• Title/Summary/Keyword: Micro-cement

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A Study on Plasma Sprayed Porous Super Austenitic Stainless Steel Coating for Improvement of Bone Ingrowth (Bone ingrowth 향상을 위해 플라즈마 용사된 초내식성 오스테나이트 스테인리스강의 다공성 코팅층에 대한 연구)

  • 오근택;박용수
    • Journal of Surface Science and Engineering
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    • v.29 no.2
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    • pp.81-92
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    • 1996
  • The cementless fixation of bone ingrowth by porous coatings on artificial hip joint prostheses are replacing polymethylmethacrylate(PMMA) bone cement fixations. However, the major interests in the field of porous metal coating are environmental corrosivity accelerated by metal ion release, deterioration in the mechanical property of the coating, and the mechanical failure of the coatings as well as the substrate. Therefore, the selection of right materials for coatings and the development of porous coating techniques must be accomplished. Because of the existing problems in Ti and Ti alloys which are used extensively, this study is focused on the plasma spraying technique for coating on super stainless steel substrate. In order to determine the optimum conditions which satisfy the requirement for the porous coatings, under the plasma spraying, we selected the experimental parameters which extensively influenced on the characteristics of the coating through the pre-examination. Spray distance has been selected among 120, 160, and 200mm and primary gas flow rate among 70, 100, and 130 SCFH. Current and secondary gas($H_2$) flow rate was fixed at 400A, and 15 SCFH respectively. To understand the characteristics of the coatings, surface morphology, cross-sectional micro-structure, surface roughness, residual stress, and corrosion resistance were elucidated and the best conditions for the bone ingrowth improvement on artificial hip joint prostheses were found.

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The effect of high-temperature on foamed concrete

  • Canbaz, Mehmet;Dakman, Hafid;Arslan, Baris;Buyuksungur, Arda
    • Computers and Concrete
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    • v.24 no.1
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    • pp.1-6
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    • 2019
  • Within the scope of this study, the foam solution was prepared by properly mixing sulfonate based foam agent with water. Furthermore, this solution was mixed with the mixture of fine sand, cement, and water to produce foamed concrete. The mixture ratios which are the percentage of foam solution used in foam concrete were chosen as 0, 20, 40 and 60% by vol. After these groups reached 28 days of strength, they were heated to 20, 100, 400 and $700^{\circ}C$ respectively. Afterward, high-temperature effects on the foamed concrete were obtained by employing physical and mechanical properties tests. Additionally, SEM (scanning electron microscope) and EDX (energy-dispersive X-ray spectroscopy) tests were employed to analyze the microstructure, and ${\mu}-CT$ (micro computed tomography) images were used to reconstruct 3-D models of the heat-treated specimens. Then, these models are analyzed to examine the void structures and the changes in these structures due to the high temperatures. The study has shown that the void structures reduce the high-temperature effects and the foam solution could be mixed with concrete up to 40 % by vol. where the high strength of foamed concrete is non-mandatory.

Effect of steel fibres and nano silica on fracture properties of medium strength concrete

  • Murthy, A. Ramachandra;Ganesh, P.
    • Advances in concrete construction
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    • v.7 no.3
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    • pp.143-150
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    • 2019
  • This study presents the fracture properties of nano modified medium strength concrete (MSC). The nano particle used in this study is nano silica which replaces cement about 1 and 2% by weight, and the micro steel fibers are added about 0.4% volume of concrete. In addition to fracture properties, mechanical properties, namely, compressive strength, split tensile strength, and flexural strength of nano modified MSC are studied. To ensure the durability of the MSC, durability studies such as rapid chloride penetration test, sorptivity test, and water absorption test have been carried out for the nano modified MSC. From the study, it is observed that significant performance improvement in nano modified MSC in terms of strength and durability which could be attributed due to the addition pozzolanic reaction and the filler effect of nano silica. The incorporation of nano silica increases the fracture energy about 30% for mix without nano silica. Also, size independent fracture energy is arrived using two popular methods, namely, RILEM work of fracture method with $P-{\delta}$ tail correction and boundary effect method. Both the methods resulted in nearly the same size-independent $G_F$ irrespective of the notch to depth ratio of the same specimen. This shows evidence that either of the two procedures could be used in practice for analysis of cracked concrete structures.

Influence of mineral by-products on compressive strength and microstructure of concrete at high temperature

  • Sahani, Ashok Kr.;Samanta, Amiya K.;Roy, Dilip K. Singha
    • Advances in concrete construction
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    • v.7 no.4
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    • pp.263-275
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    • 2019
  • In the present work, Granulated Blast Furnace Slag (GBFS) and Fly ash (FA) were used as partial replacement of Natural Sand (NS) and Ordinary Portland Cement (OPC) by weight. One control mix, one with GBFS, three with FA and three with GBFS-FA combined mixes were prepared. Replacements were 50% GBFS with NS and 20%, 30% and 40% FA with OPC. Preliminary investigation on development of compressive strength was carried out at 7, 28 and 90 days to ensure sustainability of waste materials in concrete matrix at room temperature. After 90days, thermo-mechanical study was performed on the specimen for a temperature regime of $200^{\circ}-1000^{\circ}C$ followed by furnace cooling. Weight loss, visual inspection along with colour change, residual compressive strength and microstructure analysis were performed to investigate the effect of replacement of GBFS and FA. Although adding waste mineral by-products enhanced the weight loss, their pozzolanicity and formation history at high temperature played a significant role in retaining higher residual compressive strength even up to $800^{\circ}C$. On detail microstructural study, it has been found that addition of FA and GBFS in concrete mix improved the density of concrete by development of extra calcium silicate gel before fire and restricts the development of micro-cracks at high temperature as well. In general, the authors are in favour of combined replacement mix in view of high volume mineral by-products utilization as fire protection.

Effect of surface treatment on mechanical and micro-structural properties of basalt fiber reinforced mortars

  • Sukru Ozkan
    • Computers and Concrete
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    • v.34 no.2
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    • pp.195-212
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    • 2024
  • The use of basalt fibers in various types of fiber-reinforced mortars has been increasing. One of the factors that expands the use of basalt fibers is that it is a natural fiber and therefore the production costs are lower than fibers such as PVA fiber. Basalt fibers have some drawbacks such as reducing the workability of mortars in which basalt fibers are added due to their structure, and negatively affecting the mechanical properties when used above a certain proportional amount depending on the type of mixture. For this purpose, in this study, as a different application, the surface of basalt fibers with different lengths (6 and 12 mm) was treated with Triton X-100 surfactant, and these disadvantages were tried to be reduced. In the study, a two-step method was followed. In the first one, the effectiveness of adding untreated and treated basalt fiber at 1, 1.25, 1.5, 1.75 and 2% by weight to the mortar mixtures was determined by conducting flow spread and flow rate as fresh mortar characteristics. In the second one, microstructural characterization and mechanical tests were performed as hardened mortar properties. The results showed that the flow characteristics of basalt fiber reinforced mortars treated with surfactant improved compared to untreated basalt fiber reinforced mortars. In terms of mechanical properties, the addition of 2% treated basalt fiber by weight to the mixtures allowed to obtain %18, %12, and%48 higher values of compressive, flexural, and tensile strength values, respectively, compared to the same amount of untreated basalt fiber mixtures.

A Study on the Durability and Environmentally Friendly of Inorganic Grouting Material (무기질계 지반주입재의 내구성 및 친환경적 특성에 관한 연구)

  • Chun, Byungsik;Park, Dukhyum;Kang, Hyoungnam;Do, Jongnam
    • Journal of the Korean GEO-environmental Society
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    • v.9 no.5
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    • pp.37-43
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    • 2008
  • Inorganic injection material, which is one of the ground improvement materials, consists of cement accelerator and inorganic micro particle. The inorganic injection material is known to overcome the major limitations of water glass type improvement materials, which are leaching and accompanying strength loss. The inorganic injection material is superior in durability and strength, and environmentally friendly since leaching is prevented. In this study, the effectiveness and environment-friendliness of the MIS(Micro Injection-process System) using the inorganic injection material is compared to SGR, which uses the water glass. The performed tests were unconfined compression test, chemical resistance test, and fish poison test. The unconfined compression tests showed that the MIS results in 1.7 times higher 28 day strength compared to the SGR. In addition, the strength continually increased with time for the MIS, while it decreased for the SGR. The chemical resistance tests indicated that the rate of change in length using the MIS is 10~25 times smaller than when using the SGR. The fish poison test proved that MIS was more environmentally friendly. The analysis of chemical ingredients of leached showed that the amount of $Cr^{6+}$, Pb and Si leached from the MIS is less compared to the SGR. Accordingly, the MIS grout is more high-strength than existing SGR grout. It is excellent in shortening of construction period, structural stability of foundation and environmentally friendly. So, it is considered that it has not little the problem about groundwater pollution.

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Fundamental Research on Reactivity of Silica Source in the Rapidly Cured Inorganic Micro-Defect-Free(MiDF) Concrete (촉진 양생한 무기계 MiDF 콘크리트에서 실리카질 원료의 반응성에 관한 기초 연구)

  • Choi, Hong-Beom;Kim, Jin-Man
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.2
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    • pp.166-173
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    • 2019
  • In this paper, the reaction properties of silica source in the accelerated curing conditions using autoclave and the fundamental properties of inorganic Micro Defect Free(MiDF) concrete using silica source are studied. Studies show that Si ions elution rate from silica source in autoclave curing is higher in amorphous source. In tap water conditions, solids which is source after autoclaved curing show a higher mass reduction in amorphous materials, which is attributed to the higher elution rate of ion. In $Ca(OH)_2$ solution conditions, amorphous materials show higher mass increase, due to increase in C-S-H minerals. From experiment for influence on the properties of MiDF concrete by using nano silica materials, the specimen with silica fume shows an increase in compressive strength and a decrease in absorption depending on replacement rate up to 5.5%, while nano silica with amorphous phase and high-fineness shows a decrease in compressive strength and decrease in the water absorption. The specimen with nano silica increases the pore below 10,000nm, but reduces pore between 10,000 and 100,000nm. The above results show that the porosity and absorption rate of MiDF concrete can be reduced by using amorphous nano-size silica. However, to reduce the pore of 50 to 10,000nm, better dispersion of nano material in the cement matrix will be necessary. We will focus on the this item in the next research.

An Investigation on the Long Term Durability of High-strength Shotcrete Using Field and Combined Deterioration Test (현장실험과 복합열화시험을 통한 고강도 숏크리트의 장기내구성 검토)

  • Ma, Sang-Joon;Choi, Jae-Seok;Ahn, Kyung-Chul;Kim, Sun-Myung;Kim, Dong-Min
    • Journal of the Korean Geotechnical Society
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    • v.22 no.10
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    • pp.77-91
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    • 2006
  • Domestic practices in shotcrete use have developed in many respects even now, but it still has issues about material, construction, quality standard and so on. In overseas, the construction using high strength shotcrete with $39.2{\sim}58.8 MPa$ of compressive strength is becoming common based on the shotcrete technology of high strength and durability. However, domestic shotcrete design strength is low at around 20.6 MPa of compressive strength and a long term durability is also insufficient. In this paper, field tests using high-quality additives and accelerators were performed to obtain the improvement of shotcrete strength and EFNARC standard was used to evaluate the field test results. In addition, deterioration test combined with the freezing-thawing and carbonation was also performed in order to investigate a long-term durability of high-strength shotcrete. As a result of the field test, the promotion ratio of early strength was $90{\sim}97%$ in case of using alkali-free accelerators. And the compressive strength of the shotcrete using Micro-silica fume was $45.2{\sim}55.8MPa$ and flexible strength was $5.01{\sim}6.66MPa$, so the promotion ratio of strength was $37{\sim}79%$ and $17{\sim}61%$ respectively. The promotion effect of strength by silica fine additives ratio of $7.5{\sim}10%$ for cement mass was much superior to the other cases. It was especially examined that using Micro-silica fume reduced deterioration due to mixed steel fiber and improved a long-term durability of shotcrete.

A Study on Field Test of High-Strength Shotcrete using High-quality Additions and Accelerators (고품질 혼화재와 급결제를 적용한 고강도 숏크리트의 현장실험 연구)

  • Ma, Sang-Joon;Kim, Dong-Min
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.26 no.2C
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    • pp.121-131
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    • 2006
  • The strength standard of shotcrete in Korea is relatively lower than that in Europe where high-strength shotcrete has been developed and actively applied to the common practice, so it is hard to test a quality of high-strength shotcrete. In this study, field test was performed to find a solution improving the strength and a long-term durability on domestic shotcrete. In field test, a high-strength shotcrete was produced using high-quality additions and accelerators, and an effect of additions and accelerators was observed. In addition, quality test based on EFNARC was also performed. As a result of field test, a promotion ratio of early strength is 90~97% in case of using alkali-free accelerators, therefore, alkali-free accelerators had an effect on an increase of early strength on shotcrete. A compressive strength of shotcrete using Micro-silica fume was 45.2~55.8MPa and flexible strength was 5.01~6.66MPa, so a promotion ratio of strength was 37~79%, 17~61% respectively. It was showed that increment effect of strength by the silica fume replacement of 7.5~10% for cement mass was remarkable. As a result of test, it was possible to apply high-strength shotcrete to the domestic practice using high-quality additions such as Micro-silica fume and accelerators such as alkali-free.

Tensile Behavior of Hybrid Fiber Reinforced Cement Composite According to the Hooked Steel Fiber and Polyvinyl Alcohol Fiber Blending Ratio and Strain Rate (후크형 강섬유와 폴리비닐알코올 섬유의 혼합 비율과 변형속도에 따른 하이브리드 섬유보강 시멘트복합체의 인장거동)

  • Son, Min-Jae;Kim, Gyu-Yong;Lee, Sang-Kyu;Kim, Hong-Seop;Nam, Jeong-Soo
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.21 no.6
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    • pp.98-105
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    • 2017
  • In this study, the fiber blending ratio and strain rate effect on the tensile behavior of hybrid fiber reinforced cement composite was evaluated. Hooked steel fiber and polyvinyl alcohol fiber were used for reinforcing fiber. The fiber blending ratio of HSF+PVA were 1.5+0.5, 1.0+1.0 and 0.5+1.5vol.%. As a results, the tensile strength, strain capacity and fracture toughness of the hooked steel fiber reinforced cement composites were improved by the increase of the bond strength of the fiber and the matrix according to increase of strain rate. However, the tensile stress sharply decreased after the peak stress because of the decrease in the number of straightened pull-out fibers by micro cracks in the matrix around hooked steel fiber. On the other hand, PVA fiber showed cut-off fracture at strain rate $10^{-6}/s$ with multiple cracks. However, at the strain rate $10^1/s$, the multiple cracks and strain capacity were decreased because of the pull-out fracture of PVA fiber. The HSF1.5PVA0.5 shown the highest tensile strength because the PVA fiber suppressed the micro cracks in the matrix around the hooked steel fiber and improved the pull-out resistance of hooked steel fiber. Thus, DIF of strain capacity and fracture toughness of HSF1.5PVA were greatly improved. In addition, the synergistic response of fracture toughness was positive because the tensile stress was slowly decreased after the peak stress by improvement of the pull-out resistance of hooked steel fiber at strain rate $10^1/s$.