• Title/Summary/Keyword: Nano 입자

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Synthesis of Porous Carbon Particles for the Absorption of Mercury (액상수은 제어를 위한 다공성 탄소입자 제조에 관한 연구)

  • Lee, Jung-Min;Kang, Shin-Jae;Park, Soo-Jin
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.305-305
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    • 2009
  • The carbon nano-structured materials could be applied to the fields of advanced fillers, templates, electrode materials, sensor, storage, and absorption materials. The polyacrylonitrile (PAN) based carbon nano-particles provide the remarkable properties of high specific surface area, large pore volume, chemical inertness, and good mechanical stability. In this study, well-defined carbon nano-particles were obtained through pyrolysis of polyacrylonitrile based particles. The precursor nano-particles were prepared by modified aqueous dispersion polymerization using hydrophilic poly(vinyl alcohol) in a water/ N,N-dimethylformamide mixture media. Synthesized precursor nanoparticles have relatively monodisperse particles ranging 80 ~ 250nm. Stable spherical particles are obtained without coagulum or secondary particles in our system. The characteristic of the carbon nanoparticles were investigated in terms of surface area, morphology, and size distribution.

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The Multi-Frequency NMR Relaxation and EPR Study of Nano-sized Iron Oxide

  • 황문정;이영주;이일수;장용민
    • Proceedings of the KSMRM Conference
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    • 2002.11a
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    • pp.129-129
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    • 2002
  • 목적: 초상자성 nano 산화철 입자의 특성을 연구하기 위하여, 여러 다른 자기장 세기에서의 NMR 자기공이완시간(T1/T2)을 측정하고, 초상자성 nano-particle 조영제의 기전에 관한 모델로부터 얻어 진 계산식과 비교해보며, 다양한 온도에서의 EPR spectrum을 이용하여 이들의 전자적 성질을 비교해 보고자 하였다.

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Methods to Formulate Waterborne Conjugated Polymer Nanoparticles (수분산 공액고분자 나노입자의 합성 방법론)

  • Seungju Kang;Boseok Kang
    • Journal of Adhesion and Interface
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    • v.24 no.1
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    • pp.1-8
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    • 2023
  • A conjugated polymer is the next-generation emerging semiconductor material that can be applied in various fields, from organic electronics to biomedical applications. However, its low solubility in an aqueous medium has made the use of toxic organic solvents inevitable, thereby leading to formulation of conjugated polymers in the form of waterborne nanoparticles. This review paper discusses two principles of nanoparticle formation and representative methods for synthesizing conjugated polymer nanoparticles.

Synthesis of ZnS : Cu nano-crystals and structural and optical properties (ZnS : Cu nano 업자의 합성 및 구조적.광학적 특성)

  • 이종원;이상욱;조성룡;김선태;박인용;최용대
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.12 no.3
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    • pp.138-143
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    • 2002
  • In this study, ZnS: Cu nano-crystals are synthesized by solution synthesis technique (SST). The structural properties such as crystal structure and particle morphology, and the optical properties such as light absorption/transmittance, energy bandgap, and photoluminescence (PL) excitation/emission are investigated. In an attempt to realize the Cu-doping easiness, the synthesis temperature (~$80^{\circ}C$) is applied to the synthesis bath, and the thiourea is used as sulfur precursor, unlike other general chemical synthesis route. Both undoped ZnS and ZnS : Cu nano-crystals have the cubic crystal structure and have the spherical particle shape. The position of light absorption edge is ~305 nm, indicating the occurrence of quantum size effect. The PL emission intensity and line-width are maximum and minimum, respectively, for Cu-doping concentration 0.03M. In particular, the dependence of PL intensity and line-width on the Cu-doping concentration for ZnS : Cu nano-crystals synthesized by SST is reported for the first time in this study. Experimental results of the absorption edge and the PL excitation show that the main emission peak of ZnS : Cu nano-crystals (~510 nm) in this study is due to the radiative recombination center in the energy bandgap induced by Cu dopant.

Direct indium-tin oxide (ITO) nano-patterning using ITO nano particle solution (Indium-tin oxide (ITO) 나노 입자 용액을 이용한 직접 ITO 나노 패턴 제작 기술)

  • Yang, Gi-Yeon;Yun, Gyeong-Min;Lee, Heon
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.10a
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    • pp.247-247
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    • 2009
  • 본 연구에서는 indium-tin oxide (ITO) 나노 입자 용액을 이용하여 간단한 공정을 통해 ITO 나노 패턴을 직접적으로 제작하는 기술에 대한 연구를 진행하였다. 이를 이용하여 300nm급 ITO 나노 dot 패턴을 제작하는데 성공하였으며 이를 glass 표면에 구현하는데 성공하였다.

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Synthesis of Polymer-Silica Hybrid Particle by Using Polyamine Nano Complex (폴리아민 나노 복합체를 이용한 고분자-실리카 복합체 입자 합성)

  • Kim, Dong-Yeong;Seo, Jun-Hee;Lee, Byungjin;Kang, Kyoung-Ku;Lee, Chang-Soo
    • Clean Technology
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    • v.27 no.2
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    • pp.115-123
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    • 2021
  • This study demonstrates a new method for the synthesis of organic-inorganic hybrid particles composed of an inorganic silica shell and organic core particles. The organic core particles are prepared with a uniform size using droplet-based microfluidic technology. In the process of preparing the organic core particles, uniform droplets are generated by independently controlling the flow rates of the dispersed phase containing photocurable resins and the continuous phase. After the generation of droplets in a microfluidic device, the droplets are photo-polymerized as particles by ultraviolet irradiation at the ends of microfluidic channels. The core particle is coated with a nano complex composed of polyallylamine hydrochloride (PAH) and phosphate ion (Pi) through strong non-covalent interactions such as hydrogen bonding and electrostatic interaction under optimized pH conditions. The polyamine nano complex rapidly induces the condensation reaction of silicic acid through the arranged amine groups of the main chain of PAH. Therefore, this method enabled the preparation of organic-inorganic hybrid particles coated with inorganic silica nanoparticles on the organic core. Finally, we demonstrated the synthesis of organic-inorganic hybrid particles in a short time under ambient and environmentally friendly conditions, and this is applicable to the production of organic-inorganic hybrid particles having various sizes and shapes.