• Journal of the Korean institute of surface engineering
• /
• v.47 no.1
• /
• pp.13-19
• /
• 2014

The various surface treated conditions of Fe-3.0%Ni-0.7%Cr-1.4%Mn-X steel such as as-received, ion nitriding, DLC coated, DLC coated after nitriding for 3 hrs and 6 hrs were investigated to evaluate the beneficial effect for plastic mold steel. Micro Vickers hardness tester was used to estimate nitriding depth from the hardness profile and to measure hardness on the surface. Elastic modulus and residual stress were measured by a nanoindentator. Scratch test and SP (small ball punch test) were utilized to assess the adhesive strength of DLC coating. The depth of nitriding layer was measured as $50{\mu}m$ for the condition of 3 hrs nitriding and $90{\mu}m$ for that of 6 hrs nitriding. Hardness, elastic modulus, residual stress of DLC coating were 20.37 GPa, 162.78 GPa and -1456 MPa respectively. Residual stress on the surface of DLC coating after nitriding could increase to -3914 MPa by introducing nitriding before DLC coating. During the 'Ball-On-Disc' test ${\gamma}^{\prime}$ particles pulled out from the surface of nitrized layer tend to enhance abrasive wear mode since the fraction of ${\gamma}^{\prime}$ (Fe4N) in ion-nitrized layer is known to increases with nitriding time. Thus the specific wear rate of the nitriding layer increased. Comparing with nitriding the specific wear rate in work piece disc as well as ball decreased prominently in DLC coating due to the remarkable reduction in friction coefficient.

• Journal of the Korean Society for Nondestructive Testing
• /
• v.15 no.4
• /
• pp.549-560
• /
• 1996

The purpose of this study is to investigate the usefulness of small punch(SP) test using miniaturized specimens as a method for fracture strength evaluation of CANDU pressure tube embrittled by hydrogen. According to the test results, the fracture strength evaluation as a function of hydrogen concentration at $-196^{\circ}C$ was much better than that at room temperature, as the difference of SP fracture energy(Esp) with hydrogen concentration was more significant at $-196^{\circ}C$ than at room temperature for the hydrogen concentration up to 300ppm-H. It was also observed that the peak of average AE energy, the cumulative average AE energy and the cumulative average AE energy per equivalent fracture, strain increased with the increase of hydrogen concentration. From the results of load-displacement behaviors, Esp behaviors, macro- and micro-SEM fractographs and AE test it has been concluded that the SP test method using miniaturized specimen($10mm{\times}10mm{\times}0.5mm$) will be a useful test method to evaluate the fracture strength for CANDU pressure tube embrittled by hydrogen.

• Journal of Welding and Joining
• /
• v.13 no.1
• /
• pp.78-88
• /
• 1995

This paper was performed to study the utility of the SP(small punch) test and the AE(acoustic emission) test in the evaluation of SCC(stress corrosion cracking) susceptibility for parent metal and bond line of HT80 steel-weld joint by SAW(submerged arc welding) with the various pH values. The loading rate used was 3*10$^{-4}$ mm/min and the corrosive environment used was synthetic sea water during the SP test and the AE test. According to the test results, the SCC susceptibility of the parent metal was increased in the order of pH6.0, pH8.2 and pH10.0. On the other hand, the bond line showed almost the same high SCC susceptibility in all pH concentrations. Synthetically, from the results of the SCC susceptibility, the macro- and micro-SEM observation, the microfracture behaviors by AE test and the relationship between SCC susceptibility and displacement at incipient failure, .delta.$_{i.f-AE}$, it can be concluded that the SP test and the AE test are the good test methods to evaluate the SCC susceptibility for parent metal and bond line of the weld joint with the change of environmental factors.

• Journal of the Korean Society for Precision Engineering
• /
• v.22 no.12 s.177
• /
• pp.156-162
• /
• 2005

In this paper, we study the mechanism of lead deformation by numerically simulating the stamping process by means of a commercial finite element code. It is very important to analyze effects that the lead shape makes on the lead deformation, because the lead shape is often modified in order to minimize the deformation or to increase the buckling critical load of the punch. Therefore the stamping process, first, numerically simulated by considering as a quasi-static problem. Second, the effect on the lead deformation due to the lead shape variation, a linear lead geometry and a bent lead, was numerically analyzed and discussed. Finally, the punching order was optimized fur multi-lead generating stamping process. The results show that the bent lead is little bit more shifted than the linear lead after the punching process. But the bent lead is vertically less deformed than the linear lead. The punching order to successively generate the lead is good to keep the lead space uniform. The results will be very effectively applied for the design of the blanking or punching dies in industry.

• Transactions of Materials Processing
• /
• v.6 no.5
• /
• pp.446-455
• /
• 1997

A Combined extrusion operation consists of forward and backward extrusion forming and it is possible to make the process be simple by employing it. But the metal flow pattern induced by the operation is hard to analyze accurately because the flows are non-steady, which have at least two directions dependent upon each other. So engineers in the industrial factories had conducted the two extrusion operations separately. A new process was designed by the industrial expert for forming of an alu-minum preform using the combined extrusion operation. In this study, experiments and finite element analysis was carried out to determine the process parameters. Through the preliminary experiment, it was shown that warm forming condition was more desirable than cold or hot ones. And optimal shape of initial billet could be also determined. From the compatibility test, bonde-lube was chosen as the optimal lubricant and 20$0^{\circ}C$ as the material temperature by the inspection of micro-structure. The operation was simulated by the rigid-plastic finite element method to examine the metal flow. Disap-pearing of dead metal zone was observed as the punch fell down and desirable shape was obtained from the one operation. As a result of this study, 7 operations could be reduced and 225% of material saved.

• Journal of the Korean Society of Manufacturing Process Engineers
• /
• v.3 no.1
• /
• pp.66-71
• /
• 2004

Magnesium alloys have been widely used for many structural components of automobiles and aircraft because of high specific strength and good cast-ability in spite of hexagonal closed-packed crystal structure of pure magnesium. In this study, it is studied about the forming characteristics of press forging of AZ31 magnesium alloy by MSC/MARC in case of material having one boss and MSC/Supeiforge in case of material having multi-boss with heat transfer analysis during deformation at elevated temperature. For these results it is simulated about temperature distribution, strain distribution, and stress distribution of AZ31 Magnesium alloy. During the press forging, foot regions of bosses showed greater temperature rise than other areas of AZ31 sheet. Finally the plastic strain of AZ31 sheet did not remarkably vary with increasing temperature from 373 to 473K, while it significantly increased as the forming temperature increased from 473 to 573K, which is related with the change in micro-structures, such as dynamic re-crystallization occurring during the deformation process.

• Transactions of Materials Processing
• /
• v.16 no.8
• /
• pp.614-620
• /
• 2007

Deformation characteristics and damage evolution during warm backward extrusion of bulk AZ31 Mg alloy were investigated using finite element analyses. AZ31 Mg alloy was assumed as a hardening viscoplastic material. The tensile tests of AZ31 Mg alloy in previous experimental works showed the ductile fracture even at the warm temperature of $175^{\circ}C$. In this study, damage evolution model proposed by Lee and Dawson, which was developed based on the growth of micro voids in hardening viscoplastic materials, was combined into DEFORM 2D. Effects of forming temperature, punch speed, extrusion ratio and size of work piece on formability in warm backward extrusion as well as on mechanical properties of extruded products were examined. In general, finite element predictions matched the experimental observations and supported the analyses based on experiments. Distributions of accumulated damage predicted by the finite element simulations were effective to identify the locations of possible fracture. Finally, it was concluded that the process model, DEFORM2D combined with Lee & Dawson#s damage evolution model, was effective for the analysis of warm backward extrusion of AZ31 Mg alloys.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2004.11a
• /
• pp.260-265
• /
• 2004

LTCC(Low temperature co-fired ceramic) is being recognized as a significant packaging material of electrical devices for the advantages such as relatively low temperature being needed for process, low conductor resistance and high printing resolution. In the process of LTCC electrical devices, the punched via-hole quality is one of the most important factors on the performance of the device. However, its mechanism is very complicated and optimization of the process seems difficult. In this paper, to clarify the process, via-hole punching experiments were carried out and the punched holes were examined in terms of their burr formation. The effects of thickness of PET sheet and ceramic sheet and punch-to-die clearance on via-hole quality were also discussed. Optimum process conditions are proposed and a factor k is introduced to express effect of the process variables.

• Asian Pacific Journal of Cancer Prevention
• /
• v.16 no.17
• /
• pp.7619-7625
• /
• 2015

Background: Aberrant microRNA expression has been associated with the pathogenesis of a variety of human malignancies including oral squamous cell carcinoma (SCC). In this study, we examined primary oral SCCs for the expression of 6 candidate miRNAs, of which five (miR-34a, miR-143, miR-373, miR-380-5p, and miR-504) regulate the tumor suppressor TP53 and one (miR-99a) is involved in AKT/mTOR signaling. Materials and Methods: Tumor tissues (punch biopsies) were collected from 52 oral cancer patients and as a control, 8 independent adjacent normal tissue samples were also obtained. After RNA isolation, we assessed the mature miRNA levels of the 6 selected candidates against RNU44 and RNU48 as endogenous controls, using specific TaqMan miRNA assays. Results: miR-34a, miR-99a, miR-143 and miR-380-5p were significantly down-regulated in tumors compared to controls. Moreover, high levels of miR-34a were associated with alcohol consumption while those of miR-99a and miR-143 were associated with advanced tumor size. No significant difference was observed in the levels of miR-504 between the tumors and controls whereas miR-373 was below the detection level in all but two tumor samples. Conclusions: Low levels of miR-380-5p and miR-504 that directly target the 3'UTR of TP53 suggest that p53 may not be repressed by these two miRNAs in OSCC. On the other hand, low levels of miR-34a or miR-143 may relieve MDM4 and SIRT1 or MDM2 respectively, which will sequester p53 indicating an indirect mode of p53 suppression in oral tumors.