• Title/Summary/Keyword: Microstructures and mechanical properties

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Fabrication of Quasi-crystal Strengthened Aluminum Composites by Mechanical Milling Process (기계적 밀링 공정을 이용한 준결정 강화 알루미늄 복합재료의 제조)

  • Jang Woo Kil;Shin Kwang Seon
    • Journal of Powder Materials
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    • v.12 no.3
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    • pp.208-213
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    • 2005
  • Aluminum matrix composites strengthened by the quasi-crystalline (QC) phase were developed in the present study. The icosahedral $Al_{65}Cu_{20}Fe_{15}$ phase was produced by gravity casting and subsequent heat treatment. The mechanical milling process was utilized in order to produce the Al/QC composite powders. The microstructures of the composite powders were examined by optical microscopy (OM) and scanning electron microscopy (SEM). The composite powders were subsequently canned, degassed and extruded in order to produce the bulk composite extrusions with various volume fractions of QC. The microstructure and mechanical properties of the extrusions were examined by OM, SEM, Vickers hardness tests and compression tests. It was found that the microstructures of the Al/QC composites were uniform and the mechanical properties could be significantly improved by the addition of the QC phase.

Mechanical properties and microstructures of stabilised dredged expansive soil from coal mine

  • Chompoorat, Thanakorn;Likitlersuang, Suched;Sitthiawiruth, Suwijuck;Komolvilas, Veerayut;Jamsawang, Pitthaya;Jongpradist, Pornkasem
    • Geomechanics and Engineering
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    • v.25 no.2
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    • pp.143-157
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    • 2021
  • Expansive soil is the most predominant geologic hazard which shows a large amount of shrinkage and swelling with changes in their moisture content. This study investigates the macro-mechanical and micro-structural behaviours of dredged natural expansive clay from coal mining treated with ordinary Portland cement or hydrated lime addition. The stabilised expansive soil aims for possible reuse as pavement materials. Mechanical testing determined geotechnical engineering properties, including free swelling potential, California bearing ratio, unconfined compressive strength, resilient modulus, and shear wave velocity. The microstructures of treated soils are observed by scanning electron microscopy, x-ray diffraction, and energy dispersive spectroscopy to understand the behaviour of the expansive clay blended with cement and lime. Test results confirmed that cement and lime are effective agents for improving the swelling behaviour and other engineering properties of natural expansive clay. In general, chemical treatments reduce the swelling and increase the strength and modulus of expansive clay, subjected to chemical content and curing time. Scanning electron microscopy analysis can observe the increase in formation of particle clusters with curing period, and x-ray diffraction patterns display hydration and pozzolanic products from chemical particles. The correlations of mechanical properties and microstructures for chemical stabilised expansive clay are recommended.

Evaluation of Microstructures and Mechanical Property of Variously Heat Treated 0.85% Carbon Steel by Magnetic Method (자기적 방법에 의한 0.85% 탄소강의 열처리에 따른 미세조직 및 기계적 성질 평가)

  • Byeon, Jai-Won;Kwun, S.I.
    • Korean Journal of Materials Research
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    • v.13 no.2
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    • pp.81-87
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    • 2003
  • Microstructures and mechanical properties of variously heat treated 0.85% carbon steel(eutectoid steel) were evaluated by magnetic property measurements. Microstructural analysis (pearlite interstellar spacing), measurement of mechanical properties(Rockwell hardness, yield stress, fracture stress) and magnetic properties(coercivity, remanence, hysteresis loss, saturation magnetization) were performed to clarify mutual relationships among these parameters. Water quenched specimens with martensite structure showed much higher coercivity and remanence than air cooled or furnace cooled specimens with pearlite structure. The linear dependence of coercivity and remanence on pearlite interlamellar spacing as well as on Rockwell hardness, yield stress and fracture stress was observed in the pearlitic steel. Hysteresis loss and saturation magnetization showed no distinct trend with pearlite interlamellar spacing.

Development of Microstructures and Mechanical Properties in Differential Speed Rolled Ni-30Cr Alloy (이주속압연된 Ni-30Cr 합금의 미세조직과 기계적 특성 발달)

  • Im, Yong-Deok;Park, Hyung-Ki;Song, Kuk-Hyun
    • Korean Journal of Materials Research
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    • v.25 no.3
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    • pp.149-154
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    • 2015
  • We evaluated the developed microstructures and mechanical properties of a severely plastically deformed Ni-30Cr alloy. Normal rolling and differential speed rolling were used as deformation processes, and the thicknesses of the specimens were reduced to 68 % of the original thickness after holding at $700^{\circ}C$ for 10 min and annealing at $700^{\circ}C$ for 40 min to obtain a fully recrystallized microstructure. Electron backscattering diffraction was used to analyze the characteristic distribution of the grain boundaries on the deformed and annealed specimens. Differential speed rolling was more effective for refining grains in comparison with normal rolling. The grain size was refined from 33 mm in the initial material to 8.1 mm with normal rolling and 5.5 mm with differential speed rolling. The more refined grain in the differential-speed-rolled material directly resulted in increases in the yield and tensile strengths by 68 % and 9.0%, respectively, compared to normal rolling. We systematically explain the relationship between the grain refinement and mechanical properties through a plastically deformed Ni-30Cr alloy based on the development of a deformation texture. The results of our study show that the DSR process is very effective when used to enhance the mechanical properties of a material through grain refinement.

A Study on the Mechanical Properties with the Strain rate and Strain for Aluminum 6061 Alloy in Hot Forging (알루미늄 6061 합금의 열간단조시 변형율속도 및 변형율에 따른 기계적 성질에 관한 연구)

  • 김정식;이영선;김용조;이정환
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2002.05a
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    • pp.154-158
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    • 2002
  • The mechanical properties of Al 6061 excluded bar were deformed in high temperature with the variable deformation conditions and characterized by the tensile test. Three types of different strain rate were experimentally performed by using hydraulic press, crank press and hammer and two types of the nominal strain 0.5 and 0.8 were achieved. To decide optimum forging process, the relationship among the strain rate, strain and mechanical properties was explained by analyzing the microstructures of the forged and heat heated parts. The strength was deeply related with the strain rate due to the dynamic recrystallization (DRX) in hot forging, and the best forging condition was presented in Al 6061 alloy.

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Effect of Third Elements on the Microstructures and Mechanical Properties of Ti-Al Intermetallic Compounds (Ti-Al 금속간화합물의 미세조직 및 기계적 성질에 미치는 제3원소의 영향)

  • Choi, Chang-Woo;Hong, Chun-Pyo
    • Journal of Korea Foundry Society
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    • v.12 no.2
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    • pp.139-148
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    • 1992
  • The mechanical properties of Ti-Al intermetallic compounds which contain Mn, Zr, or Cr as the third element have been evaluated by means of hardness and compression tests. Microstructures have also been examined using an optical microscope. The cast structures of Ti-Al alloys are coarsened and the lamellar volume fraction is increased by the additions of Mn or V, but the cast structures are refined by the addition of Zr. Hardness tests of room temperature and compression tests at $600^{\circ}C$ showed that the mechanical properties of Ti-Al alloys were mainly dependent on the volume fraction of the ${\alpha}_2$ phase, grain size and solid solution hardening. However according to the compression test at $1000^{\circ}C$, the yield strength of Ti-Al alloys decreased with an increase in Mn or Cr content, but increased with an increase in the Zr content.

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Formation of Ultrafine Grain and Recrystallization in 1050 Al Alloy Rolled at Cryogenic Temperature (극저온 압연한 Al 1050의 결정립 미세화 및 재결정 거동)

  • 이영범;송형락;남원종
    • Transactions of Materials Processing
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    • v.13 no.5
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    • pp.455-460
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    • 2004
  • The deformation and annealing behaviors of a 1050 Al alloy deformed at cryogenic temperature were investigated, focusing on the evolution of microstructures and mechanical properties. Especially, the effects of annealing temperature, $150~300^{\circ}C$, on microstructures and mechanical properties of the sheets received reduction of 88% at cryogenic temperature were investigated. The significant change in mechanical properties with the annealing temperatures of $200~300^{\circ}C$ would be attributed to the variations in the volume fraction of recrystallized grains and coarse equiaxed grains.

The Expectation for Material Properties of Microstructure by Application of Dynamic Response Characteristics (동적 응답 특성을 활용한 미세구조의 물성 분포에 대한 예측)

  • Lee, Jeong-Ick;Yeo, Moon-Su
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.3
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    • pp.580-586
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    • 2008
  • This paper addresses the prediction of the material property continuities of a microstructure. Prediction was made by measuring the dynamic responses distribution of the fabricated materials used in the microstructures. When these distributional material properties were used in estimating the mechanical performances of microstructures, the differences between the computer simulation and the experimental result of microstructures could be reduced and their reliability design could be made.

Effect of Extrusion Conditions on Microstructures and Mechanical Properties of AM80 Magnesium Alloys (AM80 마그네슘 합금의 미세조직 및 기계적 특성에 대한 압출조건의 영향)

  • Lee, S.K.;Kim, D.H.;Kim, D.H.;Lim, S.G.
    • Transactions of Materials Processing
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    • v.27 no.6
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    • pp.379-385
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    • 2018
  • This study investigated the effect of extrusion conditions on microstructures and mechanical properties of AM80 magnesium alloys. The billets of magnesium alloy used for hot extrusion were prepared by permanent mold casting method, and its extrusion was hot direct extrusion with different extrusion conditions. The results of microstructural analysis showed that the main phases in the as-casted alloys were ${\alpha}-Mg$, ${\beta}-Mg_{17}Al_{12}$, and lamella $Mg_{17}Al_{12}$. Hot extrusion results, The tensile strength of the most soundly manufactured extruded bars (extrusion temp: $350^{\circ}C$, extrusion ratio: 27:1, ram speed: 2mm/s) was approximately 327MPa at room temperature. The increase in the mechanical properties of hot-extruded alloys was as a result of grain refinement by dynamical recrystallization during hot extrusion.

Improvement of Mechanical Properties of UV-curable Resin for High-aspect Ratio Microstructures Fabricated in Microstereolithography (마이크로광조형에서 고 세장비 구조물 집적화 가공을 위한 UV 경화성 수지의 물성 개선)

  • Lee, Su-Do;Choi, Jae-Won;Park, In-Beak;Ha, Chang-Sik;Lee, Seok-Hee
    • Journal of the Korean Society for Precision Engineering
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    • v.24 no.12
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    • pp.119-127
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    • 2007
  • Recently, microstructures fabricated using microstereolithography technology have been used in the biological, medical and mechanical fields. Microstereolithography can fabricate real 3D microstructures with fine features, although there is presently a limited number of materials available for use in the process. Deformation of the fine features on a fabricated microstructure remains a critical issue for successful part fabrication, and part deformation can occur during rinsing or during fabrication as a result of fluid flow forces that occur during movement of mechanical parts of the system. Deformation can result in failure to fabricate a particular feature by breaking the feature completely, spatial deflection of the feature, or attaching the feature to neighboring microstructures. To improve mechanical strength of fabricated microstructures, a clay nanocomposite can be used. In particular, a high-aspect ratio microstructure can be fabricated without distortion using photocurable liquid resin containing a clay nanocomposite. In this paper, a clay nanocomposite was blended with a photocurable liquid resin to solve the deformation problem that occurs during fabrication and rinsing. An optimal mixture ratio of a clay nanocomposite was found through tensile testing and the minimal allowable distance between microstructures was found through fabrication experimentation. Finally, using these results, high-aspect ratio microstructures were fabricated using a clay nanocomposite resin without distortion.