ray diffraction. The optical(direct) band gap energy of $Cu_xSe$ thin films is 1.5 eV.

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Magnetically Driven Assemblies of γ-Fe3O4 Nanoparticles into Well-Ordered Permanent Structures

  • Byun, Myunghwan
    • 한국분말재료학회지
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    • 제24권3호
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    • pp.229-234
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    • 2017
  • We report on a simple and robust route to the spontaneous assembly of well-ordered magnetic nanoparticle superstructures by irreversible evaporation of a sessile single droplet of a mixture of a ferrofluid (FF) and a nonmagnetic fluid (NF). The resulting assembled superstructures are seen to form well-packed, vertically arranged columns with diameters of $5{\sim}0.7{\mu}m$, interparticle spacings of $9{\sim}2{\mu}m$, and heights of $1.3{\sim}3{\mu}m$ The assembled superstructures are strongly dependent on both the magnitude of magnetic field and the mixing ratio of the mixture. As the magnitude of the externally applied magnetic field and the mixing ratio of the mixture increase gradually, the size and interspacing of the magnetic nanoparticle aggregations decrease. Without an externally applied magnetic field, featureless patterns are observed for the ${\gamma}-Fe_3O_4$ nanoparticle aggregations. The proposed approach may lead to a versatile, cost-effective, fast, and scalable fabrication process based on the field-induced self-assembly of magnetic nanoparticles.