• Journal of Dairy Science and Biotechnology
• /
• 제36권2호
• /
• pp.73-80
• /
• 2018

The textural and rheological properties of cheese are major attributes for the characterization of cheese types, ripening, and consumer preferences. The use of small amplitude oscillatory rheological testing has made it possible for cheese researchers to assess the major properties of cheese, such as melting behavior and storage modulus, without irreversible deformation. In addition, large deformation testing such as textural profile analysis can assess properties such as hardness of cheese. While the sensory properties of cheese are valued by consumers, objective and reliable measurements are paramount for researchers. Ongoing development and refinement of scientific measurement methods of cheese are vital.

• 세라미스트
• /
• 제22권4호
• /
• pp.381-392
• /
• 2019

Recently, demands for lithium-ion batteries (LIB) in various fields are increasing. In particular, understanding of the reaction mechanism occurring at the electrode-electrolyte surface/interface is significant for the development of advanced LIBs. Meanwhile, research and development of LIBs highly requires a new specific characterization approach. For example, atomic force microscopy (AFM) has been utilized to the LIB research field for various purposes such as investigation of topography, electrochemical reactions, ion transport phenomena, and measurement of surface potential at high resolution. Advances in the AFM analysis have made it possible to inspect various material properties such as surface friction and Young's modulus. Therefore, this technique is expected to be a powerful method in the LIB research field. Here, we review and discuss ways to apply AFM to LIB studies.

• 한국지진공학회:학술대회논문집
• /
• 한국지진공학회 1998년도 춘계 학술발표회 논문집 Proceedings of EESK Conference-Spring 1998
• /
• pp.75-80
• /
• 1998

Dynamic measurements are used rather sparingly to determine the elastic moduli of rock cores and modulus values are not much utilized in design practices. The reason seems to result from the general perception that values obtained by dynamic measurement are much higher (about 10 time) than those determined statically. This paper presents results from dynamic and static tests on rock cores. One of the findings is that both moduli determined by statically and dynamically on a solid rock core agrees well at the same-strain. At different strain levels, the ratio between dynamic and static modult widely varies depending upon micro-cracks and discontinuites of rock cores.

• 소성∙가공
• /
• 제11권7호
• /
• pp.561-568
• /
• 2002

Micro tensile test is the most direct and convenient method to measure material properties such as Young's modulus and fracture strength. It, however, needs more accurate measurement system, mote stable and repetitive alignment and more sensitive gripping than conventional tensile test. Many researchers have put their effort on overcoming these difficulties for tile development of micro tensile tester, fabricating micro specimens of functional materials and measuring their properties. This paper will review the related vigorous researches over the world in the recent decade and explain how to apply them to a design of the fester which is under our own development.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2004년도 춘계학술대회
• /
• pp.246-251
• /
• 2004

Nano-indentation is used for measuring mechanical properties of thin films such as elastic modulus and hardness. For ductile materials, pile-up around the indenter causes the calculation of inaccurate projected contact area. This phenomenon was found by measurement of indentation shape using an atomic force microscope. In present study finite element analysis of nano-indentation was performed to compensate the effects of pile-up on the contact area. The result of finite element analysis was compared with that of nano-indentation for a ductile material. The analysis has demonstrated that the true contact area is greater than that calculated by nano-indentation. It is verified that the consideration of the effects of pile-up in nanoindentation for ductile materials using the finite element method is reasonable.

• 한국염색가공학회지
• /
• 제2권2호
• /
• pp.1-6
• /
• 1990

In order to investigate the fine structural changes of poly (ethylene terephthalate) film by hydrazinolysis, PET was treated with hydrazine hydrate in methanol at $30^{\circ}C$ for various times. Initially apparent crystallite size and degree of orientation are increased and then, gradually decreased with hydrazinolysis. According to thermoluminescence measurement, trap site decreased by dissolution and then gradually increased with growth of defect in structure. Maximum peak temperature of tan and dynamic loss modulus E" upon hydrazinolysis shifted to the lower temperature in the progress of hydrazinolysis.ysis.

• Advances in materials Research
• /
• 제13권5호
• /
• pp.355-374
• /
• 2024

Several mathematical models describe the compressive behaviour of different types of concretes, but no specific one for foamed cellular concrete (FCC) has been developed. In this work, simple compression tests on FCC specimens of different mixes were conducted to study this material's compression behaviour curve until failure. Using continuous load and displacement measurement equipment, it was possible to obtain stress-strain curves up to peak for FCC of different strengths (from 1.20 to 47.34 MPa). Elastic modulus, compressive strength and failure strain values were also determined. Through the analysis of the mentioned curves, a mathematical model of them was obtained, through which it is possible to describe the compression behaviour of FCC up to failure. The comparison between the predicted curve against experimental data shows the effectiveness of the proposed model.

• Journal of Ceramic Processing Research
• /
• 제21권2호
• /
• pp.213-216
• /
• 2020

We investigated the optimal conditions for the manufacture of a rapid SiC heating element with increased durability for a flipchip bonder. In the moulding step prior to the sintering of the SiC heating element, a pressure of either 25 or 125 MPa wasapplied by uniaxial pressing to control the micropores; this was aimed at improving the resistance of the ultimate specimen. The moulded specimen was sintered by using a vacuum furnace with silicon as a sintering additive. The measurement of thehot modulus of rupture (HMOR) of the resulting SiC sintered body revealed that the HMOR was high. In addition, a methodfor protecting the heating element from the external environment was developed. A glassy coating layer was deposited on thesurface of the structure to improve the corrosion resistance of the sintered body; further, the performance of the coating layerwas verified through a neutral and acidic salt spray test. Finally, we established the optimal process conditions formanufacturing a rapid SiC heating element with improved corrosion resistance.

• 대한소아치과학회지
• /
• 제23권3호
• /
• pp.746-763
• /
• 1996

An alternative design to conventional class II cavity preparation for proximal carious lesions is the tunnel preparation. It preserves the marginal ridge intact, thus making it possible to maintain the natural contact relationship with the adjacent tooth and minimize tooth reduction. This in vitro study was purposed to evaluate the effect of the materials' elastic constants and shear-bond strength on the marginal ridge fracture resistance of teeth restored by the tunnel technique, and to find the materials of choice for tunnel restorations. $Resinomer^{(R)}$, $Ketac-silver^{(R)}$, $Miracle-Mix^{(R)}$, and Tytin were used as restorative material. The elastic constants of each restorative material were evaluated by ultrasonic pulse measurement. Young's modulus and bulk modulus of the restorative materials were evaluated in three specimens for each material type. The shear-bond strength of the restorative materials to the dentin surface was measured after thermocycling 400 times between 6 and $60^{\circ}C$, using ten specimens for each material type. For measuring marginal ridge strength, 60 sound extracted molar teeth were distributed into six groups by size. Sound molar teeth were used as a Control group and unfilled prepared teeth were grouped as Unrestored. Another four groups were named Resinomer group, Ketac-Silver group, Miracle Mix group, and Tytin group by type of restorative material. Tunnel cavity preparation was done with ' 1/2, 2, and 4 round burs in sequence. Initial access to proximal surface was made through an occlusal access preparation started at least 2mm from the marginal ridge, and the proximal opening was formed about 2.5mm below the marginal ridge. After restoration and thermocycling, marginal ridge strength was measured using a universal testing machine. The results were as follows: 1. The Young's modulus of $Tytin^{(R)}$ was 63.95 GPa, followed by $Ketac-Silver^{(R)}$ 27.60 GPa, $Miracle-mix^{(R)}$ 18.48 GPa, and $Resinomer^{(R)}$ 10.74 GPa showing significant differences between the groups(P<0.05). The bulk modulus of the materials showed the same order as Young's modulus. The value of $Tytin^{(R)}$ showed 59.57 GPa indicating that it will deform less than other materials under the same stress. It was followed by $Ketac-Silver^{(R)}$ 23.57 GPa, Miracle $Mix^{(R)}$ 12.50 GPa, and $Resinomer^{(R)}$ 11.60 GPa. 2. The Resinomer group had a shear-bond strength of 7.41 MPa which was significantly higher than those of the Ketac-Silver group (1.80 MPa) and the Miracle Mix group (2.84 MPa) (P<0.01). All the specimens of Tytin group detatched from the dentin surface during thermocycling. 3. The mean marginal ridge strength of the Unrestored group(46.14 kgf) was significantly lower than that of the Control group (84.24 kgf) (P<0.01). The marginal ridge strength of teeth restored by the tunnel technique was, in order, Ketac-Silver group 74.06 kgf, Miracle Mix group 73.36 kgf, Resinomer group 63.47 kgf, and Tytin group 58.76 kgf. The Ketac-Silver, Miracle Mix, and Resinomer groups showed no significant difference with the Control group (P>0.05), but the Tytin group showed significantly lower strength compared to the Control group(P<0.05). The results showed that the marginal ridge strength of the teeth restored by the tunnel technique was not significantly lower than that of sound teeth. They also demonstrated that the bonding strength of the restorative material to the tooth surface should be high and the modulus of elasticity should not be lower than that of the tooth in order to restore the marginal ridge strength to its natural condition.

• Korea-Australia Rheology Journal
• /
• 제12권2호
• /
• pp.101-105
• /
• 2000

The crystallization behavior of homo polypropylene (PP) and PP in the PP-poly($\varepsilon$-caprolactone) (PCL) blends during isothermal crystallization has been investigated using differential scanning calorimeter (DSC) and advanced rheometric expansion system (ARES). From the storage modulus data of the homo PP and PP-PCL blends during isothermal crystallization, the volume fraction of crystallized material ($X_t$) of the homo PP and PP in the PP-PCL blends was calculated using the various rheological models. The results of $X_t$ of the homo PP and PP in the PP-PCL blends from ARES measurement were compared with the results from DSC. The $X_t$ of the homo PP was found to be higher in the ARES measurement than in the DSC. The crystallization rate of the homo PP was found to be faster in the rheological measurements than in the thermal analysis. The $X_t$ of PP in the PP-PCL blends with various compositions was obtained from the thermal analysis and rheological measurements. The $X_t$ of PP in the PP-PCL blends obtained from the thermal analysis and rheological measurements are not consistent. This discrepancy of $X_t$ may be due to the morphological changes resulted from the different crystallization kinetics of PP in the PP-PCL blends.