• Title/Summary/Keyword: Microwave spectrum

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Luminescence characterization of $YVO_4$: $Eu^{3+}$, $Bi^{3+}$ red phosphor by rapid microwave heating synthesis (급속 microwave 열처리 방법으로 합성한 $YVO_4$: $Eu^{3+}$, $Bi^{3+}$ 적색 형광체의 발광 특성)

  • Park, W.J.;Song, Y.H.;Moon, J.W.;Yoon, D.H.
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.18 no.4
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    • pp.169-173
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    • 2008
  • $Eu^{3+}$ and $Bi^{3+}$ co-doped $YVO_4$ phosphors were produced by a microwave heating process. When the microwave heating method was synthesized,. the particle size was very small and the particles tended to agglomerate. However, as the heating time increased, the particle size increased and the agglomeration decreased. The emission spectrum exhibited a weak band for $^5D_0{\longrightarrow}^7F_1$ at 594.91 and 602.3 nm and strong sharp peaks at 616.7 and 620.0 nm due to the $^5D_0{\longrightarrow}^7F_2$ transition of $Eu^{3+}$. Microwave heating synthesis can provide a product without long time heating as well as good homogeneous distribution of activators.

Influence of Metal Particles on the Melt Behavior of PET/PP Fiber Bundles by Microwave Heating (마이크로파 가열에 의한 PET/PP 섬유다발의 용융거동에 금속입자의 영향)

  • Shin, Dong-Ho;Lee, Seung-Goo;Joo, Chang-Whan
    • Proceedings of the Korean Fiber Society Conference
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    • 2003.04a
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    • pp.150-153
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    • 2003
  • Microwaves belong to the portion of the electromagnetic spectrum with frequencies between 300MHz and 300GHz.$\^$1)/ In microwave processing, the energy is delivered directly to materials through molecular interaction with the electromagnetic field. This result in rapid heating throughout the material thickness with the reduced thermal gradients. If microwave is applied to fibrous materials, it can be reduced processing time. (omitted)

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Microwave-assisted Solvent-free Synthesis of Some Dimethine Cyanine Dyes, Spectral Properties and TD-DFT/PCM Calculations

  • Zhang, Xiang-Han;Wang, Lan-Ying;Zhai, Gao-Hong;Wen, Zhen-Yi;Zhang, Zu-Xun
    • Bulletin of the Korean Chemical Society
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    • v.28 no.12
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    • pp.2382-2388
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    • 2007
  • A series of dimethine cyanine dyes were synthesized in a fast, efficient and high yield by the condensation of quaternary salts with 1H-indole-3-carbaldehyde in the presence of piperidine under solvent-free microwave irradiation. The products were identified by 1H NMR, IR, UV-Vis spectra and elemental analysis. The absorption and fluorescence properties of these dyes were investigated both experimentally and theoretically. Calculations performed at a combination of time-dependent density functional theory (TD-DFT) and the polarizable continuum model (PCM) reproduced the π-π* type absorption bands of the dyes. Regression analysis was used for studying theoretical results of the absorption maxima in different solvents. Compared with experimental counterparts, estimated overall uncertainties in the absorption maxima were about ±2%.

Magnetic and Microwave Absorbing Properties of Ti-and Co-Substituted Barium Ferrite (BaFe12-2X TiXCoXO19)

  • Han-Shin Cho;Yong-Jin Kim;Sung-Soo Kim
    • Journal of Magnetics
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    • v.4 no.2
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    • pp.65-68
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    • 1999
  • The M-type barium ferrite ($BaFe_{12}O_{19}$) is well known magnetic material to be used as a permanent magnet due to its strong uniaxial anisotropy. The substitution of nonmagnetic $Ti^{+4}$ and magnetically weak $Co+^2ion for Fe^{+3}$ to its strong uniaxial anisotropy. The substitution of nonmagnetic $Ti^{+4}$ and magnetically weak $Co+^2ion for Fe^{+3}$ sublattices reduces the uniaxial anisotropy and those compounds open a new application field of noise suppressor at high frequencies. In this study, the magnetic and microwave absorbing properties are investigated in Ti-and Co-substituted barium ferrites ($BaFe_{12-2X} Ti_XCo_XO_{19}$). The saturated magnetization decreases linearly with the substitution of Ti and Co. The rapid drop in coercive force is observed with Ti and Co substitution upto x=1.2. The magnetic permeability spectrum shows the natural magnetic resonance in the specimens with small coercive force and large attenuation of microwave is predicted in those specimens at high frequencies (above 4 GHz).

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Measurement of Electron Density and Electron-neutral Collision Frequency Using Cutoff Probe Based on the Plasma Reactance Measurement

  • Yu, Gwang-Ho;Kim, Dae-Ung;Na, Byeong-Geun;Seo, Byeong-Hun;Yu, Sin-Jae;Kim, Jeong-Hyeong;Seong, Dae-Jin;Sin, Yong-Hyeon;Jang, Hong-Yeong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.184-184
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    • 2012
  • We proposed a new measurement method of cutoff probe using the reactance spectrum of the plasma in cutoff probe system instead of transmission spectrum. The high accurate reactance spectrum of the plasma which is expected in previous circuit simulation of cutoff probe [1] was measured by using the automatic port extension method of the network analyzer. The measured reactance spectrum is good agreement with E/M wave simulation result (CST Microwave Studio). From the analysis of the measured reactance spectrum based on the circuit modeling, not only the electron density but also electron-neutral collision frequency can be simply obtained. The obtained results of electron density and e-n collision frequency were presented and discussed in wide range of experimental conditions, together with comparison result with previous methods (a previous cutoff probe using transmission spectrum and a single langmuir probe).

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A Derivation of Comprehensive Protection Ratio and Its Applications for Microwave Relay System Networks

  • Suh Kyoung-Whoan
    • Journal of electromagnetic engineering and science
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    • v.6 no.2
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    • pp.103-109
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    • 2006
  • This paper suggests an efficient and comprehensive algorithm of the protection ratio derivation and illustrates some calculated results applicable to the initial planning of frequency coordination in the fixed wireless access networks. The net filter discrimination associated with Tx spectrum mask and overall Rx filter characteristic has been also examined to show the effect of the adjacent channel interference. The calculations for co-channel and adjacent channel protection ratios are performed for the current microwave frequency band of 6.7 GHz including Tx spectrum mask and Rx filter response. According to results, fade margin and co-channel protection ratio reveal 41.4 and 75.2 dB, respectively, for 64-QAM and 60 km at BER $10^{-6}$. It is shown that the net filter discrimination with 40 MHz channel bandwidth provides 28.9 dB at the first adjacent channel, which yields 46.3 dB of adjacent channel protection ratio. In addition, the protection ratio of 38 GHz radio relay system is also reviewed for millimeter wave band applications. The proposed method gives some advantages of an easy and systematic extension for protection ratio calculation and is also applied to frequency coordination in fixed millimeter wave networks.

Frequency modulation of a waveguide cavity cw IMPATT diode oscillator (도파관캐비티를 사용한 임팻다이오드 발진기의 주파수변조특성)

  • 윤현보
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.12 no.6
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    • pp.1-4
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    • 1975
  • This paper dells with the impedance variations of the IMPATT diode depending upon the small a.c. coomponent superimposed on the d.c. bias. The frequency deviation of the modulated wave is measured using a carrier null method on microwave spectrum analyser. Frequency modulation is achieved by the weack a.c. signal superimposed on the d.c. bias. The bandwidth rapidly increase with increasing modulation signal magnitude for constant modulation frquency and slightly decrease with decreasing modulation frequency for constant modulation signal magnitude.

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Optically Detected Magnetic Resonance with Nitrogen-Vacancy Spin Ensemble in Diamond

  • Lee, Hyun Joon;Shim, Jeong Hyun
    • Journal of the Korean Magnetic Resonance Society
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    • v.22 no.2
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    • pp.40-45
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    • 2018
  • We report Optically-Detected Magnetic Resonance (ODMR) study on Nitrogen-Vacancy (NV) centers in diamond. The experiment can easily be conducted with basic optics and microwave components. A diamond crystal having a high-density NV center is suitable for the ODMR study. The magnetic field dependence of ODMR spectrum allowed us to determine the orientation of the diamond crystal. In addition, we measured the variation of the ODMR spectrum as a function of the excitation laser power. Thermal heating induced by optical absorption caused the monotonic decrease of zero field splitting. The contrast of the ODMR peak, however, increased and, then, began to decrease, indicating the optimal laser power for recording the ODMR spectrum.