• Title/Summary/Keyword: Micro-droplet

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Flow Near the Meniscus of a Pressure-Driven Water Slug in Microchannels

  • Kim Sung-Wook;Jin Song-Wan;Yoo Jung-Yul
    • Journal of Mechanical Science and Technology
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    • v.20 no.5
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    • pp.710-716
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    • 2006
  • Micro-PIV system with a high speed CCD camera is used to measure the flow field near the advancing meniscus of a water slug in microchannels. Image shifting technique combined with meniscus detecting technique is proposed to measure the relative velocity of the liquid near the meniscus in a moving reference frame. The proposed method is applied to an advancing front of a slug in microchannels with rectangular cross section. In the case of hydrophilic channel, strong flow from the center to the side wall along the meniscus occurs, while in the case of the hydrophobic channel, the fluid flows in the opposite direction. Further, the velocity near the side wall is higher than the center region velocity, exhibiting the characteristics of a strong shear-driven flow. This phenomenon is explained to be due to the existence of small gaps between the slug and the channel wall at each capillary corner so that the gas flows through the gaps inducing high shear on the slug surface. Simulation of the shape of a static droplet inside a cubic cell obtained by using the Surface Evolver program is supportive of the existence of the gap at the rectangular capillary corners. The flow fields in the circular capillary, in which no such gap exists, are also measured. The results show that a similar flow pattern to that of the hydrophilic rectangular capillary (i.e., center-to-wall flow) is always exhibited regardless of the wettability of the channel wall, which is also indicative of the validity of the above-mentioned assertion.

Study of Nano-scale Fullerene (C60) Clusters Formed in Micro-sized Droplet by UV Irradiation

  • Yeo, Seung-Jun;Ahn, Jeung-Sun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.571-571
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    • 2012
  • We discovered the formation of C60 aggregates in solution by means of photoluminescence spectroscopic study on C60 in solutions. From the in-depth investigation of temperature dependence of the luminescence of C60 in toluene, benzene and CS2 solutions, we reported that the C60 aggregates are formed during cooling at the freezing temperature of these solvents. Furthermore, the C60 aggregates can be changed to stable structures by irradiating with UV pulse-laser (Nd:YAG laser, 355nm). As a consequence, we could obtain nano-scale photo-polymerized C60 clusters, which appear as round-shaped nano- scale particles in high resolution transmission electron-microscopy (HRTEM) images. However, the yield of the nano-scale C60 clusters obtained by this method is too small. So we designed and developed a system to obtain C60 cluster of macroscopic quantity by using ultrasonic nebulizer. In this system, C60 solution was vaporized to several micro-sized droplets in vacuum, resulting in the formation of C60 aggregates by evaporating solvent (toluene). The system was invented to produce nano-scale carbon clusters by the irradiation of UV light upon C60 aggregates in vacuum. We have characterized the products, C60 cluster, obtained from the system by using UV absorption spectra and HPLC spectra. Although the products have a possibility of inclusion various forms of C60 cluster, results support that the product formed from the system by using vaporizer method establishes a new method to obtain C60 cluster in macroscopic quantity. In the presentation, the details of the system and the results of characterization are reported.

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Removal of Anionic Dyes and Heavy Metal Ions Using Silica Nanospheres or Porous Silica Micro-particles Modified with Various Coupling Agents (다양한 커플링제로 표면 개질된 실리카들을 활용한 음이온성 염료 및 중금속의 제거)

  • Sung, Sohyeon;Lee, Minjun;Cho, Young-Sang
    • Korean Chemical Engineering Research
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    • v.59 no.4
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    • pp.596-610
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    • 2021
  • For application in adsorption process, we synthesized silica nanospheres by Stober method, and silica particles with wrinkled surface as well as macroporous silica particles were also fabricated by utilizing emulsion droplet as micro-reactors, followed by modification of the particle surface using suitable coupling agents containing amine groups. These particles exhibited improved adsorption capacity for heavy metal ions and anionic dyes, which were difficult to be removed by conventional silica particles without surface modification. Anionic dye, methyl orange could be removed almost completely by adsorption using porous silica particles modified using APTES. The adsorption efficiency of heavy metal like copper ions was close to 100%, when porous silica was used as adsorbent particles modified with AAPTS.

Development of a Nano Replication Printing(nRP) Process using a Voxel Matrix Scanning Scheme (복셀 메트릭스 스캐닝법에 의한 나노 복화(複畵)공정 재발)

  • 박상후;임태우;양동열;이신욱;공홍진
    • Journal of the Korean Society for Precision Engineering
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    • v.21 no.2
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    • pp.210-217
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    • 2004
  • In this study, a new process, named as nano replication printing(nRP) process, is developed for printing any figure in the range of several micrometers by using voxel matrix scanning scheme. In this newly developed process, a femto-second laser is scanned on a photosensitive monomer resin in order to induce polymerization of the liquid resin according to a voxel matrix which is transformed from bitmap format file. After the polymerization, a droplet of ethanol is dropt to remove the unnecessary remaining liquid resin and then the polymerized figures with nano-scaled precision are only remaining on the glass plate. By the nRP process, any figure file of bitmap format could be reproduced as nano-scaled precision replication in the range of several micrometers. Also, nano/micro-scaled patterns for an extremely wide range of applications would become a technologically feasible reality. Some of figures with nano-scaled precision were printed in scaled replication as examples to prove the usefulness of this study.

Development of Digital 3D Real Object Duplication System and Process Technology (디지털 3차원 실물복제기 시스템 및 공정기술 개발)

  • Lee Won-Hee;Ahn Young-Jin;Jang Min-Ho;Choi Kyung-Hyun;Kim Dong-Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.23 no.4 s.181
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    • pp.183-190
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    • 2006
  • Digital 3D Real Object Duplication System (RODS) consists of 3D Scanner and Solid Freeform Fabrication System (SFFS). It is a device to make three-dimensional objects directly from the drawing or the scanning data. In this research, we developed an office type SFFS based on Three Dimensional Printing Process and an industrial SFFS using Dual Laser. An office type SFFS applied sliding mode control with sliding perturbation observer (SMCSPO) algorithm for control of this system. And we measured process variables about droplet diameter measurement and powder bed formation etc. through experiments. In case of industrial type SFFS, in order to develop more elaborate and speedy system for large objects than existing SLS process, this study applies a new Selective Dual-Laser Sintering (SDLS) process and 3-axis Dynamic Focusing Scanner for scanning large area instead of the existing f lens. In this process, the temperature has a great influence on sintering of the polymer. Also the laser parameters are considered like that laser beam power, scan speed, and scan spacing. Now, this study is in progress to evaluate the effect of experimental parameters on the sintering process.

Effects of the Glass Fiber Characteristics on the Mechanical Properties of Thermoplastic Composite (유리섬유의 특성이 열가소성 복합재료의 기계적 성질에 미치는 영향)

  • Lee, Jung-Hui;Lee, Jeong-Gwon;Lee, Gyeong-Yeop
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.7 s.178
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    • pp.1697-1702
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    • 2000
  • This study has been performed to investigate the effects of glass fiber characteristics on the mechanical properties of thermoplastic composite. The surface of glass fiber was coated with the silan e to enhance the bonding strength between fiber and matrix. A micro-droplet pull-off test was performed to investigate the influence of the silane concentration on the bonding strength. The maximum bonding strength was observed around 10.8% silane concentration. In order to examine the influence of the fiber length and fiber content on the properties of the composite, the composite materials involving tile fiber lengths of 5mm, 10mm, 15mm 20mm, and 25mm were tested. The composites used contain 20%, 30%, and 40% by weight of glass fibers. Tension and flexural tests were performed to investigate their mechanical properties of the composites. The tensile strength and tensile modulus of the composite increase with increasing the glass fiber content. The tensile modulus increases slightly with increasing the fiber length. The maximum tensile strength is observed around the fiber length of 15-20mm. The flexural modulus and strength also increase slightly with increasing the fiber length.

Repeatability Study of a Pneumatic Dispensing System for Bio-Applications (바이오 응용을 위한 공압 디스펜싱 시스템의 반복 정밀도 연구)

  • Lee, Sang-Min;Choi, In-Ho;Kim, Joon-Won
    • Journal of Sensor Science and Technology
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    • v.21 no.1
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    • pp.53-58
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    • 2012
  • Biological and chemical assays(e.g., clinical tests for medical diagnosis) are needed to handle small liquid volume with high accuracy and high reliability. Many micro-dispensing systems using various actuation methods have been developed and applied. In this research, we confirm repeatability of the cartridge-type dispensing system with various measuring methods for guarantee of an acceptable reliability. We systematically examine the dispensed volume variation and dispense rate during 500,000 shots of sequential actuation. Using the same method, we confirm the repeatability of dispensed volume while varying operating conditions and design parameter(i.e., outlet size) of the dispensing system. Also, we examine the consistency of the dispensed volume of droplet while varying the operating pressures. Furthermore, we repeatedly measure differences between an actual dispensed volume and a target volume. According to our results, it is expected that the stable and reliable performance of our dispensing system can effectively be used in various applications containing bio-solutions.

Investigation on surface hardening and corrosion characteristic by water cavitation peening with time for Al 5052-O alloy (5052-O 알루미늄 합금의 워터 캐비테이션 피닝 시간에 따른 표면 경화와 부식 특성에 관한 연구)

  • Kim, Seong-Jong;Hyun, Koang-Yong
    • Corrosion Science and Technology
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    • v.11 no.4
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    • pp.151-156
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    • 2012
  • The cavity formed by the ultrasonic generation in the fluid with the application of water cavitation peening collides into the metal surface. At this time, the surface modification effect such as the work hardening presents by the compressive residual stress formed due to the localized plastic deformation. In this investigation, the water cavitation peening technology in the distilled water with the lapse of time was applied to 5052-O aluminum alloy for aluminum ship of a high value. So, the optimum water cavitation peening time on the effect for surface hardening and anti-corrosion property was investigated. Consequently, the water cavitatin peening time on excellent hardness and corrosion resistance characteristic presented 3.5 min. and 5.0 min, respectively. The surface hardness in the optimum water cavitation peening time was improved approximately 45% compared to the non-WCPed condition. In addition, corrosion current density was decreased.

The Effect of Thickness and Solidification Rate on the Rapidly Solidified Structure of Al-Cr Alloys (급냉응고(急冷凝固)한 Al-Cr계합금(系合金)의 응고조직(凝固組織)에 미치는 응고속도(凝固速度)와 두께의 영향)

  • Cho, Soon-Hyoung;Nam, Tae-Yoon;Yoon, Eui-Pak
    • Journal of Korea Foundry Society
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    • v.5 no.2
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    • pp.118-124
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    • 1985
  • The thickness ranges and conditions to form the supersaturated solid solution in Al-Cr alloys were investigated with various rapid solidification conditions. Al-Cr alloys, rapidly solidified by using the small droplet chill quenching method, were examined by means of micro-vickers hardness, lattice parameter, thermal analysis and microscopic observation. The results obtained were as follows; 1. With the increase of solidification rate, the solidified structures were changed to intermetallic compound + solid solution, incompletely supersaturated solid solution, completely supersaturated solid solution, in turn. 2. The minimum solidification rate required to form completely supersaturated solid solution was $2.5{\times}10^{-2}cm/sec$, $3.6{\times}10^{-2}cm/sec$ and $6.0{\times}10^{-2}cm/sec$ for Al-1.0wt%Cr, Al-1,2wt%Cr and Al-1.5wt%Cr, respectively. 3. The maximum distance from the chill surface required to form completely supersaturated solid solution was 5mm, 1.3mm and 0.3mm for Al-1.0wt%Cr, Al-1.2wt%Cr and Al-1.5wt% Cr, respectively.

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Optimal Conditions of Aerosol Flow Generation for High-density and Uniform Fog Screen (고밀도 균일 안개스크린을 위한 에어로졸 유동의 최적 생성조건)

  • Shin, Dongsoo;Song, Wooseok;Kim, Jinwon;Kim, Woojin;Koo, Jaye
    • Journal of ILASS-Korea
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    • v.22 no.1
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    • pp.13-21
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    • 2017
  • The fog screen is a device projecting the media to the aerosol flow field. As major parameters to generate dense and steady fog screen, shear stress, optical blockage ratio and SMD were obtained result through experiment. The micro droplet was generated by the piezo oscillation element, and the aerosol flow mixed with an air flow was sprayed into the vertical direction from the top of the fog screen through the 280 mm slot. For produce a dense, uniform fog screen, the shear effect, optical blockage ratio and SMD between aerosol and air curtain were measured. The minimum and maximum shear stress conditions were selected and it was confirmed that the optical transmission deviation of the aerosol flow field was small when the aerosol and air curtain flow rates were changed. When the aerosol and air curtain flow power were 18 V (1.51 m/s) and 24 V (2.55 m/s), respectively, under the condition of the minimum shear stress and laminar flow, the optical blockage ratios with the spray length were small, and it produced a most stable and high density uniform fog screen by injecting a constant of $10{\mu}m$ or less.