• Title/Summary/Keyword: Microwave Properties

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Characteristics of Microwave-Assisted Extraction for Grape Seed Components with Different Solvents (추출용매에 따른 포도씨 성분의 마이크로웨이브 추출 특성)

  • Lee Eun-Jin;Kwon Joong-Ho
    • Food Science and Preservation
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    • v.13 no.2
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    • pp.216-222
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    • 2006
  • Microwave energy (2450 MHz) was applied to extract health-effective component (HEC) from grape seed. Three different solvents approved for grape seed extract such as water, ethanol and acetone, were confirmed in their microwave-heating properties and by which extraction efficiencies were determined. Microwave-assisted extraction (MAE) was performed under different parameters; microwave power : (0, 50, 100 and 150), time : (1, 3, 5, 7, and 9 min), the sample to solvent ratio : (1:20, 1:10, 1:5 and 1:2.5), and particle size(whole, 20, 40 and 60 mesh) and the subsequent extracts were used for determining their physicochemical properties, such as total yield : (TY), total phenolics : (TP), catechin content : (CC), electron donating ability : (EDA), and browning color. The heating properties of solvent demonstrated the optimal ranges of microwave and time as 100 W and 2 to 6 min. The TY and HFC content were higher with increasing powers in water and ethanol solvent, while HFC content were lower in acetone at over 100 W. The longer of extraction time up to 5 min, the higher extraction efficiency. Based upon the overall MAE efficiency and solvent recovery, it was found optimal to use 10 times volume of ethanol for 10 mesh of seed particle at 100 W.

Microwave Properties of Ag Conducting Paste with Various Preparation Conditions (Ag가 함유된 전도성 도료의 제조 조건에 따른 고주파 특성)

  • Park, Sang-Hoon;Kim, Jeong-Pyo;Seong, Won-Mo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.18 no.9
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    • pp.827-832
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    • 2005
  • Dual band internal antennas were fabricated with Ag conducting paste of various preparation conditions and different print thickness by silk screen print. We have investigated microwave properties were compared Ag conducting paste antenna with copperplate antenna at 800 MHz and 1,800 MHz. Gain of Ag conducting paste antenna was improved when preparation conditions were the single size Ag particle, using dry type resin and high Ag containing percent. However, it was lower than that of copperplate antenna within $0.1\~2.0dBi$ at 800MHz. In addition, it was improved at 800MHz when thickness of Ag conducting paste was printed more than skin depth but it was held after critical print thickness. On the other hand, it was reached level of copperplate antenna at 1,800MHz.

A study on the Microwave Dielectric Properties of Ba(Mg,Co)(Ta,Nb)$O_3$ Ceramics (Ba(Mg,Co)(Ta,Nb)$O_3$ 세라믹의 마이크로파 유전특성에 관한 연구)

  • Lee, Moon-Kee;Chung, Jang-Ho;Bae, Seon-Gi;Lee, Young-Hi
    • Proceedings of the KIEE Conference
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    • 1998.11c
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    • pp.752-754
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    • 1998
  • $Ba(Mg_{(1-x)}Co_x)_{1/3}(Ta_{(1-x)}Nb_x)_{2/3}O_3$ ($x=0.3{\sim}0.6$) ceramics were prepared by the conventional mixed oxide method. The sintering temperature and time were of $1400{\sim}1575[^{\circ}C]$,5[hr.] respectively. The structural and microwave dielectric Properties were investigated with composition ratio and sintering temperature. And then the application for the microwave dielectric resonator was investigated.

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Microwave-assisted Solvent-free Synthesis of Some Dimethine Cyanine Dyes, Spectral Properties and TD-DFT/PCM Calculations

  • Zhang, Xiang-Han;Wang, Lan-Ying;Zhai, Gao-Hong;Wen, Zhen-Yi;Zhang, Zu-Xun
    • Bulletin of the Korean Chemical Society
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    • v.28 no.12
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    • pp.2382-2388
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    • 2007
  • A series of dimethine cyanine dyes were synthesized in a fast, efficient and high yield by the condensation of quaternary salts with 1H-indole-3-carbaldehyde in the presence of piperidine under solvent-free microwave irradiation. The products were identified by 1H NMR, IR, UV-Vis spectra and elemental analysis. The absorption and fluorescence properties of these dyes were investigated both experimentally and theoretically. Calculations performed at a combination of time-dependent density functional theory (TD-DFT) and the polarizable continuum model (PCM) reproduced the π-π* type absorption bands of the dyes. Regression analysis was used for studying theoretical results of the absorption maxima in different solvents. Compared with experimental counterparts, estimated overall uncertainties in the absorption maxima were about ±2%.

Microwave Dielectric Properties of BaO-$(Nd,\;Bi)_2O_3-Tio_2$ Ceramic for Microwave Resonators (고주파 공진기용 BaO-$(Nd,\;Bi)_2O_3-Tio_2$계 세라믹스의 마이크로파 유전특성)

  • Yoon, Jung-Rag;Lee, Heun-Yong
    • Proceedings of the KIEE Conference
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    • 1997.11a
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    • pp.320-323
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    • 1997
  • The microwave dielectric properties of X Ba0-$0.15(Nd_{0.87}Bi_{0.13})_2O_3$-(0.85-X) $TiO_2$ ($X=0.13{\sim}0.17$) and 0.16Ba0-$0.15(Bi_xNd_{1-x})_2O_3-0.69TiO_2$ ($X=0.10{\sim}0.16$) ceramics were investigated. Dielectric constant, quality factor and temperature coefficient of resonant frequency of 0.16Ba0-$0.15(Nd_{0.87}Bi_{0.13})_2O_3-0.69TiO_2$ ceramics sintered at $1320^{\circ}C$ for 2 hours were 89.2, 1920(at 4GHz) and 5.2ppm/$^{\circ}C$, respectively.

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One-step Microwave Synthesis of Hierarchical Structured LiFePO4 using Citric Acid

  • Wu, Mihye;Choi, Sungho;Kang, Yongku;Jung, Ha-Kyun
    • Bulletin of the Korean Chemical Society
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    • v.35 no.10
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    • pp.2901-2905
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    • 2014
  • The hierarchical-structured $LiFePO_4$ cathode materials were synthesized by one-step microwave synthesis, and their electrochemical properties were investigated. Addition of citric acid during the reaction lead to the formation of hierarchical structured $LiFePO_4$, which has both nano- and micron-characteristics advantageous for energy density and electrode fabrication. Adjusting the molar ratio of Fe to citric acid enhanced the electrochemical properties of $LiFePO_4$.

Magnetic and Microwave Absorbing Properties of Ti-and Co-Substituted Barium Ferrite (BaFe12-2X TiXCoXO19)

  • Han-Shin Cho;Yong-Jin Kim;Sung-Soo Kim
    • Journal of Magnetics
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    • v.4 no.2
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    • pp.65-68
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    • 1999
  • The M-type barium ferrite ($BaFe_{12}O_{19}$) is well known magnetic material to be used as a permanent magnet due to its strong uniaxial anisotropy. The substitution of nonmagnetic $Ti^{+4}$ and magnetically weak $Co+^2ion for Fe^{+3}$ to its strong uniaxial anisotropy. The substitution of nonmagnetic $Ti^{+4}$ and magnetically weak $Co+^2ion for Fe^{+3}$ sublattices reduces the uniaxial anisotropy and those compounds open a new application field of noise suppressor at high frequencies. In this study, the magnetic and microwave absorbing properties are investigated in Ti-and Co-substituted barium ferrites ($BaFe_{12-2X} Ti_XCo_XO_{19}$). The saturated magnetization decreases linearly with the substitution of Ti and Co. The rapid drop in coercive force is observed with Ti and Co substitution upto x=1.2. The magnetic permeability spectrum shows the natural magnetic resonance in the specimens with small coercive force and large attenuation of microwave is predicted in those specimens at high frequencies (above 4 GHz).

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Effects of Food Height for Microwave Blanching on Vegetables and Reheating on Cooked Rice (식품의 높이 변화가 채소류의 마이크로파 데치기 및 쌀밥의 데우기에 미치는 영향)

  • Kum, Jun-Seok;Han, Ouk
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.27 no.2
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    • pp.281-285
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    • 1998
  • For the purpose of improving the qualities of carrot, spinach and cooked rice, the effects of food height(0mm: H0, 5mm: H5, 10mm: H10, 15mm: H15) for microware blanching and reheating on physicochemical properties were investigated. In carrot blanching, color values of each treatment were not different, and cutting forces of microware blanching carrots were decreased as carrot height increased. In spinach blanching, the shape of orignal form was changed as height increased. In cooked rice reheating, H10 had the highest overall acceptance score. Physicochemical properties were changed by food hight of microwave blanching and reheating on food.

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The effect of g1ass frit arid BaWO$_4$ Addition Microwave Dielectric Prperties of BaTiO$_3$-3TiO$_2$ Ceramics (Glass 첨가 및 BaWO$_4$ 첨가에 따른 BaTiO$_3$-3TiO$_2$ 세라믹스의 고주파 유전 특성)

  • 윤중락;김지균;이헌용
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.335-338
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    • 1998
  • The effect of glass flit addition on microwave dielectric properties of BaTiO$_3$-3TiO$_2$ ceramic was studied. Addition of glass frit to this system obtained sintered sample below sintering temperature 105$0^{\circ}C$. At BaTiO$_3$-3TiO$_2$+ g1ass frit 3wt% + BaWO$_4$6 wt%m, this ceramic showed excellent microwave properties of dielectric constant 34, Q$\times$f 8,100, temperature coefficient of resonant frequency 4 ppm/$^{\circ}C$ .

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