• Journal of the Korean Ceramic Society
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• v.29 no.11
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• pp.912-918
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• 1992

Microstructure evolution including morphological change in the vicinity of the electrodes, porosity change and grain boundary migration was observed in polycrystalline CoO subject to electric fields at 1100 and 121$0^{\circ}C$ in air. At the cathode, the transported cations react with oxygen in the surrounding to form new lattices, while, at the anode, the reverse reaction occurs leading to lattice annihilation. Lattice formation also takes place at the surface of pores near the cathode inducing pore-filling effect. Grain boundary migration was found bo be enhanced or retarded depending on the field direction. It is therefore implied that the driving force of grain boundary migration is the vectorial sum of the curvature-induced chemical potential gradient and the electric field applied.

• Journal of Powder Materials
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• v.3 no.4
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• pp.266-270
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• 1996

The microstructure evolution during sintering of a compact being composed of three layers of (WC-15%Co)/Fe powder mixture with different Fe contents has been observed. The Fe contents in the respective (WC-15%Co)/Fe layers were varied by 20%. 50%, and 90% in sequence by volume from a top layer to a bot- tom layer. The sintering temperatures and times were varied from 110$0^{\circ}C$ to 125$0^{\circ}C$ and from 1 h to 4 h, The compact layer was not densified below 120$0^{\circ}C$ in 4 h. Appropriate sintering temperature and time conditions for making a multi-layered hard metal compact were determined as 125$0^{\circ}C$ and 3 h, respectively.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.222-225
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• 2006

The effect of lubrication on the development of textures and Microstructure was studied by different lubricating condition during hot rolling of AA1050 aluminum alloy. Hot rolling without lubrication led to the evolution of the pronounced through-thickness texture gradients, whereas hot rolling with lubrication gave rise to the formation of uniform rolling texture in the whole thickness layer. The variation of texture and microstructure according to hot rolling condition are investigated by X-ray diffractometer (XRD) and Electron Back-Scattered Diffraction (EBSD). The experimental results were discussed base on the finite element method (FEM) simulation. FEM calculation reveals that a larger friction between roll and sheet causes the deviated strain state from a plane strain leading to the formation of shear textures in the thickness layers close to the surface.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2004.10a
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• pp.19-22
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• 2004

A numerical system to extract effective elastic properties of polycrystalline thin-films for MEMS devices is already developed. In this system, the statistical model based on lattice system is used for modeling the microstructure evolution simulation and the key kinetics parameters of given micrograph, grain distributions and deposition process can be extracted by inverse method proposed in the system. In this work, the effective elastic properties of polysilicon, $BaTiO_3\;and\;ZrTiO_4$ are extracted using this system and by employing the fraction of the potential site($f_P$) as a kinetics parameter for the microstructure evolution, the statistical tendency of these materials is studied.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.10a
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• pp.207-210
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• 2004

The deformation behavior of copper during equal channel angular pressing (ECAP) was calculated using a three-dimensional version of a constitutive model based on the dislocation density evolution. Finite element simulations of the variation of the dislocation density and the dislocation cell size with the number of ECAP passes are reported. The calculated stress, strain and cell size are compared with the experimental data for Cu deformed by ECAP in a modified Route C regime. The results of FEM analysis were found to be in good agreement with the experiments. After a rapid initial decrease down to about 200 nm in the first ECAP pass, the average cell size was found to change little with further passes. Similarly, the strength increased steeply after the first pass, but tended to saturate with further pressings. The FEM simulations also showed strain non-uniformities and the dependence of the resulting strength on the location within the workpiece.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2002.05a
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• pp.129-132
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• 2002

A unified elastic-viscoplastic ocnstitutive model based on dislocation density considerations is described. A combination of a kinetic equation, which describes the mechanical response of a material at a given microstructure in terms of dislocation glide and evolution equations for internal variables characterizing the microstructure provide the constitutive equations of the Model. Microstructural features of the material, such as the grain size, spacing between second phase particles etc., are directly implemented in the constitutive equations. The internal variables are associated with the total dislocation density in the simple version of the model. The model has a modular structure and can be adjusted to describe a particular type of metal forming processes.

• Journal of the Korea Institute of Military Science and Technology
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• v.9 no.2 s.25
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• pp.70-76
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• 2006

The microstructure evolution during a hot forging of Waspaloy was investigated using the recrystallization model and FEM simulation. In order to obtain an uniform microstructure, hot forging was carried out by two step. The change of grain size during hot forging has a deep connection with dynamic recrystallization behavior. Avrami-type constitutive equation for the dynamic recrystallization was implemented into an user subroutine of 2D FE simulator. The evolution of grain structure in the two-step forging of Waspaloy was simulated using the 2D FEM user-subroutine. The detailed variation of microstructures due to dynamic recrystallization could effectively be predicted at various locations in a forged pancake.

• Transactions of Materials Processing
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• v.10 no.1
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• pp.35-41
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• 2001

The high temperature deformation behavior of SCM 440 can be characterized by the hot torsion test in the temperature ranges of $900^{\circ}C$~$1100^{\circ}C$ and strain rate ranges of 0.05/sec~5/sec. The aim of this paper is to establish the quantitative equation of the volume fraction of dynamic recrystallization (DRX) as a function of processing variables, such as strain rate ($\varepsilon$), temperature (T), and strain ('$\varepsilon$). During hot deformation, the evolution of microstructure could be analyzed from work hardening rate ($\theta$). For the exact prediction of dynamic softening mechanism the critical strain ($\varepsilon_c$), the strain for maximum softening rate ($\varepsilon^*$ and Avrami' exponent (m') were quantitatively expressed by dimensionless parameter, Z/A, respectively. The transformation-effective strain-temperature curve for DRX could be composed. It was found that the calculated results were agreed with the experimental data for the steel at any deformation conditions.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.05a
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• pp.411-414
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• 2008

In order to study the effect of lubrication during hot rolling, ferritic stainless steel (FSS) sheet were hot-rolled with and without application of lubrication. The effect of two hot rolling processes on the evolution of texture and microstructure after hot rolling, cold rolling and subsequent recrystallization annealing was studied by means of macro-texture analysis and microstructure observations. After hot rolling, the specimen rolled with lubrication showed rolling textures at the sheet surface, while the specimen rolled without lubrication displayed shear textures in the outer layers of the sheet. Hot rolling with lubrication was beneficial to the formation of strong recrystallization textures at sheet surface. However, hot rolling with lubrication led to the formation of orientation colonies in outer thickness layers of the recrystallized sheet.

• Journal of Powder Materials
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• v.21 no.4
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• pp.271-276
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• 2014

15Cr-1Mo base oxide dispersion strengthened (ODS) steel which is considered to be as a promising candidate for high- temperature components in nuclear fusion and fission systems because of its excellent high temperature strength, corrosion and radiation resistance was fabricated by using mechanical alloying, hot isostatic pressing and hot rolling. Torsion tests were performed at room temperature, leading to two different shear strain routes in the forward and reverse directions. In this study, microstructure evolution of the ODS steel during simple shearing was investigated. Fine grained microstructure and a cell structure of dislocation with low angle boundaries were characterized with shear strain in the shear deformed region by electron backscattered diffraction (EBSD). Grain refinement with shear strain resulted in an increase in hardness. After the forward-reverse torsion, the hardness value was measured to be higher than that of the forward torsion only with an identical shear strain amount, suggesting that new dislocation cell structures inside the grain were generated, thus resulting in a larger strengthening of the steel.