• Analytical Science and Technology
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• v.25 no.6
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• pp.370-374
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• 2012

As for quality evaluation of paper records, it is very important to measure acidity and moisture in paper. In the case important paper records, it should be measured directly in field. But ISO standard analytical method would be limited to measure directly in field for quality evaluation of paper records until now. Therefore it could be to use mobile small NIR spectrometer for being analyzed by direct and non-invasive method in field. The wavelength range of small spectrometer has from 900 to 1700 nm, and the surface of paper could be measured by diffused reflected optical fiber probe. Thus, the acidity and moisture could be analyzed on the paper record with from 1970 to 2003. As the result, it could be confirmed to have each more than 0.9 as the correlation of acidity and moisture. Thus, it will be possible to develope the evaluation system of paper record with mobile small NIR spectrometer and optical fiber by the result.

• Korean Journal of Optics and Photonics
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• v.7 no.4
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• pp.348-356
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• 1996

A mobile CARS spectrometer is constructed to measure the instantaneous temperature of gases, of which software include the quick fit methods and a least square fitting method to obtain temperatures from the spectra. Two quick-fit-methods give smaller variance of temperatures than the least square fitting method even though they consume much shorter time to yield temperatures. The precision and accuracy of CARS temperature is measured in the graphite tube blackbody furnace in reference to a radiation pyrometer. The accuracy of the CARS temperature is $\pm$2% from 1000K to 2400K and the precision is $\pm$35K at 1600K with the most accurate quick-fit-method. As a demonstration of the instantaneous measurement, the spectrometer is applied for measurement of the turbulent combustion at a certain condition. eograms(HS) are made using a relatively small number of synthesized 2D images. The influence of aliasing artifacts caused by insufficient or improper sampling is presented, and a new sampling theory is proposed, which is used to making holographic stereograms. Also, the optical system for extension of viewing distance and viewing zone is proposed. Results of this analysis can be applied to design normal holographic stereograms and computer based holographic stereograms.

• Journal of Radiation Protection and Research
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• v.40 no.4
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• pp.194-201
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• 2015

We have investigated the EPR signal properties in 12 components of two mobile phones (LCD, OLED) using electron paramagnetic resonance (EPR) spectrometer in this study.EPR measurements were performed at normal atmospheric conditions using Bruker EXEXSYS-II E500 spectrometer with X-band bridge, and samples were irradiated by $^{137}Cs$ gamma-ray source. To identify the presence of radiation-induced signal (RIS), the EPR spectra of each sample were measured unirradiated and irradiated at 50 Gy. Then, dose-response curve and signal intensity variating by time after irradiation were measured. As a result, the signal intensity increased after irradiation in all samples except the USIM plastic and IC chip. Among the samples, cover glass(CG), lens, light guide plate(LGP) and diffusion sheet have shown fine linearity ($R^2$ > 0.99). Especially, the LGP had ideal characteristics for dosimetry because there were no signal in 0 Gy and high rate of increase in RIS. However, this sample showed weakness in fading. Signal intensity of LGP and Diffusion Sheet decreased by 50% within 72 hours after irradiation, while signals of Cover Glass and Lens were stably preserved during the short period of time. In order to apply rapidly EPR dosimetry using mobile phone components in large-scale radiation accidents, further studies on signal differences for same components of the different mobile phone, fading, pretreatment of samples and processing of background signal are needed. However, it will be possible to do dosimetry by dose-additive method or comparative method using unirradiated same product in small-scale accident.

• Korean Journal of Clinical Pharmacy
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• v.16 no.1
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• pp.23-27
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• 2006

Doxorubicin (DXR) is a type of anti-cancer drug called an 'anthracycline glycoside', It works by impairing DNA synthesis, a crucial feature of cell division, and thus is able to target rapidly dividing cells. Doxorubicin is a very serious anti-cancer medication with definite potential to do great harm as well as great good. A liquid chromatography-tandem mass spectroscopy (LC-MS/MS) method was developed to identify and quantify DXR in small-volume biological samples. After the addition of internal standard (IS, $5{\mu}L\;of\;1{\mu}M/ml$ daunorubicin methanol solution) into the serum sample, the drug and IS were extracted by methanol. Following vortex for a 1min and centrifugation at 15,000g for 10 min the organic phase was transferred and evaporated under a vacuum. The residue was reconstituted with $350{\mu}L$ of mobile phase and $10{\mu}L$ was injected into C18 column with mobile phase composed of 0.05M ammonium acetate (0.1 M acetic acid adjusted to pH 3.5) and acetonitrile (40:60, v/v). The flow rate was kept constant at $350{\mu}L/min$. The ions were quantified in the multiple reaction mode (MRM), using positive ions, on a triple quadrupole mass spectrometer. The lower limits of quantification for Doxorubicin in plasma and small tissues were approximately 0.5 ng/mL and 0.5 ng/mL respectively. Intra- and inter-assay accuracy (% of nominal concentration) and precision (% CV) for all analytes were within 15%, respectively.