• Title/Summary/Keyword: Microstructure analysis

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Static analysis of cutout microstructures incorporating the microstructure and surface effects

  • Alazwari, Mashhour A.;Abdelrahman, Alaa A.;Wagih, Ahmed;Eltaher, Mohamed A.;Abd-El-Mottaleb, Hanaa E.
    • Steel and Composite Structures
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    • v.38 no.5
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    • pp.583-597
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    • 2021
  • This article develops a nonclassical model to analyze bending response of squared perforated microbeams considering the coupled effect of microstructure and surface stress under different loading and boundary conditions, those are not be studied before. The corresponding material and geometrical characteristics of regularly squared perforated beams relative to fully filled beam are obtained analytically. The modified couple stress and the modified Gurtin-Murdoch surface elasticity models are adopted to incorporate the microstructure as well as the surface energy effects. The differential equations of equilibrium including the Poisson's effect are derived based on minimum potential energy. Exact closed form solution is obtained for bending behavior of the proposed model considering the classical and nonclassical boundary conditions for both uniformly distributed and concentrated loads. The proposed model is verified with results available in the literature. Influences of the microstructure length scale parameter, surface energy, beam thickness, boundary and loading conditions on the bending behavior of perforated microbeams are investigated. It is observed that microstructure and surface parameters are vital in investigation of the bending behavior of perforated microbeams. The obtained results are supportive for the design, analysis and manufacturing of perforated nanobeams that commonly used in nanoactuators, nanoswitches, MEMS and NEMS systems.

Atomic Scale Investigation of TRIP Steels (변태 유기 소성강(TRIP steel)의 미세구조와 원자 단위 분석)

  • Lim, N.S.;Kang, J.S.;Kim, S.I.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.273-276
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    • 2008
  • In this study, microstructure and distribution of alloy elements were investigated in thermo-mechanically processed C-Mn-Si transformation induced plasticity (TRIP) steels. The microstructures of TRIP steels were investigated by using advanced analysis techniques, such as three dimensional atom probe tomography (3D-APT). At first, the microstructure was observed by using TEM. TEM results revealed that microstructure of C-Mn-Si TRIP steel was composed of ferrite, bainte, and retained austenite. 3D-APT was used to characterize atomic-scale partitioning of added elements at the phase interface. In the retained austenite phase, Ti and B were enriched with C. However, there was no fluctuation of Mn and Si concentration across the interface. Through these analysis techniques, the advanced characteristics of constituent microstructure in C-Mn-Si TRIP steels were identified.

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Prediction of microstructure during high temperature forming of Ti-6Al-4V alloy (Ti-6Al-4V 합금의 고온성형 시 미세조직 예측에 관한 연구)

  • 이유환;신태진;황상무;이종수
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.05a
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    • pp.57-60
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    • 2003
  • The purpose of this study is to investigate the high temperature deformation behavior of Ti-6Al-4V alloy and to predict the final microstructure under given forming conditions. Equiaxed and widmanstatten of Ti-6Al-4V alloys were prepared as initial microstructure and the compression tests were performed to obtain the flow curves at high temperatures (700∼1100$^{\circ}C$) and various strain rates (10$\^$-4/∼10$^2$/s). Form the results of compression test various parameters such as strain rate sensitivity (m) and activation energy (Q) were calculated and used to establish constitutive equations. To predict the final microstructure after forming, finite element analysis was performed considering the microstructural parameters such as the grain size and the volume fraction of second phase.

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Microstructure analysis of 8 ㎛ electrolytic Cu foil in plane view using EBSD and TEM

  • Myeongjin Kim;Hyun Soon Park
    • Applied Microscopy
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    • v.52
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    • pp.2.1-2.6
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    • 2022
  • With the lightening of the mobile devices, thinning of electrolytic copper foil, which is mainly used as an anode collection of lithium secondary batteries, is needed. As the copper foil becomes ultrathin, mechanical properties such as deterioration of elongation rate and tear phenomenon are occurring, which is closely related to microstructure. However, there is a problem that it is not easy to prepare and observe specimens in the analysis of the microstructure of ultrathin copper foil. In this study, electron backscatter diffraction (EBSD) specimens were fabricated using only mechanical polishing to analyze the microstructure of 8 ㎛ thick electrolytic copper foil in plane view. In addition, EBSD maps and transmission electron microscopy (TEM) images were compared and analyzed to find the optimal cleanup technique for properly correcting errors in EBSD maps.

Microstructure Generation and Linearly Elastic Characteristic Analysis of Hierarchical Models for Dual-Phase Composite Materials (이종 입자복합재의 미세구조 생성과 계층적 모델의 선형 탄성적 응답특성 해석)

  • Cho, Jin-Rae
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.31 no.3
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    • pp.133-140
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    • 2018
  • This paper is concerned with the 2-D micostructure generation for $Ni-A{\ell}_2O_3$ dual-phase composite materials and the numerical analysis of mechanical characteristic of hierarchical models of microstructure which are defined in terms of the scale of microstructure. The microstructures of dual-phase composite materials were generated by applying the mathematical RMDF(random morphology description functions) technique to a 2-D RVE of composite materials. And, the hierarchical models of microstructure were defined by the number of Gaussian points. Meanwhile, the volume fractions of metal and ceramic particles were set by adjusting the level of RMD functions. The microstructures which were generated by RMDF technique are definitely random even though the total number of Gaussian points is the same. The randomly generated microstructures were applied to a 2-D beam model, and the variation of normal and shear stresses to the scale of microstructure was numerically investigated. In addition, through the crack analyses, the influence of RMDF randomness and Gauss point number on the crack-tip stress is investigated.

FE Analysis of Hot Forging Process and Microstructure Prediction for Lower Arm Connector (로워암 커넥터 열간단조 공정의 유한요소해석 및 미세조직 예측)

  • Park, Jong-Jin;Hwang, Han-Sub;Lee, Sang-Joo;Hong, Seung-Chan;Lim, Sung-Hwan;Lee, Kyung-Sub;Lee, Kyung-Jong
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.27 no.7
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    • pp.1243-1250
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    • 2003
  • In the present study, hot forging process for a lower arm connector of an automobile was investigated. An FEM code, DEFORM-3D, was used to analyze the process and the process parameters, such as temperature, strain and strain rate, were obtained. The microstructure of the connector was predicted by applying the Sellars and Yada microstructure evolution models to the process parameters. The method of microstructure prediction used in the present study seems to be effective for the quality assurance of a forged automotive product.

Reheating Process and FEM Analysis of Inductive Heating (재가열 공정과 유도 가열의 FEM 해석)

  • 손영익
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.03b
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    • pp.195-198
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    • 1999
  • For the thixoforming process beside an existing solidus-liquidus interval, the reheating conditions to obtain the globular microstructure are very important. It relies on the control of globular microstructure of semi-solid alloys that contain non-dendritic particles. To obtain the globular microstructure in cross section of billet, the optimal design of the induction coil is necessary. Therefore, in this paper the optimal coil design to minimize electromagnetic end effect will be proposed. The results of coil design were also applied to the reheating process to obtain a fine globular microstructure. Finally, reheating data base of aluminum alloys for thixoforming and FEM model for induction heating based on the optimal coil design have been proposed.

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Analytical Method for Determination of Microstructure of SBR and SBR Content in Blended Rubber Composites Using Pyrolytic Technique

  • Eunji Chae;Sung-Seen Choi
    • Elastomers and Composites
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    • v.57 no.4
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    • pp.188-196
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    • 2022
  • Styrene-butadiene rubber(SBR) is a copolymer of styrene and butadiene. It is composed of 1,2-unit, 1,4-unit, and styrene, and its properties are dependent on its microstructure. In general, rubber composites contain a single rubber or a blended rubber. Similarly, SBR is used by mixing with natural rubber(NR) and butadiene rubber(BR). The composition of a rubber article affects its physical and chemical properties. Herein, an analytical method for determining the microstructure of SBR using via pyrolysis is introduced. Pyrolysis-gas chromatography/mass spectrometry is widely used to analyze the microstructure of polymeric materials. The microstructure of SBR can be determined by analyzing the principal pyrolysis products formed from SBR, such as 4-vinylcyclohexene, styrene, 2-phenylpropene, 3-phenylcyclopentene, and 4-phenylcyclohexene. An analytical method for determining the composition of SBR/NR, SBR/BR, and SBR/NR/BR blends via pyrolysis is introduced. The composition of blended rubber can be determined by analyzing the principal pyrolysis products formed from each rubber component.

A Novel Method for 3D Surface and Solid Construction Analysis of Fabric Microstructure (직물 미세구조의 3차원 표면 및 솔리드 형성 방법)

  • Lee, Ye-Jin;Lee, Byung-Cheol
    • Korean Journal of Human Ecology
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    • v.21 no.3
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    • pp.539-550
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    • 2012
  • In-depth knowledge of fabric microstructure is essential for understanding clothing comfort since it plays a significant role in heat and mass transfer between the human body and clothing. In this study, a novel method was employed for investigating 3D surfaces and solid construction characteristics of specific fabrics by using a reverse engineering technique. The surface construction data were obtained by a confocal laser scanning microscope and then manipulated by a 3D analysis program. Triangle mesh was used for connecting each 3D point, with clouds and fabric surface characteristics created by rendering techniques. For generating a 3D solid model, determinants of radius of curvature was used. According to the proposed method, actual surface expression of the real fabric was achieved successfully. The results from this methodology can be applied to the detailed analysis of clothing comfort that is highly influenced by the microstructure of the fabric.