• Title/Summary/Keyword: Microstructural & Mechanical properties

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Manufacturing of Ni-Cr-B-Si + WC/12Co Composite Coating Layer Using Laser Cladding Process and its Mechanical Properties (레이저 클래딩 공정을 이용한 Ni-Cr-B-Si + WC/12Co 복합 코팅층의 제조 및 기계적 특성)

  • Ham, Gi-Su;Kim, Chul-O;Park, Soon-Hong;Lee, Kee-Ahn
    • Journal of Powder Materials
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    • v.24 no.5
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    • pp.370-376
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    • 2017
  • In this study we manufacture a Ni-Cr-B-Si +WC/12Co composite coating layer on a Cu base material using a laser cladding (LC) process, and investigate the microstructural and mechanical properties of the LC coating and Ni electroplating layers (reference material). The initial powder used for the LC coating layer is a powder feedstock with an average particle size of $125{\mu}m$. To identify the microstructural and mechanical properties, OM, SEM, XRD, room and high temperature hardness, and wear tests are implemented. Microstructural observation of the initial powder and LC coating layer confirm the layer is composed mainly of ${\gamma}-Ni$ phases and WC and $Cr_{23}C_6$ carbides. The measured hardness of the LC coating and Ni electroplating layers are 653 and 154 Hv, respectively. The hardness measurement from room up to high temperatures of $700^{\circ}C$ result in a hardness decrease as the temperature increases, but the hardness of the LC coating layer is higher for all temperature conditions. Room temperature wear results show that the wear loss of the LC coating layer is 1/12 of the wear level of the Ni electroplating layer. The measured bond strength is also greater in the LC coating than the Ni electroplating.

Microstructure Control and Tensile Property Measurements of Hot-deformed γ-TiAl alloy (열간가공된 γ-TiAl 합금의 미세조직 제어 및 기계적 특성 평가)

  • Park, Sung-Hyun;Kim, Jae-Kwon;Kim, Seong-Woong;Kim, Seung-Eon;Park, No-Jin;Oh, Myung-Hoon
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.6
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    • pp.256-262
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    • 2019
  • The microstructural features and texture development by both hot rolling and hot forging in ${\gamma}-TiAl$ alloy were investigated. In addition, additional heat treatment after hot forging was conducted to recognize change of the microstructure and texture evolution. The obtained microstructural features through dynamic recrystallization after hot deformed ${\gamma}-TiAl$ were quite different because two kinds of formation process were occurred depending on deformation condition. However, analyzed texture tends to be random orientation due to intermediate annealing up to ${\alpha}+{\beta}$ region during the hot deformation process. After additional heat treatment, microstructure transformed into fully lamellar microstructure and randomly oriented texture was also observed due to the same reason as before. Tensile test at room temperature demonstrated that anisotropy of mechanical properties were not appeared and transgranular fracture was occurred between interface of ${\alpha}_2/{\gamma}$. As a result, it could be suggested that microstructural features influenced much more than texture development on mechanical properties at room temperature.

Variation in Microstructural Homogeneity and Mechanical Properties of Extruded Mg-5Bi Alloy Via Controlling Billet Shape (빌렛 형상 제어를 통한 Mg-5Bi 합금 압출재의 조직 균일도 및 기계적 물성 변화)

  • Jin, S.C.;Cha, J.W.;Park, S.H.
    • Transactions of Materials Processing
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    • v.31 no.6
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    • pp.344-350
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    • 2022
  • Extruded Mg-Bi binary alloys are known to have an undesirable bimodal grain structure containing a large amount of coarse unrecrystallized grains. Accordingly, to improve the microstructural homogeneity of extruded Mg-Bi alloys, it is necessary to promote the dynamic recrystallization (DRX) behavior during hot extrusion. An effective way to promote DRX is an increase in nucleation sites for DRX through a pre-deformation process before extrusion, such as cold pre-forging and hot pre-compression. However, the application of these pre-deformation processes increases the cost of final extruded Mg products because of an increase in energy consumption and decrease in productivity. Therefore, a low-cost new continuous process with high productivity is required to improve the microstructural homogeneity and mechanical properties of extruded Mg alloys without a drastic increase in the entire process cost. This study proposes a new extrusion method using an extrusion billet with a truncated cone shape (i.e., tapered billet) instead of a conventional extrusion billet with a cylindrical shape. When the hot extrusion of a Mg-5Bi alloy is conducted using the tapered billet, the DRX behavior during extrusion is considerably promoted. The DRX fraction and average grain size of the extruded alloy significantly increase and decrease from 65% to 91% and from 225 ㎛ to 49 ㎛, respectively. Consequently, the extruded Mg-5Bi alloy fabricated using the tapered billet has a finer homogeneous grain structure and higher tensile elongation than the extruded counterpart fabricated using the cylindrical billet.

Mechanical properties related to the microstructure of seven different fiber reinforced composite posts

  • de la Pena, V?ctor Alonso;Darriba, Iria L;Valea, Martin Caserio;Rivera, Francisco Guitian
    • The Journal of Advanced Prosthodontics
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    • v.8 no.6
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    • pp.433-438
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    • 2016
  • PURPOSE. The aim of this in vitro study was to evaluate the mechanical properties (bending strength and hardness) of seven different fiber reinforced composite posts, in relation to their microstructural characteristics. MATERIALS AND METHODS. Two hundred eighty posts were divided into seven groups of 40, one group for each type of post analyzed. Within each group, 15 posts were subjected to three-point bending strength test, 15 to a microhardess meter for the Knoop hardness, and 10 to Scanning Electron Microscope in order to determine the diameter of the fibers and the percentage of fibers embedded in the matrix. To compare the flexural strength in relation to the type of fiber, matrix, and the hardness of the posts, a Kruskal-Wallis H test was used. The Jonckheere-Terpstra test was used to determine if the volume percent of fibers in the post influenced the bending strength. RESULTS. The flexural strength and the hardness depended on the type of fibers that formed the post. The lower flexural strength of a post could be due to deficient bonding between the fiber and the resin matrix. CONCLUSION. According to the results, other factors, besides the microstructural characteristics, may also influence the mechanical properties of the post. The feature that has more influence on the mechanical properties of the posts is the type of fiber.

Effect of Ca Addtion on Microstructure and Mechanical Properties of Mg-11Li-3Zn-1Sn-0.4Mn Based Alloys (Mg-11Li-3Zn-1Sn-0.4Mn 마그네슘 합금의 Ca 첨가에 따른 미세조직 및 기계적 특성평가)

  • Kim, Jung-Han;Kim, Yong-Ho;Yoo, Hyo-Sang;Son, Hyeon-Taek;Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.25 no.6
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    • pp.269-273
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    • 2015
  • The effect of adding Ca on the microstructural and mechanical properties of as-cast Mg-11Li-3Zn-1Sn(wt%) alloys were investigated. Mg-11Li-3Zn-1Sn-0.4Mn with different Ca additions (0.4, 0.8, 1.2 wt%) were cast under an $SF_6$ and $Co_2$ atmosphere at $720^{\circ}C$. The cast billets were homogenized at $400^{\circ}C$ for 12h and extruded at $200^{\circ}C$. The microstructural and mechanical properties were analyzed by OM, XRD, SEM, and tensile tests. The addition of Ca to the Mg-11Li-3Zn-1Sn-0.4Mn alloy resulted in the formation of $Ca_2Mg_6Zn_3$, MgSnCa intermetallic compound. By increasing Ca addition, the volume fraction and size of $Ca_2Mg_6Zn_3$ with needle shape were increased. This $Ca_2Mg_6Zn_3$ intermetallic compound was elongated to the extrusion direction and refined to fine particles due to severe deformation during hot extrusion. The elongation of the 0.8 wt% Ca containing alloy improved remarkably without reduction strength due to the formation of fine grain and $Ca_2Mg_6Zn_3$ intermetallic compounds by Ca addition. It is probable that fine and homogeneous $Ca_2Mg_6Zn_3$ intermetallic compounds played a significant role in the increase of mechanical properties.

Mechanical Behavior of A356 depending on the Variation of Microstructure (A356 합금 미세조직변화에 따른 기계적 특성에 관한 연구)

  • Kim K. J.;Kwon Y. N.;Lee Y. S.;Lee J. H.;Lee S. H.;Lee J. H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.05a
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    • pp.273-276
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    • 2004
  • A356 alloy is one of the most popular casting aluminum alloys due to its good castability. It is well known that the mechanical properties of A356 alloy strongly depend on its characteristic microstructure, such as the size of eutectic Si, primary $\alpha$ dendrite and so on. These microstructural features are determined during the casting and solidification process, which implies the strong relationship with mechanical properties with solidification methods. In the present study, the mechanical characteristics of A356 alloy was investigated by using squeeze cast control arm in terms of the microstructural features, such as the size of eutectic Si, primary a dendrite. By doing so, the most favorable microstructure of A356 could be determined for Al control arm that should be one of the most reliable parts in automobile.

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Similar and Dissimilar Welding Properties of Zirconium by TIG Welding (텅스텐아크용접에 의한 Zirconium의 동종 및 이종용접 특성 분석)

  • Kim, Jin Yeong;Hwang, Hyo-Woon;Lee, Dae Hyun;Lee, Jae Gwan;Lee, Dong-Geun
    • Journal of the Korean Society for Heat Treatment
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    • v.34 no.4
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    • pp.165-170
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    • 2021
  • Zirconium has excellent mechanical strength and high heat resistance and excellent corrosion resistance, and it is very important to study zirconium's dissimilar welding properties since it can be used in various applications under harsh environments. Similar welding of pure zirconium and dissimilar metal welding of pure zirconium and pure titanium were performed by TIG welding, and the welding properties were studied in association with microstructural and mechanical properties. In the Zr/Zr welded specimen, sound FZ and HAZ regions showed a basketweave microstructure composed of plate α phase. FZ region of Zr/Ti dissimilar welded specimen exhibited a maximum hardness value of 354.8 Hv, which is about three times higher than that of Ti base metal, due to the precipitation of very fine metastable ω and α phases in the beta matrix. In addition, due to the microstructural continuity in the FZ and HAZ regions, excellent elongation property of 21% was exhibited.