• Tunnel and Underground Space
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• v.27 no.3
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• pp.172-184
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• 2017

The hardness and mechanical properties of the minerals in the Daejeon granite according to depths were investigated by indentation test, load-unload test, and cycle test of dynamic ultra-micro hardness. As a result of the tests, it was possible to classify into three mineral groups (Group-1, -2, -3). The Martens hardness was not significantly different between 41 m and 223 m depths in three mode tests. Nevertheless, they showed in the order of a cycle test < load-unload test < indentation test. Considering the average Martens hardness, elastic modulus, and indentation work for each mineral group, their boundaries were relatively clear. In conclusion, A relatively accurate hardness of minerals can be obtained by three mode tests of dynamic ultra-micro hardness. In addtion, it was possible to characterize the elastic modulus and the elastic-plastic properties of the minerals from the load-unload and cycle tests.

• Journal of Power System Engineering
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• v.20 no.5
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• pp.5-13
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• 2016

This study is on wear damage of the material for a molding machine that be used at finally cutting of metal beam made in roll forming process of vehicle bump beam process line. SKD11 steel was used with the material for cutting mold jig. In the cutting mold jig, Ti diffusion heat treatment after vacuum heat treatment was carried out for upgrade of surface hardness and anti-wear. Also, the heat treatments by various methods were performed to compare the wear damage degree against above the existing heat treatment. Wear loss and friction coefficient were obtained from wear test. And, micro Vickers hardness values were compared with damaged parts or not of cutting mold jig. Micro Vickers hardness value appeared higher at the undamaged part by Ti diffusion heat treatment. The micro Vickers hardness well followed a two-parameter Weibull probability distribution.

• Journal of the Korean Society for Heat Treatment
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• v.11 no.1
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• pp.54-61
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• 1998

Since Cr-Mo-V steel has excellent fracture and creep properties at elevated temperature, they are extensively used as steam turbine components such as the turbine rotor. However, the turbine rotor steel used to suffer material degradation during long term service. Therefore, the assessment of the safety and residual life of the turbine rotor is periodically required during service. One of the most convenient techniques for that is the hardness method mainly due to its simplicity and nondestructive characteristics. In this research, six specimens with different aging times of turbine rotor steel were artificially prepared by an isothermal heat treatment at $630^{\circ}C$. The micro Vickers hardnesses of specimens were measured at room temperature. The relationships between the fracture properties and the hardness ratio were investigated. And also an indirect method to evaluate the residual life of degraded turbine rotor was proposed based on the micro Vickers hardness measurement.

• Transactions of Materials Processing
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• v.32 no.4
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• pp.180-190
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• 2023

This study deals with residual stress prediction and hardness evaluation within cross ball grooved inner race fabricated by cold upsetting process consisted of upsetting and ejection steps. A raw workpiece material of AISI 5120H (SCr420H) is first spheroidized and annealed, then phosphophyllite coated to form solid lubricant layer on its outer surface. To investigate influences of the heat treatment, uni-axial compression tests and Vickers micro-hardness measurements are conducted. Three-dimensional elasto-plastic FE simulations on the upsetting step and the ejection one are performed to visualize the residual stress and the ductile (plastic deformation) damage. External feature of the fabricated inner race is fully captured by using an optical 3D scanner, and the micro-hardness is measured on internal cross-sections. Consequently, the dimensional compatibility between the simulated inner race and the fabricated one is ensured with a difference of under 0.243mm that satisfied permissible error range of ±0.50mm on the grooved surface, and the predicted residual stress is verified to have similar distribution tendency with the measured Vickers micro-hardness.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2008.11a
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• pp.707-708
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• 2008

• Journal of Korea Foundry Society
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• v.15 no.6
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• pp.588-595
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• 1995

SiC particles reinforced Mg-Zr, Mg-Zn and Mg-Zn-Zr composites were manufactured by Rheocompocasting method. Effects of Zn, Zr addition on microstructures and hardness were investigated by using the micro Vickers hardness tester, the optical and scanning electron microscopy. By the Zr addition to the pureMg/SiCp composites, SiC particles become more homogeneously dispersed and grain refined so that the micro hardness of the composite increased. In case of Zn addition, although grain refinement and homogeneous dispersion effects of SiC particles were not obtained, hardness was more increased than the only Zr added composite by the formation of many Mg-Zn intermetallic compounds at grain boundary. In the Mg-Zn-Zr/SiCp composite, the highest value of hardness was obtained by triple effects such as grain refining, dispersion hardening of SiC particles and Mg-Zn compounds.

• Restorative Dentistry and Endodontics
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• v.36 no.2
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• pp.132-138
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• 2011

Objectives: The purpose of this study was to evaluate curing degree of three dual-cure resin cements with the elapsed time in self-cure and dual-cure mode by means of the repeated measure of micro-hardness. Materials and Methods: Two dual-cure self-adhesive resin cements studied were Maxcem Elite (Kerr), Rely-X Unicem (3M ESPE) and one conventional dual-cure resin cement was Rely-X ARC resin cement (3M ESPE). Twenty specimens for each cements were made in Teflon mould and divided equally by self-cure and dual-cure mode and left in dark, $36^{\circ}C$, 100% relative humidity conditional-micro-hardness was measured at 10 min, 30 min, 1 hr, 3 hr, 6 hr, 12 hr and 24 hr after baseline. The results of micro-hardness value were statistically analyzed using independent samples t-test and one-way ANOVA with multiple comparisons using Scheffe's test. Results: The micro-hardness values were increased with time in every test groups. Dual-cure mode obtained higher micro-hardness value than self-cure mode except after one hour of Maxcem. Self-cured Rely-X Unicem showed lowest value and dual-cured Rely-X Unicem showed highest value in every measuring time. Conclusions: Sufficient light curing to dual-cure resin cements should provided for achieve maximum curing.

• Journal of Power System Engineering
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• v.21 no.3
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• pp.37-44
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• 2017

In this study, failure analysis of the angular pin for molding machines to aluminum component molding was carried out. SM45C steel was used for the angular pin, it was surface hardened by the induction surface hardening heat treatment. The cross section of damaged angular pin was observed, and micro Vickers hardness value from the fractured part was measured. Brittle fracture was occurred from the fracture surface of angular pin, therefore, impact toughness value was evaluated by V-notch Charpy impact test. It was confirmed that the impact absorption energy was high when was tempered at a high temperature for a long time, and the toughness was slightly increased. Also, 2-parameter Weibull statistical analysis was investigated in order to evaluate the reliability of the measured micro Vickers hardness values and absorbed energy. The micro Vickers hardness and absorbed energy well followed a two-parameter Weibull probability distribution, respectively. The reverse design against angular pin was proposed as possible by using test results.

• Korean Journal of Materials Research
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• v.18 no.11
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• pp.604-609
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• 2008

The sintering behavior of zircon with silica was investigated. Zircon with 5 vol% of sedimentation $SiO_2$ resulted in the apparent density of $4.45\;g/cm^3$, the diametral tensile strength of $12.125\;kgf/cm^2$, and the micro Vickers hardness of 1283 HV. The dissociation temperature and mechanical characteristics of the $ZrSiO_4$ were changed with different kinds of $SiO_2$. $SiO_2$ addition prevented dissociation of $ZrSiO_4$. Zircon with 5 vol% of sedimentation $SiO_2$ and with 5 vol% of fused $SiO_2$ resulted in increased diametral tensile strength and increased micro Vickers hardness by suppression of $ZrSiO_4$ dissociation and low temperature liquid $SiO_2$ formation. Zircon with fumed $SiO_2$ and quartz $SiO_2$ resulted in decreased diametral tensile strength and decreased micro Vickers hardness because of cristobalite and quartz phase formation and high temperature liquid $SiO_2$ formation. Zircon with 10 vol% of $SiO_2$ resulted in decreased diametral tensile strength and decreased micro Vickers hardness because of weak particle coupling due to excess formation of liquid $SiO_2$.

• Journal of Powder Materials
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• v.21 no.2
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• pp.97-101
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• 2014

The 304 stainless steel powders were prepared by high energy ball milling and subsequently sintered by spark plasma sintering, and the microstructural characteristics and micro-hardness were investigated. The initial size of the irregular shaped 304 stainless steel powders was approximately 42 ${\mu}m$. After high energy ball milling at 800 rpm for 5h, the powders became spherical with a size of approximately 2 ${\mu}m$, and without formation of reaction compounds. From TEM analysis, it was confirmed that the as-milled powders consisted of the aggregates of the nano-sized particles. As the sintering temperature increased from 1073K to 1573K, the relative density and micro-hardness of sintered sample increased. The sample sintered at 1573K showed the highest relative density of approximately 95% and a micro-hardness of 550 Hv.