• 접착 및 계면
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• 제12권3호
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• pp.88-93
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• 2011

페놀수지에 함침된 탄소나노튜브 (CNT)의 최적 분산제조공정은 전기저항 측정으로 구해졌으며, 플라즈마 처리된 탄소섬유와 CNT-페놀수지 나노복합재료간의 계면특성이 전기-미세역학시험법에 의해 연구되었다. 탄소섬유의 젖음성은 플라즈마 처리 후에 현격하게 증가되었다. 탄소섬유와 CNT-페놀수지 나노복합재료의 표면에너지는 Wilhelmy 플레이트 시험법으로 측정되었다. 탄소섬유 표면의 활성화로 인하여 플라즈마 처리 후 전진 접촉각은 $65^{\circ}$에서 $28^{\circ}$로 감소되었다. 이는 정적 접촉각과 상호 일치함을 보여 주었다. 플라즈마 처리된 탄소섬유와 CNT-페놀수지 나노복합재료간의 접착일은 플라즈마 처리전보다 증가하였다. 또한, 계면전단강도와 겉보기 강성도 탄소섬유에 대한 플라즈마 처리로 증가하였다.

• 접착 및 계면
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• 제23권4호
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• pp.122-129
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• 2022

본 연구에서는 산소 플라즈마 처리시간을 실험 변수로 하여 금속섬유를 처리한 후 섬유표면에 산소함유 기능성 관능기를 도입하여 금속섬유의 친수성을 향상시키기 위한 연구로 플라즈마 처리 전, 후의 표면 특성 변화를 scanning electron microscope (SEM)과 x-ray photoelectron spectroscopy (XPS)를 사용하여 관찰하였다. 또한 플라즈마 처리시간이 금속섬유의 표면에 미치는 영향을 관찰하기 위해 극성 용매와 비극성 용매에 대한 금속섬유의 접촉각 변화를 측정하였다. 측정된 접촉각을 이용해 표면 자유에너지 변화를 계산한 후 산소 플라즈마 처리 전, 후의 금속섬유에 대한 접촉각과 표면 자유에너지를 비교하였으며 접착일과의 상관관계도 고찰하였다. 이런 금속섬유의 표면 변화가 다른 소재와의 복합 시 계면에서의 전단강도 향상에 미치는 영향을 알아보기 위해 microdroplet 시편을 제조하여 계면 전단강도를 측정하였으며 접착일과의 상관관계도 함께 파악하였다. 따라서, 금속섬유의 산소플라즈마 처리는 섬유표면에 물리적인 표면적 증가로 인한 수지와의 접촉면의 증가와 표면의 산소함유 기능성 관능기의 도입에 따른 접촉각, 표면 에너지의 변화에 따른 표면 친수화로 고분자 수지와의 계면 전단강도를 향상시켜주는 결과를 얻었다.

• 한국전산구조공학회논문집
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• 제31권1호
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• pp.17-21
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• 2018

오늘날까지 적층 마이크로 외팔보의 고유진동수에 대하여 연구가 진행되었다. 마이크로 보는 실리콘 재질로 만들어 지지만, 그것의 상하 표면은 얇은 금 박막층(~30nm)이 증착되어 있다. 초음파 검사를 위해 초음파 테스트 플랫폼을 사용했으며, 시간영역 신호는 광학적으로 측정되었다. 고유진동수는 파형을 고속 Fourier 변환을 통해 정량화하였으며, 결과적으로 고전적인 보 이론과 일치하는 결과를 보여 주었다. 본 연구는 마이크로/나노스케일 재료와 마이크로 구조에 대한 동적평가기법을 제공할 것으로 기대된다.

• Advances in aircraft and spacecraft science
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• 제4권5호
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• pp.585-611
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• 2017

This article covenants with the post buckling witticism of carbon nanotube reinforced composite (CNTRC) beam supported with an elastic foundation in thermal atmospheres with arbitrary assumed random system properties. The arbitrary assumed random system properties are be modeled as uncorrelated Gaussian random input variables. Unvaryingly distributed (UD) and functionally graded (FG) distributions of the carbon nanotube are deliberated. The material belongings of CNTRC beam are presumed to be graded in the beam depth way and appraised through a micromechanical exemplary. The basic equations of a CNTRC beam are imitative constructed on a higher order shear deformation beam (HSDT) theory with von-Karman type nonlinearity. The beam is supported by two parameters Pasternak elastic foundation with Winkler cubic nonlinearity. The thermal dominance is involved in the material properties of CNTRC beam is foreseen to be temperature dependent (TD). The first and second order perturbation method (SOPT) and Monte Carlo sampling (MCS) by way of CO nonlinear finite element method (FEM) through direct iterative way are offered to observe the mean, coefficient of variation (COV) and probability distribution function (PDF) of critical post buckling load. Archetypal outcomes are presented for the volume fraction of CNTRC, slenderness ratios, boundary conditions, underpinning parameters, amplitude ratios, temperature reliant and sovereign random material properties with arbitrary system properties. The present defined tactic is corroborated with the results available in the literature and by employing MCS.

• 한국고분자학회:학술대회논문집
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• 한국고분자학회 2006년도 IUPAC International Symposium on Advanced Polymers for Emerging Technologies
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• pp.15-16
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• 2006

Since two-photon polymerization (TPP) emerged as a new technology over a decade ago, a large variety of micro-objects including 3-D micro-optical components, micromechanical devices, and 3-D photonic crystals have been fabricated using TPP with a high spatial resolution of approximately submicron scale to 100 nm. Recent efforts have been made to improve the fabrication efficiency and precision of micro-objects obtained with TPP; in particular, many studies have been carried out with the aim of developing efficient two-photon absorbing chromophores. In this presentation, we will discuss our efforts to develop highly efficient two-photon absorbing materials and also describe recent attempts to enhance the resolution and to improve the fabrication efficiency of nanofabrications based on TPP.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2003년도 추계학술발표대회 논문집
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• pp.42-45
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• 2003

Nondestructive damage sensing and mechanical properties for acid-treated carbon nanotube (CNT) and nanofiber (CNF)/epoxy composites were investigated using electro-micromechanical technique and acoustic emission (AE). Carbon black (CB) was used to compare to CNT and CNF. The results were compared to the untreated case. The fracture of carbon fiber was detected by nondestructive acoustic emission (AE) relating to electrical resistivity under double-matrix composites test. Sensing for fiber tension was performed by electro-pullout test under uniform cyclic strain. The sensitivity for fiber damage such as fiber fracture and fiber tension was the highest for CNT/epoxy composites. Reinforcing effect of CNT obtained from apparent modulus measurement was the highest in the same content. For surface treatment case, the damage sensitivity and reinforcing effect were higher than those of the untreated case. The results obtained from sensing fiber damage were correlated with the morphological observation of nano-scale structure using FE-SEM. The information on fiber damage and matrix deformation and reinforcing effect of carbon nanocomposites could be obtained from electrical resistivity measurement as a new concept of nondestructive evaluation.

• Structural Engineering and Mechanics
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• 제38권6호
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• pp.803-823
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• 2011

In this paper, the three dimensional Parallel Realistic Failure Process Analysis ($RFPA^{3D}$-Parallel) code based on micromechanical model is employed to investigate the bonding behavior in FRP sheet bonded to concrete in single shear test. In the model, the heterogeneity of brittle disordered material at a meso-scale was taken into consideration in order to realistically demonstrate the mechanical characteristics of FRP-to-concrete. Modified Mohr-coulomb strength criterion with tension cut-off, where a stressed element can damage in shear or in tension, was adopted and a stiffness degradation approach was used to simulate the initiation, propagation and growth of microcracks in the model. In addition, a Master-Slave parallel operation control technique was adopted to implement the parallel computation of a large numerical model. Parallel computational results of debonding of FRP-concrete visually reproduce the spatial and temporal debonding failure progression of microcracks in FRP sheet bonded to concrete, which agrees well with the existing testing results in laboratory. The numerical approach in this study provides a useful tool for enhancing our understanding of cracking and debonding failure process and mechanism of FRP-concrete and our ability to predict mechanical performance and reliability of these FRP sheet bonded to concrete structures.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2011년도 제40회 동계학술대회 초록집
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• pp.447-447
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• 2011

We studied to detect the mass variation using micro mechanical resonator. For measuring the resonance frequency of the micro mechanical system, optical method using laser interference is selected. A simple resonator is prepared by attaching an AFM cantilever on the piezo stack. The piezo stack makes a the cantilever vibrated with its resonance frequency. To change the mass of the resonator, gold was evaporated on the cantilever. We measured how much resonance frequency was changed according to the amount of gold attached on cantilever. This resonator is able to perform the role of a mass sensor and has a resolution of the order of micrograms. The fabrication of the resonator and measurement setup for detecting the mechanical resonance will be introduced in this presentation.

• Geomechanics and Engineering
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• 제14권2호
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• pp.203-209
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• 2018

Reliable estimation of compressive as well as tensile in-situ stresses is critical in the design and analysis of underground structures and openings in rocks. Kaiser effect technique, which uses acoustic emission from rock specimens under cyclic load, is well established for the estimation of in-situ compressive stresses. This paper investigates the Kaiser effect on marble specimens under cyclic uniaxial compressive as well as cyclic uniaxial tensile conditions. The tensile behavior was studied by means of Brazilian tests. Each specimen was tested by applying the load in four loading cycles having magnitudes of 40%, 60%, 80% and 100% of the peak stress. The experimental results confirm the presence of Kaiser effect in marble specimens under both compressive and tensile loading conditions. Kaiser effect was found to be more dominant in the first two loading cycles and started disappearing as the applied stress approached the peak stress, where felicity effect became dominant instead. This behavior was observed to be consistent under both compressive and tensile loading conditions and can be applied for the estimation of in-situ rock stresses as a function of peak rock stress. At a micromechanical level, Kaiser effect is evident when the pre-existing stress is smaller than the crack damage stress and ambiguous when pre-existing stress exceeds the crack damage stress. Upon reaching the crack damage stress, the cracks begin to propagate and coalesce in an unstable manner. Hence acoustic emission observations through Kaiser effect analysis can help to estimate the crack damage stresses reliably thereby improving the efficiency of design parameters.

• 접착 및 계면
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• 제9권3호
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• pp.20-26
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• 2008

형상기억합금(SMA)의 구조는 부가된 온도 혹은 응력에 의해 마텐자이트로부터 오스테나이트로의 변화가 가능하다는 것은 잘 알려져 있다. 형상기억합금섬유의 자체 형상회복력으로 인해 응력과 온도가 적용되는 동안에 응력이나 경화 모니터링 센서 또는 작동기로서 사용되었다. 초탄성 현상은 연속적인 기계적 하중 하에서나 온도변화 중에 응력-변형률 곡선에서 확인되었다. 반복하중 실험을 통해 응력-변형률 곡선에서 나타난 초탄성 현상 구간이 나타나는 응력 이력현상이 발생함을 확인하였다. 이것은 형상기억합금섬유 혹은 에폭시에 함침된 형상기억합금섬유 복합재료가 반복하중으로 계면물성 저하로 인한 형상기억 회복 성능의 저하를 의미한다. 강성도가 큰 에폭시 사용과 형상기억합금섬유의 표면처리 이후 형상기억합금섬유와 에폭시 사이의 계면결합력의 증대에도 불구하고 유사한 불완전한 초탄성을 보여 주었다. 단-형상기억합금섬유/에폭시 복합재료 내부에 남은 잔류 열과 이에 따른 잔류 응력으로 인해 에폭시에 함침된 단-형상기억합금섬유에서는 경화과정에서 불완전한 회복을 나타났다.