• Title/Summary/Keyword: Microstructure

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Formation of Shear Texture and Microstructure in AA3004 Sheet (AA3004에서 전단변형 미세조직 및 집합조직의 형성)

  • 이강노;김종국;김훈동;황병복;허무영
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2002.05a
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    • pp.184-186
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    • 2002
  • The evolution of texture and microstructure during warm rolling and subsequent annealing in aluminium 3004 alloy sheet was investigated by X-ray texture measurements and microstructure observations. Warm rolling at 250$^{\circ}C$ led to the development of strong through thickness texture gradients with shear textures at the surface layer and a regular rolling texture in the center of the sheets. FEM simulations indicated that these texture gradients are caused by pronounced strain gradients throughout the sheet thickness. Upon recrystallization annealing, in the sheet center the characteristic cube-recrystallization texture developed, while in the surface layers with a pronounced shear texture continuous recrystallization took place which led to the formation of a very fine grained microstructure. It is concluded that the very complex strain history in the near-surface layers together with the resulting high work-hardening rate gave rise to the formation of the ultra-fine grains with an average size smaller than 2$\mu\textrm{m}$.

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The Effect of Temperature, Frequency and Microstructure on Fatigue Crack Propagation in Ti-6A1-4V Alloy (Ti-6A1-4V 합금의 피로거동에 미치는 온도, 주파수 및 미세조직의 영향)

  • 김현철;김승한;임병수;김두현;이용태
    • Transactions of the Korean Society of Automotive Engineers
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    • v.4 no.1
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    • pp.198-207
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    • 1996
  • The effect of temperature, frequency and microstructure on fatigue crack propagation property of Ti-6A1-4V alloy has been investigated. The temperatures employed were room temperature, 20$0^{\circ}C$ and 40$0^{\circ}C$. The frequencies were 20Hz and 8 Hz. The microstructures tested were equiaxed and bimodal microstructures. Mechanical properties and fatigue crack growth rates were measured in different test conditions. From the experimental results, following conclusions were obtained. Bimodal microstructure showed superior fatigue crack growth resistance to equiaxed microstructure. Under all test conditions, fatigue crack growth rate increased with test temperature. Wine the frequency decreasing from 20Hz to 8Hz, fatigue crack growth rate increased.

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A Study on the Microstructure of Terminological Dictionaries (전문용어사전의 미시구조에 관한 연구)

  • 김성진;정동열
    • Journal of the Korean Society for Library and Information Science
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    • v.35 no.1
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    • pp.143-162
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    • 2001
  • As technical intellectual work now has become prolific and various, rapid evolution of technical terms needs to collect and manage them systematically and efficiently. The purpose of this study is to suggest the microstructure for systematic definitions of definiendum in terminological dictionaries. This study reveals specific properties or differences of terminography on the basis of terminology and lexicography, analyzes problems of microstructure in a current terminological dictionary, and, based upon the theoretical and practical analysis, attempts to derive structural and methodical suggestions for microstructure of terminological dictionaries.

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Strength and Microstructure of Reactive Powder Concrete Using Ternary Pozzolanic Materials

  • So, Hyoung-Seok;Janchivdorj, Khulgadai;Yi, Je-Bang;Jang, Hong-Seok;So, Seung-Young
    • Journal of the Korea Institute of Building Construction
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    • v.13 no.1
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    • pp.48-57
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    • 2013
  • To consider the practicality and economic feasibility of developing reactive powder concrete (RPC), the strength and microstructure properties of RPC using ternary pozzolanic materials (silica fume, blast furnace slag, fly ash) were investigated in this study. Through the investigation, it was found that the compressive strength of RPC using ternary pozzolanic materials was increased significantly compared to that of the original RPC containing silica fume only. A considerable improvement in the flexural strength of RPC using ternary pozzolanic materials was found, and then the utilization of a structural member subjected to bending was expected. The X-ray diffractometer (XRD) analysis and Scanning Electronic Microscope (SEM) revealed that the microstructure of RPC was denser using the ternary pozzolanic materials than the original RPC.

Corrosion Characteristics of hot rolled and thermo-mechanically treated steel rebar in concrete pore solution (콘크리트 기공 솔루션에서의 열간 압연 및 열 기계 처리 철근의 부식 특성)

  • Lee, Han-Seung;Singh, Jitendra Kumar
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2018.05a
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    • pp.202-203
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    • 2018
  • Chemistry and microstructure of steel reinforcement bars play an important role to control the corrosion in concrete environments. In present study, we have chosen two different microstructure of steel rebars produced from companies and assessed their corrosion characteristics in simulated concrete pore (SCP) solution with prolonged exposure periods. Hot rolled steel rebar showed more corrosion resistance compare to thermo-mechanically treated (TMT) one. The growth of passive is greater in hot rolled (A) than TMT (B) due to orientation of microstructure. TMT steel rebar exhibit distorted microstructure with many micro cells which enhances the galvanic coupling and induce the deterioration while on the other hand hot rolled rebars exhibit fine grain boundary which responsible in growth of uniform, adherent and protective passive film resultant improved impedance was observed.

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Effects of Sintering Additives on the Microstructure Development in Silicon Oxynitride Ceramics

  • Kim, Joosun;Chen, I-Wei
    • The Korean Journal of Ceramics
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    • v.6 no.3
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    • pp.224-228
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    • 2000
  • Using a small amount of additives and amorphous Si₂N₂O powders, O-SiAlON ceramics have been hot-pressed and its microstructure and mechanical properties were investigated. Scandium oxide was demonstrated to be an effective densification additive for O-SiAlON. Amorphous Si₂N₂O was densified at relatively low temperatures and a microstructure with acicular grains was developed. Fine grains found in materials obtained from amorphous powders suggest that nucleation and crystallization of O-SiAlOH is relatively easy compared with the Si₃N₄-SiO₂reaction.

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Effect of Microstructure on Corrosion Behavior of TiN Hard Coatings Produced by Two Grid-Attached Magnetron Sputtering

  • Kim, Jung Gu;Hwang, Woon Suk
    • Corrosion Science and Technology
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    • v.5 no.1
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    • pp.15-22
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    • 2006
  • The introduction of two-grid inside a conventional process system produces a reactive coating deposition and increases metal ion ratio in the plasma, resulting in denser and smoother films. The corrosion behaviors of TiN coatings were investigated by electrochemical methods, such as potentiodynamic polarization test and electrochemical impedance spectroscopy (EIS) in deaerated 3.5% NaCl solution. Electrochemical tests were used to evaluate the effect of microstructure on the corrosion behavior of TiN coatings exposed to a corrosive environment. The crystal structure of the coatings was examined by X-ray diffractometry (XRD) and the microstructure of the coatings was investigated by scanning electron microscopy (SEM) and transmission electron spectroscopy (TEM). In the potentiodynamic polarization test and EIS measurement, the corrosion current density of TiN deposited by two grid-attached magnetron sputtering was lower than TiN deposited by conventional magnetron type and also presented higher Rct values during 240 h immersion time. It is attributed to the formation of a dense microstructure, which promotes the compactness of coatings and yields lower porosity.

Study on the bainitic microstructure in low carbon HSLA steels (저탄소.저합금 강의 베이나이트 미세 구조 연구)

  • Kang, J.S.;Ahn, S.S.;Yoo, J.Y.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.154-157
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    • 2007
  • The austenite phase observed in low carbon HSLA steels is well known to be decomposed to various bainitic microstructures, such as granular bainite, acicular ferrite and bainitic ferrite during continuous cooling process. These bainitic microstructures have been usually identified by using either scanning electron microscope (SEM) or transmission electron microscope (TEM). However, SEM and TEM images do no exactly coincide, because of the quite different sample preparation method in SEM and TEM observations. These conventional analysis method is, thus, not suitable for characterization of the complex bainitic microstructure. In this study, focused ion beam (FIB) technique was applied to make site-specific TEM specimens and to identify the 3-dimensional grain morphologies of the bainitic microstructure. The morphological feature and grain boundary characteristics of each bainitic microstructure were exactly identified.

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Microstructure of Fat Free Plain Set-type Yogurt Containing Folic Acid

  • Kayanush J. Aryana
    • Food Science of Animal Resources
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    • v.24 no.3
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    • pp.273-276
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    • 2004
  • The objective of this study was to investigate the microstructure of folic acid-contained yogurt. Folic acids (25 and 50%) were added to milk preparation prior to pasteurization, then starter culture was added. The microstructure of yogurt containing folic acid was determined by the size of cluster of casein micelle using scanning electron microscopy and transmission electron microscopy. The cluster of casein micelle in yogurt containing folic acid were showed larger size than in control (p<0.05). In addition of 50% of folic acid, cluster of casein micelle per unit area was exhibited the highest number among tested yogurts. From these results, folic acid concentration of yogurt may be affected by mouth-feel of yogurt texture as well as the aggregation of casein micelle.

Effect of Powder Synthesis Processing on the Microstructure and Electrical Conductivity of Sintered $CNTs/Fe/Al_2O_3$ Nanocomposites

  • Choa, Yong-Ho;Yoo, Seung-Hwa;Yang, Jae-Kyo;Park, Jin-Woo;Oh, Sung-Tag;Kang, Kae-Myung;Kang, Sung-Goon
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1087-1088
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    • 2006
  • The microstructure and electrical conductivity of CNTs dispersed $Al_2O_3$ nanocomposites depending on the powder processing and CNTs content were demonstrated. The composite powders with homogeneous dispersion of CNTs could be synthesized by a catalytic route for direct formation of CNTs on nano-sized Fe dispersed $Al_2O_3$ powders. The sintered nanocomposite using the composite powder with directly synthesized CNTs showed homogeneous microstructure and enhanced elelctrical conductivity. The influence of powder processing on the properties of sintered nanocomposites was discussed by the observed microstructural features.

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