• Korean Journal of Materials Research
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• v.22 no.10
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• pp.513-518
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• 2012

Recently, automobile parts have been required to have high strength and toughness to allow for weight lightening or improved stability. But, traditional micro-alloyed steel cannot be applied in automobile parts. In this study, we considered the influence of quenching temperature and cooling rate for specimens fabricated by vacuum induction furnace. Directly quenched micro-alloyed steel for hot forging can be controlled according to its micro structure and the heat-treatment process. Low carbon steel, as well as alloying elements for improvement of strength and toughness, was used to obtain optimized conditions. After hot forging at $1,200^{\circ}C$, the ideal mechanical properties (tensile strength ${\geq}$ 1,000 MPa, Charpy impact value ${\geq}\;100\;J/cm^2$) can be achieved by using optimized conditions (quenching temperature : 925 to $1,050^{\circ}C$, cooling rate : ${\geq}\;5^{\circ}C/sec$). The difference of impact value according to cooling rate can be influenced by the microstructure. A fine lath martensite micro structure is formed at a cooling rate of over $5^{\circ}C/sec$. On the other hand, the second phase of the M-A constituent microstructure is the cause of crack initiation under the cooling rate of $5^{\circ}C/sec$.

• Journal of Technologic Dentistry
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• v.31 no.3
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• pp.9-14
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• 2009

This study evaluated the mechanical properties of Ti-Cu alloys with the hope of developing an alloy for dental casting with better mechanical properties than unalloyed titanium. Ti-Cu alloys with four concentrations of Cu(2,5,10wt%) were made in an argon-arc melting furnace. The microstructure and micro-Vickers hardness were determined. X-ray diffraction pattern test was performed on the polished specimens. The microstructure of 2%Cu and 5%Cu alloys are shown acicular ${\alpha}Ti$ phase formed on the surfaces of previously formed $\beta$grains. The 10%Cu alloys has essentially a eutectoid structure; this structure includes lamella of ${\alpha}Ti$ and $Ti_2Cu$ phase that transformed from ${\alpha}Ti$ at the eutectoid temperature. The micro-Vickers hardness of CP Ti specimens was significantly(p<0.05) lower than that of any of the other alloys. Among the Ti-Cu alloys, the 10%Cu alloys exhibited a significantly(p<0.05) higher hardness value. but lower than that of Ti-6%Al-4%V alloy. From these results, it was concluded that new alloys for dental castings should be designed as Ti-Cu based alloys if other properties necessary for dental castings were obtained.

• Journal of the Korea institute for structural maintenance and inspection
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• v.4 no.1
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• pp.121-129
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• 2000

In general. service life of the sea-shore concrete structures is largely influenced by the corrosion of reinforcing steel due to the chloride contamination, and the penetration of chloride ions into concrete is governed by concrete condition state as a micro-structure. In this study, characteristics of chloride diffusion in concrete are analyzed in accordance with the mixing properties and durability of concrete, by considering the facts that micro-structure of concrete varies with the mixing properties and can indirectly be analyzed by using the durability test. In order to predict the service life of existing concrete structures, chloride diffusion equation for the concrete structures under various service conditions and the major parameters used in that equation are formulated as the mathematical models. Based on the results of chloride diffusion analysis in accordance with the mixing properties and durability of concrete and mathematical models formulated in this study, a prediction system is developed to predict the corrosion initiation of reinforcing steel in the sea-shore concrete structures.

• Applied Science and Convergence Technology
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• v.23 no.1
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• pp.54-59
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• 2014

The roll-to-roll (R2R) fabrication method to make micro-scale pillar arrays for biomimetic functionalization of surfaces is presented. Inspired by the micro-structure of plants in nature, a surface with a synthetic micro-scale pillar array is fabricated via maskless photolithography. After the surface is SAM (self-assembled monolayer) coated with trichlorosilane in a vacuum desiccator, it displays a hydrophobic property even in R2R replicas of original substrate, whose properties are further characterized using various pitches and diameters. In order to perform a comparison between the original micro-pattern and its replicas, surface morphology was analyzed using scanning electron microscopy and wetting characteristics were measured via a contact angle measurement tool with a $10{\mu}L$ water droplet. Efficient roll-to-roll imprinting for a biomimetic functionalized surface has the potential for use in many fields ranging from water repelling and self-cleaning to microfluidic chips.

• Journal of the Korea Concrete Institute
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• v.17 no.5 s.89
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• pp.857-868
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• 2005

This paper deals with the accumulated damage in concrete structures due to the cyclic freeze-thaw as an environmental load. The cyclic ice body nucleation and growth processes in porous systems are affected by the thermo-physical and mass transport properties, and gradients of temperature and chemical potentials. Furthermore, the diffusivity of deicing chemicals shows significantly higher value under cyclic freeze-thaw conditions. Consequently, the disintegration of concrete structures is aggravated at marine environments, higher altitudes, and northern areas. However, the properties of cyclic freeze-thaw with crack growth and diffusion of chloride ion effects are hard to be identified in tests, and there has been no analytic model for the combined degradations. The main objective is to determine the driving force and evaluate the reduced strength and stiffness by freeze-thaw. For the development of computational model of those coupled deterioration, micro-pore structure characterization, pore pressure based on the thermodynamic equilibrium, time and temperature dependent super-cooling with or without deicing salts, nonlinear-fracture constitutive relation for the evaluation of internal damage, and the effect of entrained air pores (EA) has been modeled numerically. As a result, the amount of ice volume with temperature dependent surface tensions, freezing pressure and resulting deformations, and cycle and temperature dependent pore volume has been calculated and compared with available test results. The developed computational program can be combined with DuCOM, which can calculate the early aged strength, heat of hydration, micro-pore volume, shrinkage, transportation of free water in concrete. Therefore, the developed model can be applied to evaluate those various practical degradation cases as well.

• Proceedings of the KSME Conference
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• 2004.04a
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• pp.252-257
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• 2004

Nanometer-sized structures are being applied to many devices including micro/nano electronics, optoelectronics, quantum devices, MEMS/NEMS, biosensors, etc. Especially, the thin film with submicron thickness is a basic structure for fabricating these devices, but its mechanical behaviors are not well understood. The mechanical properties of the thin film are different from those of the bulk structure and are difficult to measure because of its handling inconvenience. Several techniques have been applied to mechanical characterization of the thin film, such as nanoindentation test, micro/nano tensile test, strip bending test, etc. In this study, we focus on the strip bending test because of its high accuracy and moderate specimen preparation efforts, and measure Au thin film, which is a very popular material in micro/nano electronic devices. Au film is deposited on Si substrate by evaporation process, of which thickness is 100nm. Using the strip bending test, we obtain elastic modulus, yield and ultimate tensile strength, and residual stress of Au thin film.

• The Transactions of the Korean Institute of Electrical Engineers C
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• v.49 no.6
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• pp.367-374
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• 2000

This paper presents a method to fabricate freestanding structures by (100) silicon anisotropic etching and nickel electroless plating. The electroless plating process is simpler than the electroplating, and provides good coating uniformity and improved mechanical properties. Furthermore, the (100) silicon anisotropic etching in KOH solution with being aligned to <100> direction provides vertical (100) sidewalls on etched (100) surface. In this paper, the effects of the nickel electroless plating condition on the properties of electroless plated metal structures are investigated to apply fabrication of micro structures and then various micro structures are fabricated by nickel electroless plating. And then, the structures are released by silicon anisotropic etching in KOH solution with a large gap between the structure and the substrate. The fabricated cantilever structures are $210\mum$. wide, $5\mum$. thick and $15\mum$. over the silicon substrate, and the comb structure has the comb electrodes which are $4\mum$. wide and $4.3\mum$. thick separated by$1\mum$. It is released by silicon anisotropic etching in KOH solution. The gap between the structure and the substrate is $2.5\mum$.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.03b
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• pp.180-183
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• 1999

It is well known that Fe3Al intermetallic compound shows an anomalous peak of the yield strength at about 50$0^{\circ}C$ and then decrease at higher temperatures The dislocation structure was examined by transmission electron microscopy and high temperatures. The dislocation structure was examined by transmission electron microscopy and high temperature mechanical properties were examined by tensile and load relaxation tests. The flow stress curves obtained from load relaxation tests were then analyzed in terms of internal variable deformation theory. it was found that the flow curves consisted of three micro-deformation mechanisms -i. e inelastic deformation mode plastic deformation mode and dislocation creep deformation mode depending on both dislocation structure and deformation temperature. The flow curves could be well described by the constitutive equations of these three micro-deformation mechanisms based on the internal variable deformation theory.

• Steel and Composite Structures
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• v.28 no.3
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• pp.381-388
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• 2018

In this paper, forced vibration of micro cylindrical shell reinforced by functionally graded carbon nanotubes (FG-CNTs) is presented. The structure is subjected to transverse harmonic load and modeled by beam model. The size effects are considered based on strain gradient theory containing three small scale parameters. The mixture rule is used for obtaining the effective material properties of the structure. Based on sinusoidal shear deformation theory of beam, energy method and Hamilton's principle, the motion equations are derived. Applying differential quadrature method (DQM) and Newmark method, the frequency curves of the structure are plotted. The effect of different parameters including, CNTs volume percent and distribution type, boundary conditions, size effect and length to thickness ratio on the frequency curves of the structure is studied. Numerical results indicate that the dynamic deflection of the FGX-CNT-reinforced cylindrical is lower with respect to other type of CNT distribution.

• Journal of the Korean Society of Safety
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• v.32 no.1
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• pp.9-14
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• 2017

Diffusion bonding is a technique that has the ability to join materials with minimum change in joint micro-structure and deformation of the component. The quality of the joints produced was examined by metallurgical characterization and the joint micro-structure developed across the diffusion bonding was related to changes in mechanical properties as a function of the bonding time. An increase in bonding time also resulted in an increase in the micro-hardness of the joint interface from 55 VHN to 180 VHN, The increase in hardness was attributed to the formation of intermetallic compounds which increased in concentration as bonding time increased.