• Nuclear Engineering and Technology
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• 제49권7호
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• pp.1442-1450
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• 2017

In liquid metal fast breeder reactors, postulated failures of the plant protection system may lead to serious unprotected accidental consequences. Unprotected transients are generically categorized as transient overpower accidents and transient under cooling accidents. In both cases, core meltdown may occur and this can lead to a molten fuel coolant interaction (MFCI). The understanding of MFCI phenomena is essential for study of debris coolability and characteristics during post-accident heat removal. Sodium is used as coolant in liquid metal fast breeder reactors. Viewing inside sodium at elevated temperature is impossible because of its opaqueness. In the present study, a methodology to depict MFCI phenomena using a flat panel detector based imaging system (i.e., real time radiography) is brought out using a woods metal-water experimental facility which simulates the $UO_2-Na$ interaction. The developed imaging system can capture attributes of the MFCI process like jet breakup length, jet front velocity, fragmented particle size, and a profile of the debris bed using digital image processing methods like image filtering, segmentation, and edge detection. This paper describes the MFCI process and developed imaging methodology to capture MFCI attributes which are directly related to the safe aspects of a sodium fast reactor.

• 대한방사선기술학회지:방사선기술과학
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• 제41권5호
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• pp.437-444
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• 2018

Whole-Body counters have been used to evaluate the internal contamination of gamma emitting radionuclides. Among the whole-body counters used in domestic nuclear facilities, Fastscan made by CANBERRA contains 2 NaI(Tl) detectors and is generally used to monitor the primary internal exposure. It has the advantage of achieving MDA even with short time measurements. Accuscan is a bed type, and has good energy resolution because it is composed of HPGe detector. Since the Accuscan with better energy resolution than Fastscan has better able to identify radionuclides, it is used to monitor secondary internal exposure. Some nuclear facilities have only Fastscan. We analyzed statistically whether Fastscan is enough to ensure accuracy and precision comparing with Accuscan. To do this, we prepared a CRM created by the Korea Research Institute of Standards and Science. We also obtained the data of 6 Fastscans and 5 Accuscans in domestic nuclear facilities. As a result of the study, although Fastscan compared with Accuscan is not as accurate as the Accuscan, the precision is statistically same. However, accuracy of Fastscan is in compliance with international standards except low energy range. In terms of accuracy and precision except radionuclides emitting low energy, it is possible to measure radioactivity inside workers even in nuclear facilities where only Fastscan is used.

• 대한전자공학회논문지
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• 제3권1호
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• pp.18-23
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• 1966

동철종으로 부터 후방 산란되는 감마선을 측정하므로써 그의 두께를 수정할 수 있는 두께계의 실용성에 관하여 실험적인 검토를 하였다. 본 두께계의 특징은 선원으로부터 반사되는 1 차방사선과 철판으로 부터 후방 산란되는 2차 방사선을 적시에 동일한 씬티레이숀 검출기로 검출하며 사용되는 선원의 방사선 강도도 20μc 정도로 적으므로 일절의 방사선 차폐물이 불필요하므로 가반형 두께계로서 적당하다. 씬티레이숀 검출기로 부터의 출력 펄스는 프리암프, 메인암프, 및 단채널 파고분석기를 거쳐 후방 산란 감마선만을 선별한 다음 계수률계상에서 두께로 직독하도록 할 수 있다. 광판의 두께 변화에 대한 지시감도를 크게 하기 위한 선원의 위치 파고분석기의 window width, 사용될 선원의 에너지와 강도등의 최적치를 구하기 위한 실험을 행하였다. 이 두께계로서 강철판 또는 파이프의 내벽상의 작은 흠이나 부식처를 용이하게 발견할 수 있다. 실측결과 3∼8mm 두께 범위에서 약 ±3%의 정밀도를 얻었고 20mm 두께에서는 약 ±10%로 저하되었다.

• 대한본초학회지
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• 제23권4호
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• pp.171-177
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• 2008

Objectives: This study presents a reversed-phase high-performance liquid chromatography- pulsed amperometric detection(RP-HPLC-PAD) method for the determination of puerarin and daidzin in Puerariae Radix extract and Chinese medicinal preparations. Methods: Chromatographic separation was performed using a 10% acetonitrile with a reversed-phase column(Unison UK-C18, $100mm{\times}2.0mm$ I.D.; $3{\mu}m$). The analyses were detected by pulsed amperometric detector(PAD) in alkaline conditions by combining with post-column NaOH solution. Geniposide was used as an internal standard. Results: The limit of detection(S/N=3) and the limit of quantification(S/N=10) were 0.025 ng, 0.075 ng for puerarin, and 0.05 ng, 0.15 ng for daidzin, respectively. The intra- and inter-day precisions(RSDs) were less than 6.5% and average recoveries of puerarin were 99.7-101.3% and those of daidzin were 101.0-102.8%. Conclusions: According to above results, we developed a determination method for puerarin and daidzin in Puerariae Radix with high sensitivity and selectivitely.

• 대한핵의학회지
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• 제27권1호
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• pp.104-111
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• 1993

Trace elements are important components in the biological system, as a structural material and metabolic controller. Neutron activation analysis (NAA) with high neutron flux and high energy resolution Ge (Li) detector coupled to multichannel analyzer (MCA) has been one of the most accurate method for the determination of ultra-trace level components, and is applicable to biological material. In human body, the NAA can be used for quantitation of trace elements in various organs and tissue with endocrinological and metabolic disease and industrial metal poisoning. In this study, Triga Mark III nuclear reactor in Korea Atomic Research Institute was used for quantitation of trace eleement in human lung cancer tissues by neutron activation analysis. In the squamous cell carcinoma tissues, Br, Hg, La, Sb, Sc, Cl, Fe and I content were lower than normal lung tissues, and K, Rb and Se content were higher. In the adenocarcinoma tissues, Fe, Au, La, Sc and Zn content were lower than normal lung tissues, and Rb, Co and Se content were higher. Rb content was higher in the adenocarcinoma tissues than in the squamous cell carcinoma tissues. Fe and Na content were higher in the squamous cell carcinoma tissues than in the adenocarcinoma tissues.

• Journal of Radiation Protection and Research
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• 제15권2호
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• pp.87-100
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• 1990

자연환경 방사선의 주 요소의 하나인 지각 방사선에 의한 피폭선량을 정량적으로 측정 해석하기 위하여 24개월간에 걸친 TLD에 의한 연속 적산선량 측정과 주기적인 감마선 분광분석을 수행하였다. TLD로는 LiF PTFE disk형을 사용하였으며 감마선 분광분석에서는 $3&{\phi}{\times}3'$원주형 Nal(Tl) 섬광검출기와 휴대형 다중파고 분석기 (4096 ch)를 사용하였다. 측정한 선량은 모두 실효 선량당량으로 평가하였으며 부수적으로 우주선 전리 성분에 의한 선량당량도 평가할 수 있었다. 분산 가중 평균값을 취한 결과에 의하면 대전 지역의 측정점에서 지각 방사선과 우주선 전리 성부의 체외 피폭에 의한 년간 실효 선량당량은 각각 $564{\pm}4\;{\mu}Sv(64.8{\pm}0.5nSv{\cdot}h^{-1}$ 및 $300{\pm}2\;{\mu}Sv(34.3{\pm}0.2nSv{\cdot}h^{-1}$로 나타났다.

• Nuclear Engineering and Technology
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• 제5권4호
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• pp.291-309
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• 1973

TRIGA Mark II와 III 원자로의 여러가지 가동조건에 있어서 노벽으로 부터의 누설 ${\gamma}$선에 의한 조사선양률을 3"$\times$3"원통형 NaI(T1) 섬광계수기와 400 channel파 고분석장치로 측정하였는데 측정된 spectrum으로부터 조사선양률을 산출하는데는 실제적면에서 복잡하기 짝이 없는 response matrix 방법대신 정도가 좋으면서도 비교적 그 과정이 단순한 Moriuchi의 specturm -조사선양률 환산 이론을 적용하였다. 연구결과에 따르면 노심에서 발생된 누설 ${\gamma}$선의 기본적인 spectrum 형태는 원자로의 열출력이나 차장벽에 의한 강도의 감쇠에 별로 영향을 받지 않고 있으며 원자로 누설${\gamma}$선에 의란 전조사선양률의 공기중에서의 감쇠는 폭 넓은 energy분포에도 불구하고 지수함수적 감쇠를 하고 있음이 판명되있다. 이 전조사선양률은 원자로의 열출력에 대체로 비례하고 있으나 TRIGA Mark III과 같은 가동형노심의 경우는 측정된 spectrum이 매우 다양한바, 그로부터 산출된 전조사선양률의 크기에는 관계없이, spectrum 분해방법을 적용하여 노심에서 발생된 누설 ${\gamma}$선과 원자로가동중 발생되는 여지 ${\gamma}$선의 기여를 판별 해석하는데 성공하였다.

• 한국식품위생안전성학회지
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• 제3권4호
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• pp.211-215
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• 1988

아황산염류는 표백, 살균, 간별 방지 및 황산화 등의 목적으로 식품첨가물로 많이 사용되고 있다. 이러한 아황산염류의 시험 방법은 우리나라 보사부의 공정시험으로 지정된 적정법과 비색법 이외도 GLC, HPLC, AAS 등을 이용한 많은 분석방법들이 연구되어 왔으나 그 정밀도, 검출한계, 안정성 등에 많은 문제가 있다. 이에 저자 등은 IC를 이용하여 아황산염류를 신속하고 정확하게 정량할 수 있는 방법을 모색하여 다음과 같은 결과를 얻었다. 1) I.C를 이용하여 $SO_2^{-2}$로서 0.2ppm까지 검출할 수 있었으며 분석기산은 20분 이내였다. 2) 흡수액은 아호아산이온의 안정성을 고려하여 3% $H_2O_2$을 사용함으로써 안정한 황산이온으로 산화시켜 정량하였다. 3) 증류수에 표준액을 첨가한 후 증류하여 측정한 회수율은 99.8%로 양호하였으나 실제 식품에 첨가한 경우는 식품의 종류에 따라 회수율의 차이가 있었다.

• Nuclear Engineering and Technology
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• 제54권3호
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• pp.1062-1070
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• 2022

In the present communication, pure and stable α-Bismuth Oxide (Bi₂O₃) nanoparticles (NPs) were synthesized by low temperature solution combustion method using urea as a fuel and calcined at 500℃. The synthesized sample was characterized by using powder X-ray Diffraction (PXRD), Scanning Electron Microscopy (SEM), Energy dispersive X-ray analysis (EDAX), Transmission Electron Microscopy (TEM), Fourier Transform Infrared Spectroscopy (FTIR) and UV-Visible absorption spectroscopy. The PXRD pattern confirms the formation of mono-clinic, stable and low temperature phase α-Bi₂O₃. The direct optical energy band gap was estimated by using Wood and Tauc's relation which was found to be 2.81 eV. The characterized sample was studied for X-ray/gamma ray shielding properties in the energy range 0.081-1.332 MeV using NaI (Tl) detector and multi channel analyzer (MCA). The measured shielding parameters agrees well with the theory, whereas, slight deviation up to 20% is observed below 356 keV. This deviation is mainly due to the influence of atomic size of the target medium. Furthermore an accurate theory is necessary to explain the interaction of X-ray/gamma ray with the NPs.The present work opens new window to use this facile, economical, efficient, low temperature method to synthesize nanomaterials for X-ray/gamma ray shielding purpose.

• Nuclear Engineering and Technology
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• 제55권5호
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• pp.1519-1526
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• 2023

For the first time Aluminium-BariumeZinc oxide nanocomposite (ZABONC) was synthesized by solution combustion method where calcination was carried out at low temperatures (600℃) to study the electromagnetic (EM) (X/γ) radiation shielding properties. Further for characterization purpose standard techniques like PXRD, SEM, UV-VISIBLE, FTIR were used to find phase purity, functional groups, surface morphology, and to do structural analysis and energy band gap determination. The PXRD pattern shows (hkl) planes corresponding to spinel cubic phase of ZnAl₂O4, cubic Ba(NO₃)₂, α and γ phase of Al₂O₃ which clearly confirms the formation of complex nano composite. From SEM histogram mean size of nano particles was calculated and is in the order of 17 nm. Wood and Tauc's relation direct energy band gap calculation gives energy gap of 2.9 eV. In addition, EM (X/γ) shielding properties were measured and compared with the theoretical ones using standard procedures (NaI (Tl) detector and multi channel analyzer MCA). For energy above 356 keV the measured shielding parameters agree well with the theory, while below this value slight deviation is observed, due to the influence of atomic/crystallite size of the ZABONC. Hence synthesized ZABONC can be used as a shielding material in EM (X/γ) radiation shielding.