• Title/Summary/Keyword: Nanoparticle Fabrication

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Fabrication and Characterization of Ag Nanoparticle Dispersed Polymer Nanofiber and Ag Nanofiber Using Electrospinning Method (전기방사법을 이용한 Ag 나노입자 분산 고분자 나노파이버와 Ag 나노파이버 제조 및 특성 평가)

  • Kim, Hee-Taik;Hwang, Chi-Yong;Song, Han-Bok;Lee, Kun-Jae;Joo, Yeon-Jun;Hong, Seong-Jei;Kang, Nam-Kee;Park, Seong-Dae;Kim, Ki-Do;Cho, Yong-Ho
    • Journal of Powder Materials
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    • v.15 no.2
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    • pp.114-118
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    • 2008
  • Functional nanomaterial is expected to have improved capacities on various fields. Especially, metal nanoparticles dispersed in polymer matrix and metal nanofiber, one of the functional nanomaterials, are able to achieve improvement of property in the electric and other related fields. In this study, the fabrication of metal (Ag) nanoparticle dispersed nanofibers were attempted. The Ag nanoparticle dispersed polymer nanofiber and Ag nanofiber were fabricated by electrospinning method using electric force. First, PVP/$AgNO_3$ nanofibers were synthesized by electrospinning in $18{\sim}22kV$ voltage with the starting materials (Ag-nitrate) added polymer (PVP; poly (vinylpyrrolidone)). Then Ag nanoparticle dispersed polymer nanofibers were fabricated to reduce hydrogen reduction at $150^{\circ}C$ for 3hr. And Ag nanofibers were synthesized by the decomposited of PVP at $300{\sim}500^{\circ}C$ for 3hr. The nanofibers were analyzed by XRD, TGA, FE-SEM and TEM. The experimental results showed that the Ag nanofibers could be applied in many fields as an advanced material.

Visible light emission from $C_60$ and Si nanoparticle film by laser process (C60 및 Si 초미립자 박막의 Laser 반응에 의한 가시광선발광)

  • ;Hideomi Koinuma
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.11a
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    • pp.598-601
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    • 2000
  • We investigated the fabrication of Si nanoparticle and $C_{60}$ thin films by pulsed laser ablation. As a result, we observed visible green photoluminescence spectra in the Si/C$_{60}$ multilayer films after laser annealing. It is considered that this green photoluminescence is occurred from SiC particles, which is produced reaction of Si nanoparticles with $C_{60}$ via laser annealing.ing.

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Fabrication and Characterization of PCL/TiO2 Nanoparticle 3D Scaffold (PCL/TiO2 Nanoparticle 3차원 지지체 제조 및 특성 평가)

  • Kim, Jung-Ho;Lee, Ok Joo;Sheikh, Faheem A.;Ju, Hyung Woo;Moon, Bo Mi;Park, Hyun Jung;Park, Chan Hum
    • Polymer(Korea)
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    • v.38 no.2
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    • pp.150-155
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    • 2014
  • Polycaprolactone (PCL) is a synthetic biodegradable polymer with excellent mechanical properties. $TiO_2$ (titanium dioxide) has a hydrophilic, high density and excellent biocompatibility. In this work, we produced three-dimensional porous scaffolds with PCL and $TiO_2$ nanoparticles using a salt-leaching method. Physical properties of the scaffolds were analyzed by FE-SEM, FTIR, TGA and compressive strength. Interestingly, the addition of $TiO_2$ nanoparticles decreased the water absorption and swelling ratio of the porous scaffolds. However, the compressive strength was increased by $TiO_2$. CCK-8 assay, which is generally used for the analysis of cell growth, shows that $TiO_2$ nanoparticles have no cytotoxicity. Taken together, we suggest that the PLC/$TiO_2$-scaffold can be used for biomedical applications.

Periodically Aligned Metal Nanoparticle Array for a Plasmonic Absorber and Its Fabrication Technique (플라즈모닉 흡수체를 위한 금속 나노입자 주기구조 제작 기술)

  • Choi, Minjung;Ryu, Yunha;Bae, Kyuyoung;Kang, Gumin;Kim, Kyoungsik
    • Korean Journal of Optics and Photonics
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    • v.28 no.6
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    • pp.361-365
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    • 2017
  • In this paper, we demonstrate a facile fabrication technique for a periodically aligned metal nanoparticle array, for a narrow-band plasmonic absorber. The metal nanoparticles are fabricated by e-beam evaporation and heat treatment processes on top of a periodic aluminum groove template. The plasmonic absorber is constructed with the transferred metal nanoparticle array, sputtered 33-nm-thick $Al_2O_3$, and 200-nm-thick metal reflector layers on silicon substrate. 46-nm-diameter and 76-nm-lattice metal-nanoparticle-array-based plasmonic absorber has performed as a narrow-band absorber with a central wavelength of 572 nm and full width at half maximum (FWHM) of 109.9 nm.

Fabrication of $Cu_xSe$ thin films by selenization of $Cu_xSe$ nanoparticles prepared by a colloidal process (CIS 태양전지용 이원 화합물 $Cu_xSe$ 나노입자를 이용한 $Cu_xSe$ 박막 제조)

  • Kim, Kyun-Hwan;Ahn, Se-Jin;Yun, Jae-Ho;Gwak, Ji-Hye;Kim, Do-Jin;Yoon, Kyung-Hoon
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.06a
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    • pp.96-98
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    • 2009
  • This report summarizes our recent efforts to produce large-grained CIGS materials from porous nanoparticle thin films. In our approach, a $Cu_xSe$ nanoparticle colloid were first prepared by reacting a mixture of CuI in pyridine with $Na_2Se$ in methanol at reduced temperature. purified colloid was sprayed onto heated molybdenum-coated sodalime glass substrates to form thin film. After thermal processing of the thin film under a selenium ambient. $Cu_xSe$ colloid and thin film were characterized by scanning electron microscopy, x-ray diffraction. The optical(direct) band gap energy of $Cu_xSe$ thin films is 1.5 eV.

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Magnetically Driven Assemblies of γ-Fe3O4 Nanoparticles into Well-Ordered Permanent Structures

  • Byun, Myunghwan
    • Journal of Powder Materials
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    • v.24 no.3
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    • pp.229-234
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    • 2017
  • We report on a simple and robust route to the spontaneous assembly of well-ordered magnetic nanoparticle superstructures by irreversible evaporation of a sessile single droplet of a mixture of a ferrofluid (FF) and a nonmagnetic fluid (NF). The resulting assembled superstructures are seen to form well-packed, vertically arranged columns with diameters of $5{\sim}0.7{\mu}m$, interparticle spacings of $9{\sim}2{\mu}m$, and heights of $1.3{\sim}3{\mu}m$ The assembled superstructures are strongly dependent on both the magnitude of magnetic field and the mixing ratio of the mixture. As the magnitude of the externally applied magnetic field and the mixing ratio of the mixture increase gradually, the size and interspacing of the magnetic nanoparticle aggregations decrease. Without an externally applied magnetic field, featureless patterns are observed for the ${\gamma}-Fe_3O_4$ nanoparticle aggregations. The proposed approach may lead to a versatile, cost-effective, fast, and scalable fabrication process based on the field-induced self-assembly of magnetic nanoparticles.