• Title/Summary/Keyword: Microcrack

Search Result 169, Processing Time 0.027 seconds

Superconductivity and Surface Morphology of YBCO/CeO$_2$ Thin Films on Sapphire Substrate by Pulsed Laser Deposition (사파이어 기판 위에 펄스-증착법으로 성장한 YBCO/CeO2박막의 초전도성과 표면 모폴러지)

  • Kang, Kwang-Yong;J. D. Suh
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
    • /
    • 2003.02a
    • /
    • pp.88-91
    • /
    • 2003
  • The crystal structure and properties of YBa$_2$Cu$_3$$O_{7-x}$(YBCO) and CeO$_2$ thin films deposited on r-plane (1(equation omitted)02) sapphire substrate by pulsed- laser deposition(PLD) have been investigated. C-axis oriented epitaxial YBCO thin films with critical temperature (Tc) of 88 K were routinely grown on (200) oriented CeO$_2$ buffer layers with thickness in the range between 20 to 80 nm. When the thickness of the (200)oriented CeO$_2$ buffer layer increases over than 80 nm, the superconducting properties of YBCO thin films on that were deteriorated. The decrease in Tc of YBCO thin films was explained by the microcrack formation in CeO$_2$ buffer layer. These results indicate that the thickness of the (200) oriented CeO$_2$ buffer layer is critical to the epitaxial YBCO thin nim growth on r-plane (1(equation omitted)02) sapphire substrate.e.

  • PDF

Fabrication of YSZ buffer layer for YBCO coated conductor by MOCVD method (MOCVD법에 의한 YBCO coated conductor용 YSZ 완충층 제작)

  • 선종원;김형섭;정충환;전병혁;김찬중
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
    • /
    • 2003.02a
    • /
    • pp.129-132
    • /
    • 2003
  • Yttria stabilized zirconia (YSZ) buffer layers were deposited by a metal organic chemical vapor deposition (MOCVD) technique using single liquid source for the application of YBa$_2$Cu$_3$$O_{7-x}$ (YBCO) coated conductor. Y:Zr mole ratio was 0.2:0.8, and tetrahydrofuran (THF) was used as a solvent. The (100) single crystal MgO substrate was used for searching deposition condition. Bi-axially oriented CeO$_2$ and NiO films were fabricated on {100}〈001〉 Ni substrate by the same method and used as templates. At a constant working pressure of 10 Torr, the deposition temperatures (660~80$0^{\circ}C$) and oxygen flow rates (100~500 sccm) were changed to find the optimum deposition condition. The best (100) oriented YSZ film on MgO was obtained at 74$0^{\circ}C$ and $O_2$ flow rate of 300 sccm. For YSZ buffer layer with this deposition condition on CeO$_2$/Ni template, full width half maximum (FWHM) values of the in-plane and out-of-plane alignments were 10.6$^{\circ}$ and 9.8$^{\circ}$, respectively. The SEM image of YSZ film on CeO$_2$/Ni showed surface morphologies without microcrack.k.

  • PDF

Effects of the Type of Martensite on Fatigue Limit of Ferrite-Martensitic Steel (페라이트-마르텐사이트 복합 조직강의 피로한도에 미치는 마르텐사이트 조직형태의 영향)

  • Kim, Min-Gun;Ji, Jueng-Keun
    • Journal of Industrial Technology
    • /
    • v.20 no.B
    • /
    • pp.87-94
    • /
    • 2000
  • A study has been made on the behavior of microscopic fatigue crack growth at the stress level of the fatigue limit with ferrite-martensitic structures. For the above purpose, two types of the microstructures were prepared ; one is the microstructure having the ferrite encapsulating the islands of second phase martensite(FEM), the other is the microstructure with the martensite encapsulating the islands of ferrite(MEF). It has been pointed out that the fatigue limits of these microstructures are related to the critical stress at which the microcrack in the ferrite proceeds to the martensite. The high fatigue limit might be excepted for the MEF microstructure in which the critical crack length would be restricted within the second phase spacing in contrast with the FEM microstruture. However, the fatigue tests shows that no appreciable difference of the fatigue limits among them were recognized. Also, it turned out from the metallographic observations that the micro crack path is very much affected by the microstructures, so that the microcracks grow according to the 3-dimentional situation of its microstructures.

  • PDF

Constitutive Modeling of Asphalt Concrete with Time-Dependent Damage Growth (손상이 증가하는 아스팔트 콘크리트의 점탄성 구성모델)

  • 이현종
    • Computational Structural Engineering
    • /
    • v.10 no.4
    • /
    • pp.229-238
    • /
    • 1997
  • Mechanical behavior of asphalt concrete that accounts for viscoelasticity and damage evolution under cyclic loading conditions is modeled and presented in this paper. An elastic-viscoelastic correspondence principle in terms of pseudo variables is applied to separately evaluate viscoelasticity and time-dependent damage growth in asphalt concrete. A microcrack growth law, which is commonly employed in linear viscoelastic fracture mechanics, is successfully used for describing the damage growth in the body. A constitutive equation in terms of stress and pseudo strain is first established for controlled-strain mode, and then transformed to controlled-stress constitutive equation by simply replacing stress and pseudo strain with pseudo stress and strain. The transformed constitutive equation in terms of pseudo stress satisfactorily predicts the mechanical behavior of asphalt concrete all the way up to failure under controlled-stress modes.

  • PDF

Crack Healing Behavior with Healing Temperature in Si3N4/SiC Composite Ceramics (Si3N4/SiC 복합 세라믹의 온도에 따른 크랙 힐링 관찰과 확산거동)

  • Song, Oh-Sung;Ando, Kotoji;Takahashi, Koji;Nakao, Wataru;Ryu, Ji-Ho
    • Korean Journal of Materials Research
    • /
    • v.15 no.12
    • /
    • pp.780-785
    • /
    • 2005
  • To investigate the microcrack healing behavior of $Si_3N_4-20wt\%SiC-8wt\%Y_2O_3$ composite ceramics(SNCY8), we observe the crack length evolution a! the time of 20, 40, 60 minutes with in-situ optical microscopy by varying healing temperature of $800\~1200^{\circ}C$. Crack healing obviously occurred as heating temperature and time increased. We proposed a simple model of effective diffusion based on the crack length evolution with healing condition, and determined the effective diffusion coefficient as Our result implies that we may predict the healing ability quantitatively with temperature and time in structural ceramics through the effective diffusion coefficient model.

Enhanced Durability Performance of High Early Strength Concrete for Early Traffic Opening (조기교통개방 콘크리트의 내구성능 향상에 관한 연구)

  • 원종필;김현호;안태송
    • Journal of the Korea Concrete Institute
    • /
    • v.13 no.4
    • /
    • pp.362-370
    • /
    • 2001
  • The internal or external restraint of thermal and dry shrinkage movements could thus generate tensile stresses in concrete pavement for early traffic opening. Restrained shrinkage and thermal stresses could produce microcracks in concrete which increase its permeability and accelerate its long-term deterioration under weathering and load effects. Fiber reinforced concrete is an effective approach to the control of microcrack and crack development under tensile stresses. This study aims at evaluation of the durability of high early strength concrete for early traffic opening and increase of service life. Three different types of regulated-set cement which recently has been used much in Korea were adopted. Fibers were added and their mixtures were compared with plain high early strength concrete mixture. The use of fibers increased durability performance of high early strength concrete using regulated-set cement than the corresponding plain mixtures.

A review of pathophysiological mechanism of Bisphosphonate-related osteonecrosis of the jaw (임상가를 위한 특집 1 - 비스포스포네이트 관련 골괴사의 병태생리학적 기전에 대한 검토)

  • Kwon, Tae-Geon
    • The Journal of the Korean dental association
    • /
    • v.52 no.4
    • /
    • pp.192-202
    • /
    • 2014
  • Bisphosphonate(BP) significantly influence the hone remodeling process. Increasing number of patients with osteoporosis and metastatic bone disease need high dose or long term bisphosphonate therapy. Major adverse effect is jaw bone necrosis and now the bisphosphonate-related necrosis of the jaw(BRONJ) is the major concern of dental practitioner. This study intended to perform the review of the current understandings concerning the pathophysiology of BRONJ. Even though pathophysiological mechanism of BRONJ is not clearly elucidated but now suggested as largely two different concepts; so-called "inside-out" or "outside-in" theory. Inside-out theory emphasize the osteonecrosis of the jaw is the initial major event and subsequent infection and inflammation is the second event that accompanies bone exposure and death of overlying mucosa. However, in "outside-in" theory, infection or inflammation initiated by traumatized oral epithelium is the major event of BRONJ. Both theory would be partially explain BRONJ. Recent research reveals the immune modulating effect and influence of microcrack accumulation by BP. These findings and those of others might explain the missing part of outside-in theory.

Mechanical and Electrical Characteristics of $Al_2O_3-ZrO_2/A_2O_3$-TZP Structural Ceramics ($Al_2O_3-ZrO_2/A_2O_3$-TZP 세라믹스의 제조 및 기계적.전기적 특성)

  • 박재성;남효덕;이희영
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
    • /
    • 1999.11a
    • /
    • pp.335-338
    • /
    • 1999
  • The effect of monoclinic $ZrO_2$(pure) and tetragonal $ZrO_2$ containing 5.35wt% $Y_2$$O_3$(Y-TZP) addition on the mechanical properties and thermal shock resistance of $Al_2$$O_3$ ceramic were investigated. The addition of $ZrO_2$(m) and Y-TZP increased sintering density of $Al_2$$O_3$. The vickers hardness increased with increasing the volume fraction of Y-TZP going through a maximum at 20wt%. The hardness of the specimens was found to be depend on the sintering density. With increasing the volume fraction of $ZrO_2$(m) and Y-TZP, the fracture toughness of the composite is increased. This result may be taken as evidence that toughening of ${Al_2}{O_3}$ can also be achieved by the transformation toughening and microcrack toughening of $ZrO_2$. The property of the& shock for ${Al_2}{O_3}$-$ZrO_2$ composites was improved by increasing the volume fraction of monoclinic $ZrO_2$(pure).Grain size increased with increasing the volume fraction of $ZrO_2$.

  • PDF

Local brittle zone of offshore structural steel welds (해양구조용 강재의 국부취화영역에 관한 연구)

  • 김병천;엄정현;이종섭;이성학;이두영
    • Journal of Welding and Joining
    • /
    • v.7 no.2
    • /
    • pp.35-48
    • /
    • 1989
  • This study is concerned with a correlation of microstructure and local brittle zone (LBZ) in offshore structural steel welds. The influence of the LBZ on fracture toughness was investigated by means of simulated heat-affected zone (HAZ) tests as well as welded joint tests. Micromechanical processes involved in void and cleavage microcrack formation were also identified using notched round tensile tests and subsequent SEM observations. The LBZ in the HAZ of a multiphase welded joint is the interstitially reheated coarse grained HAZ, which is influenced by metallurgical factors such as effective grain size, the major matrix structure and the amount of high-carbon martensite-austenite (M-A) constituents. The experimental results indicate that Chirpy energy was found to scale monotonically with the amount of M-A constituents, confirming that the M-A constituent is the major microstructural factor controlling the HAZ toughness. In addition, voids and microcracks are observed to initiate at M-A constituents by the shear cracking process. Thus, the M-A constituent played an important role in initiating the voids and microcracks, and consequently caused brittle fracture.

  • PDF

The Effect of the DIC Speckle Patterns for a Microcrack Measurement (미소균열 측정에 대한 DIC 스펙클 형상의 영향)

  • Lee, Jun Hyuk;Kwon, Oh Heon
    • Journal of the Korean Society of Safety
    • /
    • v.34 no.4
    • /
    • pp.15-21
    • /
    • 2019
  • In order to secure the safety of various machinery, it is very important to develop a technique for accurately and quickly measuring the cracks generated in the mechanical equipment and evaluating the mechanical characteristics. The evaluation of the mechanical properties is accompanied by an appropriate strain measurement according to the material and crack occurrence of the target structure. Especially, when micro cracks are generated, the evaluation method is very important. Digital image correlation is an optical full field displacement measuring method which is using currently with speckles in the interested area. However the evaluation method and conditions of image distributions have to be considered carefully to measure the crack occurrence because the images of the speckle patterns affect the quality of displacement results. In this study, the speckle pattern density is characterized to improve the accuracy of the measurement method. And also the micro crack initiation is detected by the measured displacement in the adopted speckle pattern distribution. It is shown that the proposed method is useful to determine the density pattern distribution for the accurate measurement and crack detection.